Preparation method of sponge platinum
A technology of sponge platinum and ammonium chloroplatinate, which is applied in the field of preparation of sponge platinum, can solve the problems of large reagent consumption, high energy consumption, and long dissolution process time, and achieve the effect of short process cycle and easy promotion
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[0026] The embodiment of the present invention provides a method for preparing sponge platinum, which is specifically implemented according to the following steps:
[0027] Step 1. Slurry crude ammonium chloroplatinate with pure water in a volume ratio of 5-10:1, heat it to 80-90°C, add hydrochloric acid and sodium chlorate, and stir to obtain a mixed solution;
[0028] Wherein, the amount of hydrochloric acid added is 10%-20% of the solution volume after slurrying, the amount of sodium chlorate added is 5%-10% of the mass of crude ammonium chloroplatinate, and the stirring time is 1-2h;
[0029] Step 2. Boil the mixed solution of step 1 and keep it for 2-4 hours, then add ammonium chloride, and filter the mixed solution after cooling to obtain high-purity ammonium chloroplatinate; wherein the amount of ammonium chloride added is crude 50%-100% of the mass of ammonium chloroplatinate;
[0030] Step 3. Slurry the high-purity ammonium chloroplatinate, adjust the pH to 8-9 and heat to 60...
Example Embodiment
[0034] Example 1
[0035] Embodiment 1 of the present invention provides a method for preparing sponge platinum, which is specifically implemented according to the following steps:
[0036] Add 1kg of crude ammonium chloroplatinate to 10L of water for slurrying, add 1.2L of industrial hydrochloric acid and 70g of sodium chlorate to 85°C, keep the temperature and stir for 1h, boil the solution for 2h to remove chlorine, add 800g of ammonium chloride to the solution, After the solution is cooled, it is filtered to obtain high-purity ammonium chloroplatinate. The high-purity ammonium chloroplatinate is slurried by adding 7L of water, adding flake caustic so as to adjust the pH to 8, and heating to 65°C, adding an appropriate amount of hydrazine hydrate to obtain platinum;
[0037] Wash the platinum element with pure water and filter out the platinum black, then add hydrochloric acid, and then add hydrogen peroxide until the platinum black is completely dissolved. After dissolution, heat...
Example Embodiment
[0038] Example 2
[0039] Embodiment 2 of the present invention provides a method for preparing sponge platinum, which is specifically implemented according to the following steps:
[0040] Add 1kg of crude ammonium chloroplatinate to 8L of water for slurrying, add 1.5L of industrial hydrochloric acid and 60g of sodium chlorate to 88°C, and keep the temperature and stir for 1.5h. The solution was boiled for 3h to drive off chlorine. Add 900g of ammonium chloride to the solution. After the solution is cooled, it is filtered to obtain high-purity ammonium chloroplatinate. The high-purity ammonium chloroplatinate is slurried by adding 8L of water, and the pH value is adjusted to 8 by adding flake caustic soda. Proper amount of hydrazine hydrate to obtain platinum element;
[0041] Wash the platinum element with pure water and filter out the platinum black, then add hydrochloric acid, and then add hydrogen peroxide until the platinum black is completely dissolved. After dissolution, he...
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