The application discloses a kind of
cobalt molybdenum oxide nanosheet self-supporting
electrocatalyst and its preparation method and application, it is related to electrocatalytic
biomass conversion technical field.The catalyst with foam
metal is conductive base, CoMoO4
Nanosheet is uniformly grown on its surface, and open pore network is formed by interweaving
Nanosheet each other, and part is self-assembled into three-dimensional micron flower hierarchical structure.The application is realized by hydrothermal and reduction
atmosphere heat treatment synergic control, and the integration self-supporting
electrode construction is realized, and the obtained catalyst is rich in
oxygen vacancy, and 5-
hydroxymethylfurfural (HMF) can be electrocatalytically oxidized to prepare 2,5-
furan dicarboxylic acid under extremely low driving potential, which shows excellent large current activity and
high selectivity, significantly inhibits
oxygen evolution competition reaction, and has long-term catalytic stability, and has wide industrialization prospect in
biomass high value utilization.