Unlock instant, AI-driven research and patent intelligence for your innovation.

Sample signal amplification method using terahertz wave band graphene absorber

A signal amplification and graphene technology, which is applied in the field of terahertz signal amplification of samples, can solve the problems that it is difficult to achieve a close fit between metamaterials and the surface of the sample to be tested, and meet the needs of rapid detection, smooth surface, and close fit. Effect

Active Publication Date: 2020-04-03
ZHEJIANG UNIV
View PDF8 Cites 2 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, although the metamaterials currently used in sample detection in this discipline can significantly enhance the sample signal, due to the existence of periodic microstructures, it is difficult to achieve a close fit between the metamaterial and the surface of the sample to be tested.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Sample signal amplification method using terahertz wave band graphene absorber
  • Sample signal amplification method using terahertz wave band graphene absorber
  • Sample signal amplification method using terahertz wave band graphene absorber

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0052] (1) The making of graphene absorber;

[0053]Take a silicon wafer or a quartz wafer, ultrasonically clean it in acetone, isopropanol and water for 10 minutes, blow dry with nitrogen, evaporate 10nm of titanium and 200nm of gold on the surface as an anti-transmission layer, and stick it on the gold surface Polyimide tape (thickness: 50-100μm), there should be no air bubbles between the polyimide tape and the metal anti-transmission layer. After the end, a layer of graphene is transferred on the polyimide tape. Schematic diagram of the structure of the graphene absorber Such as figure 1 shown.

[0054] Wherein, the transfer of graphene can adopt the following methods;

[0055] Release the purchased graphene into the water for at least 2 hours, use tweezers to clamp the silicon wafer or quartz wafer with polyimide tape to fit the graphene in the water, adjust the graphene to a suitable position, remove the graphene from the water surface, vertically Place it upright for...

Embodiment 2

[0071] (1) The making of flexible graphene absorber;

[0072] Take a polyimide film with a thickness of 50 μm, ultrasonically clean it in acetone, isopropanol, and water for 10 minutes, blow dry with nitrogen, and evaporate 10 nm of titanium and 150 nm of gold on the surface as an anti-transmission layer by evaporation, and then Transfer a layer of graphene on polyimide tape.

[0073] Wherein, the transfer of graphene can adopt the following methods;

[0074] After releasing the purchased graphene into the water for at least 2 hours, hold the polyimide film with tweezers, put it in the water at an angle, and press the polyimide film into the water with another tweezer if necessary; One side fits the graphene in the water, adjust it to a suitable position, remove the graphene from the water, place it vertically for 3 minutes to let the excess water flow out, then let it dry for 30 minutes, then dry it in an oven at 100°C for 20 minutes, and let it stand to room temperature Th...

Embodiment 3

[0084] (1) The making of graphene absorber;

[0085] Take a silicon or quartz wafer, ultrasonically clean it in acetone, isopropanol, and water for 10 minutes, blow dry it with nitrogen, and vapor-deposit 10nm of titanium and 100nm of gold on the surface as an anti-transmission layer, and stick it on the gold surface Polyimide tape (thickness is 50-100 μ m), no air bubbles can exist between the polyimide tape and the metal anti-transmission layer, and then transfer one layer of graphene on the polyimide tape.

[0086] Wherein, the transfer of graphene can adopt the following methods;

[0087] After releasing the purchased graphene into the water for at least 2 hours, use tweezers to clamp the silicon wafer or quartz wafer with polyimide tape to fit the graphene in the water, adjust the graphene to a suitable position, and remove the graphene from the water. Put it vertically for 3 minutes to allow excess water to flow out, then let it dry for 30 minutes, then dry it in an ove...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
thicknessaaaaaaaaaa
thicknessaaaaaaaaaa
Login to View More

Abstract

The invention discloses a sample signal amplification method using a terahertz wave band graphene absorber. The method comprises the steps of manufacturing the graphene absorber through the steps of metal evaporation, graphene transfer and the like; preparing sample solutions with different concentrations; dropwise adding a sample solution to the surface of the graphene absorber, and then airing at normal temperature; collecting the terahertz time domain signals of all sample points to be detected and the reference sample points on the surface of the graphene absorber, calculating the absorption rates of the sample points to be detected and the reference sample points according to the terahertz time domain signals, and calculating the intensity change of an absorption peak according to theintensity value corresponding to the highest point of the absorption peak. According to the method, the absorption peak of the graphene absorber is changed through the interaction between graphene and a sample, and then a sample signal is amplified. The method is high in detection sensitivity, is easy, convenient and rapid to operate, and can satisfy the increasing rapid detection requirements.

Description

technical field [0001] The invention relates to a sample terahertz signal amplification method, in particular to a sample signal amplification method using a terahertz band graphene absorber. Background technique [0002] Due to its fast detection speed and simple operation, spectral technology has gradually attracted extensive attention of scholars at home and abroad. Terahertz spectroscopy, as an emerging spectroscopy technology, has gradually attracted the attention of scholars from all over the world. Since the vibration, rotational energy levels, and intermolecular forces of many macromolecules are in the terahertz band, terahertz waves have great potential for the detection of samples. In areas where terahertz spectroscopy has great application prospects, such as security inspection, biology, medicine, agriculture, and material characterization, there is a demand for trace or even ultra-trace nondestructive testing. Moreover, in actual detection applications, the sur...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/3586
CPCG01N21/3586
Inventor 应义斌徐文道谢丽娟
Owner ZHEJIANG UNIV