Process and system for producing cyclohexane plasticizer by liquid phase hydrogenation of o-benzene plasticizer

A technology of o-benzene plasticizer and liquid phase hydrogenation, which is applied in the field of liquid-phase hydrogenation of o-benzene plasticizer to produce cyclohexane plasticizer, and can solve the problem of long process reaction time and high moisture content in product test results. , unstable product quality and other problems, to achieve the effect of good separation and purification effect, good mixing heating and separation and purification effect

Active Publication Date: 2020-05-19
ZHENGZHOU RAILWAY VOCATIONAL & TECH COLLEGE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Studies have shown that the traditional production equipment for preparing plasticizers has long process reaction time, high energy consumption, low output per unit time, unstable product quality, high water content and high acid value in product test results
And the prepared o-phthalic plasticizer has toxicity and carcinogenicity

Method used

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  • Process and system for producing cyclohexane plasticizer by liquid phase hydrogenation of o-benzene plasticizer
  • Process and system for producing cyclohexane plasticizer by liquid phase hydrogenation of o-benzene plasticizer
  • Process and system for producing cyclohexane plasticizer by liquid phase hydrogenation of o-benzene plasticizer

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Embodiment Construction

[0019] see figure 1 , which shows a schematic diagram of the production system of cyclohexane plasticizers produced by liquid-phase hydrogenation of o-phthalic plasticizers in the present invention, and its specific structure is as follows:

[0020] Including feed preheater 1, vacuum distillation tower 2, extraction and separation tower 3, solvent regeneration tower 4, light component tank 5, heavy component tank 6, first condenser 7, second condenser 8, first vacuum pump 9. The second vacuum pump 10. Wherein, the feed preheater 1 is provided with the first feed port A and the first discharge port B communicated therewith, the second feed port C and the second discharge port D communicated therewith; the first condenser 7. The second condenser 8 is respectively provided with a water inlet E and a water outlet F connected thereto, a feed inlet G and a discharge outlet H connected thereto; the bottom of the vacuum distillation tower 2 is provided with an inert gas inlet K, a h...

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Abstract

The invention relates to a process and a system for producing a cyclohexane plasticizer by liquid phase hydrogenation of an o-benzene plasticizer. The process for preparing a cyclohexane plasticizer by liquid phase hydrogenation of an o-benzene plasticizer comprises the following steps: (1) heated inert gas is introduced into the bottom of a reduced pressure distillation tower in a pulse pneumaticconveying manner; and (2) a plasticizer product is preheated and then enters the bottom of the reduced pressure distillation tower, and the inlet of the plasticizer product on the reduced pressure distillation tower is higher than the inlet of the inert gas, so that the plasticizer product is mixed and heated with the rising inert gas flow in the downward flowing process, and the target product is separated from the by-product. According to the process and the system disclosed by the invention, heated inert gas is fed into the reduced pressure distillation tower in a pulse manner, and the characteristic that the flow of inert gas is changing is utilized to better simulate the characteristics of fluidization, mixing and heating at the bottom of the reduced pressure distillation tower, so that better mixing, heating, separation and purification effects on the plasticizer product are realized.

Description

technical field [0001] The invention relates to the field of preparing cyclohexane plasticizers by liquid-phase hydrogenation of ortho-benzene plasticizers, in particular to a production process and system for preparing cyclohexane-type plasticizers by liquid-phase hydrogenation of ortho-benzene plasticizers. Background technique [0002] At present, plasticizers are the largest additives in the modern plastics industry. They play a decisive role in promoting the development of the plastics industry, especially the PVC industry. They also have a wide range of applications in synthetic rubber, coatings, adhesives, and sealing materials. Applications. Studies have shown that the traditional production equipment for preparing plasticizers has long process reaction time, high energy consumption, low output per unit time, unstable product quality, high moisture content and high acid value in product test results. Moreover, the prepared o-phthalic plasticizer has toxicity and car...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07C67/303C07C67/54C07C67/48C07C69/75B01D3/10
CPCB01D3/10C07C67/303C07C67/48C07C67/54C07C2601/14C07C69/75
Inventor 陈彬李咚杨丽纳张颢倚刘少卿刘楚然胡文莉
Owner ZHENGZHOU RAILWAY VOCATIONAL & TECH COLLEGE
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