A kind of preparation method of cadmium molybdate modified copper-based composite electrical contact material
A technology of electrical contact materials and copper-based composites, applied in contacts, circuits, electrical switches, etc., can solve problems such as shortage of Ag resources, Cd vapor pollution, etc., achieve improved microstructure performance and service performance, high interface bonding strength, The effect of improving the degree of uniform dispersion
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Embodiment 1
[0016] Example 1 A preparation method of cadmium molybdate modified copper-based composite electrical contact material
[0017] Include the following steps
[0018] (1) Take the amount of Na in the formula 2 MoO 4 1.5g was dissolved in 100mL water to obtain a mixed solution, and the copper alloy powder (48g) was added with a formula dosage of 50% and stirred to form a suspension, and then 50mL CdCl 2 Add the aqueous solution into the suspension and continue to stir, and obtain a composite powder after filtering, washing, and drying; the CdCl 2 CdCl in aqueous solution 2 The mass fraction is 2.6%.
[0019] (2) After mixing the obtained composite powder with the remaining copper alloy powder (48g) in the formula, press molding at 400Mpa, sinter at 965°C for 0.5h, and heat-extrude the sintered composite material into a 50x6mm Plate, and then through rolling (pressed blanking amount is 0.2mm), annealing treatment (450 ℃, heat preservation 0.5h)), after stamping, obtain a φ5 ...
Embodiment 2
[0022] Example 2 A preparation method of cadmium molybdate modified copper-based composite electrical contact material
[0023] Include the following steps
[0024] (1) Take the amount of Na in the formula 2 MoO 4 3.7g was dissolved in 100mL water to obtain a mixed solution, and the copper alloy powder (38g) with a formula consumption of 40% was added and stirred to form a suspension, and then 50mL CdCl 2 Add the aqueous solution into the suspension and continue to stir, and obtain a composite powder after filtering, washing, and drying; the CdCl 2 CdCl in aqueous solution 2 The mass fraction is 6.5%.
[0025] (2) After mixing the obtained composite powder with the remaining copper alloy powder (57g) in the formula, press molding at 350Mpa, sinter at 950°C for 0.2h, and heat-extrude the sintered composite material into a 50x6mm Plate, and then through rolling (pressed blanking amount is 0.2mm), annealing treatment (440 ℃, heat preservation 0.5h)), after stamping, obtain ...
Embodiment 3
[0028] Example 3 A preparation method of cadmium molybdate modified copper-based composite electrical contact material
[0029] Include the following steps
[0030] (1) Take the amount of Na in the formula 2 MoO 4 6g is dissolved in 100mL water to obtain a mixed solution, add copper alloy powder (55g) with a formula consumption of 60% and stir to form a suspension, and then 50mL CdCl 2 Add the aqueous solution into the suspension and continue to stir, and obtain a composite powder after filtering, washing, and drying; the CdCl 2 CdCl in aqueous solution 2 The mass fraction is 10.4%.
[0031] (2) After mixing the obtained composite powder with the remaining copper alloy powder (37g) in the formula, press molding at 450Mpa, sinter at 970°C for 0.8h, and heat-extrude the sintered composite material into a 50x6mm Plate, and then after rolling (pressed blanking amount is 0.2mm), annealing treatment (460 ° C, heat preservation 1h)), after stamping, obtain a φ5 × 2mm contact el...
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