Preparation method of static cracking agent
A technology of static breaking agent and diluent, which is applied in the direction of conjugated synthetic polymer artificial filament, fiber type, textile and papermaking, etc. It can solve the problems of poor crushing effect, long cracking time, low expansion pressure, etc., and achieves convenience and high efficiency Carry out and improve the effect of static crushing and expansion pressure
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[0029] Preparation of pretreated snail material: Take snails according to the mass ratio of 12~20:1~3, add glycerin, mix and grind for 1~3h, heat treatment in a muffle furnace at 450~550°C for 1~3h, heat up to 700~900°C, and keep warm for 1~3h After 2 hours, cool down to room temperature naturally, and discharge the material to obtain the pretreated snail material.
[0030] Water reducing agent: Mix sodium lignosulfonate and aluminum chloride according to the mass ratio of 1:2~5 to obtain the water reducing agent.
[0031] Reinforcing agent: Mix silicon powder, white carbon black and carboxymethyl cellulose at a mass ratio of 1:1~3:1 to obtain a reinforcing agent.
[0032] Diluent: Mix triacetin and dimethylformamide at a mass ratio of 1:2~5 to obtain a diluent.
[0033] Silicon-containing material: Mix hydrogen-containing silicone oil, trimethylchlorosilane, and polydimethylsiloxane at a mass ratio of 3~7:1:0.1 to obtain silicon-containing material.
[0034] Additive: Mix s...
Embodiment 1
[0042] Impregnation solution: Mix dibenzylidene sorbitol and n-butanol at a mass ratio of 1:20 to obtain the impregnation solution.
[0043] Preparation of pretreated snail material: Take snails and add glycerin to mix and grind for 1 hour at a mass ratio of 12:1, heat-treat in a muffle furnace at 450°C for 1 hour, heat up to 700°C, keep warm for 1 hour, cool naturally to room temperature, and discharge to obtain pretreatment Escargot.
[0044] Water reducer: Mix sodium lignosulfonate and aluminum chloride at a mass ratio of 1:2 to obtain a water reducer.
[0045] Reinforcing agent: Mix silicon powder, white carbon black and carboxymethyl cellulose at a mass ratio of 1:1:1 to obtain a reinforcing agent.
[0046] Diluent: Mix triacetin and dimethylformamide at a mass ratio of 1:2 to obtain a diluent.
[0047] Silicon-containing material: Mix hydrogen-containing silicone oil, trimethylchlorosilane, and polydimethylsiloxane at a mass ratio of 3:1:0.1 to obtain silicon-containin...
Embodiment 2
[0056] Impregnation solution: Mix dibenzylidene sorbitol and n-butanol at a mass ratio of 1:25 to obtain the impregnation solution.
[0057] Preparation of pretreated snail material: Take snails and add glycerin to mix and grind for 2 hours at a mass ratio of 16:2, heat-treat in a muffle furnace at 500°C for 2h, heat up to 800°C, keep warm for 1.5h, cool naturally to room temperature, and discharge the material to obtain pre-treated snails. Handle snail material.
[0058] Water reducer: Mix sodium lignosulfonate and aluminum chloride at a mass ratio of 1:3 to obtain a water reducer.
[0059] Reinforcing agent: Mix silicon powder, white carbon black and carboxymethyl cellulose at a mass ratio of 1:2:1 to obtain a reinforcing agent.
[0060] Diluent: Mix triacetin and dimethylformamide at a mass ratio of 1:4 to obtain a diluent.
[0061] Silicon-containing material: mix hydrogen-containing silicone oil, trimethylchlorosilane, and polydimethylsiloxane at a mass ratio of 5:1:0.1...
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