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A kind of conductive nanofiber film and preparation method thereof

A nanofiber membrane, conductive nanotechnology, applied in the direction of fiber processing, fiber type, fiber chemical characteristics, etc., can solve the problems of cumbersome silver plating process, large amount of palladium, uneven silver plating layer, etc., and achieves novel method, repeatability High, simple process effect

Active Publication Date: 2022-03-04
DONGHUA UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The technical problem to be solved by the present invention is to provide a conductive nanofibrous film and its preparation method, which overcomes the defects of large amount of palladium during chemical silver plating in the prior art, cumbersome silver plating process, and uneven silver plating layer, and simultaneously provides a method for using Method for making nanofibers uniformly conductive

Method used

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  • A kind of conductive nanofiber film and preparation method thereof
  • A kind of conductive nanofiber film and preparation method thereof
  • A kind of conductive nanofiber film and preparation method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0034] (1) Dissolve 1 mg of palladium chloride in DMF at room temperature for 8 hours to obtain PdCl with a concentration of 1 ppm 2 solution, adding PAN into the solution, magnetically stirring the spinning solution at 70° C. and 500 rpm for 4 hours until the PAN is completely dissolved to obtain a spinning solution of 8% wt PAN. Stand still for 5 minutes to remove the air bubbles in the solution to obtain a uniform and stable spinning solution.

[0035] (2) Electrospinning process parameters are: voltage 18kV, the distance from the needle of the spinning solution injector to the receiving plate of the rotating receiving system is 12cm, the diameter of the spinneret of the electrospinning device is 0.67-0.90mm, and the spinning speed is 6.5ml / h, the spinning time is 8h, the ambient temperature is 25°C, and the ambient humidity is 60%. A uniform nanofiber membrane was obtained by electrospinning, and a piece of electrospun nanofiber membrane with a size of 5*5cm was cut, with...

Embodiment 2

[0038] (1) Dissolve 1 mg of palladium chloride in DMF at room temperature for 8 hours to obtain PdCl with a concentration of 1 ppm 2 solution, adding PAN into the solution, magnetically stirring the spinning solution at 70° C. and 500 rpm for 4 hours until the PAN is completely dissolved to obtain a spinning solution of 8%wt PAN. Stand still for 5 minutes to remove the air bubbles in the solution to obtain a uniform and stable spinning solution.

[0039] (2) Electrospinning process parameters are: voltage 18kV, the distance from the needle of the spinning solution injector to the receiving plate of the rotating receiving system is 12cm, the diameter of the spinneret of the electrospinning device is 0.67-0.90mm, and the spinning speed is 6.5ml / h, the spinning time is 8h, the ambient temperature is 25°C, and the ambient humidity is 60%. The nanofiber membrane was obtained by electrospinning, and a piece of electrospun nanofiber membrane with a size of 5*5cm was cut, with a mass...

Embodiment 3

[0042] (1) Dissolve 1 mg of palladium chloride in DMF at room temperature for 8 hours to obtain PdCl with a concentration of 1 ppm 2 solution, adding acrylonitrile into the solution, magnetically stirring the spinning solution at 70° C. and 500 rpm for 4 hours until PAN was completely dissolved to obtain a spinning solution of 8% wt acrylonitrile. Stand still for 5 minutes to remove the air bubbles in the solution to obtain a uniform and stable spinning solution.

[0043] (2) Electrospinning process parameters are: voltage 18kV, the distance from the needle of the spinning solution injector to the receiving plate of the rotating receiving system is 12cm, the diameter of the spinneret of the electrospinning device is 0.67-0.90mm, and the spinning speed is 6.5ml / h, the spinning time is 8h, the ambient temperature is 25°C, and the ambient humidity is 60%. The nanofiber membrane was obtained by electrospinning, and a piece of electrospun nanofiber membrane with a size of 5*5cm wa...

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Abstract

The invention relates to a conductive nanofiber membrane and a preparation method thereof. The fiber membrane is obtained by chemically silver-plating the palladium-containing polyacrylonitrile PAN nanofiber membrane as a carrier. The preparation method of the invention can change the conductivity of the nanofiber membrane and the morphology of the nanofiber membrane by adjusting process parameters. The preparation method is novel, the process is simple, the adjustment is flexible, the repetition rate is high, the processing is convenient, the flexibility is large and thin, and it is especially suitable for application in the field of intelligent textiles.

Description

technical field [0001] The invention belongs to the field of conductive materials and preparation thereof, in particular to a conductive nanofiber film and a preparation method thereof. Background technique [0002] Nanofibrous membrane has the characteristics of controllable fiber scale and structure morphology and porous structure, which can greatly increase the specific surface area, such as catalysts, sensors, filter materials, etc. Among them, conductive nanofiber materials have both the characteristics of nanofibers and excellent electrical conductivity, and can meet some special performance requirements. They have outstanding application performance in the fields of myocardial and nerve tissue engineering, electrical sensors, and electrical energy storage. [0003] Polymer nanofibers prepared by electrospinning are generally non-conductive, which limits their potential applications to a certain extent. After metallizing the nanofibers by physical or chemical methods, ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D01F6/54D01F1/10D06M11/83D04H1/728D04H1/43D01D5/00D06M101/28
CPCD06M11/83D01F6/54D01F1/10D04H1/728D04H1/43D01D5/003D06M2101/28
Inventor 陈奕翔俞丹王炜王泽鸿
Owner DONGHUA UNIV
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