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Micro-encapsulation magnesium oxide and preparation method thereof

A technology of microencapsulation and magnesium oxide, which is applied in baking, food forming, food science and other directions, can solve problems such as complex methods, achieve the effects of simple process, ensure food safety, and improve suspension stability

Pending Publication Date: 2020-02-18
郑州瑞普生物工程有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

But the method is complex

Method used

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  • Micro-encapsulation magnesium oxide and preparation method thereof
  • Micro-encapsulation magnesium oxide and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1~5

[0029] Embodiments 1-5: Preparation of Microencapsulated Magnesium Oxide Samples 1-5

[0030] see figure 1 , the preparation method comprises the following steps:

[0031] 1. Hydrogenate palm oil in a water bath at 80-90°C to obtain liquid hydrogenated palm oil;

[0032] 2. Starch sodium octenyl succinate was dissolved in purified water heated to 80°C to obtain a solution;

[0033] 3. Add the magnesium oxide powder into the sodium starch octenyl succinate solution while stirring;

[0034] 4. Add liquid hydrogenated palm oil, turn on the emulsification shearing machine, set the speed at 2500-3000R / min, and the shearing time is 15-30min;

[0035] 5. The emulsified emulsion is transferred to the material temporary storage tank for spray drying; the inlet air temperature is 190°C, the outlet air temperature is 98°C, and the atomization frequency is 45HZ;

[0036] Among them, the mass ratio of magnesium oxide: hydrogenated palm oil: sodium starch octenyl succinate is 10-5:4-2:1...

Embodiment 6

[0040] Embodiment 6: Angle of repose detection of samples 1-5

[0041] According to the existing angle of repose measurement method: take 50g of samples 1-5 respectively, and test them on the standard funnel. The test results of samples 1-5 are all the same. The angle of repose of typical sample 1 is 26°, and the angle of repose is <30°. The material provided by the application can have better fluidity, which is convenient for mixing and processing.

Embodiment 7

[0042] Embodiment 7: the sedimentation velocity detection of sample 1~5

[0043] Take 1g of magnesium oxide, dissolve it in 100g of purified water, stir and mix, and record the sedimentation time. The sedimentation time of ordinary magnesium oxide is 10min. Take 1g of microcapsule magnesium oxide in samples 1-5 and dissolve it in 100g of purified water. Settling time, the settling time of samples 1-5 is similar, the settling time of typical sample 1 is greater than 2 hours.

[0044] It shows that the microcapsule magnesium oxide prepared by the method provided by the present application can be better dispersed in the solution, avoid rapid sedimentation, and can achieve higher stability in the solution.

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Abstract

The invention discloses a micro-encapsulation magnesium oxide and a preparation method thereof. The method comprises the following steps of: evenly mixing a starch sodium octenylsuccinate solution andmagnesium oxide powders under a stirring condition to obtain a mixture, adding a liquid hydrogenated palm oil into the mixture, and carrying out emulsifying and shearing processing on an emulsifyingand shearing machine to obtain a shearing mixture; carrying out spray drying on the shearing mixture to obtain the micro-encapsulation magnesium oxide; and adding the magnesium oxide, the hydrogenatedpalm oil and the starch sodium octenylsuccinate solution at a mass ratio of (10-5):(4-2):1, wherein the mass ratio of the starch sodium octenylsuccinate to water in the starch sodium octenylsuccinatesolution is 1:(15-30). By use of the method, a magnesium oxide fine powder is taken as a core material, and the starch sodium octenylsuccinate and the hydrogenated palm oil are compound wall materials and are prepared to obtain a magnesium oxide microcapsule through a spray drying method.

Description

technical field [0001] The application relates to a microencapsulated magnesium oxide and a preparation method thereof, belonging to the technical field of inorganic non-metallic materials. Background technique [0002] Magnesium oxide is a white powder, odorless, tasteless, water-insoluble granular solid matter. The common dosage form of magnesium oxide is powder or granules, and it is used as a flour improver or pH regulator in the food industry. At present, there is no microencapsulated magnesium oxide product. [0003] The existing microencapsulation products are mainly concentrated in flame retardant materials such as magnesium hydroxide, mainly because the existing microencapsulation process often needs to use harmful substances to the human body. After microencapsulation, the products cannot be directly used as raw materials for the food industry. use. Microcapsule products used as raw materials in the food industry are mainly obtained by embedding unstable food act...

Claims

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Application Information

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IPC IPC(8): A23L29/00A21D2/02A23P10/30
CPCA23L29/015A21D2/02A23P10/30
Inventor 梅志恒陈永龙张春光
Owner 郑州瑞普生物工程有限公司