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Rapid detection device for carbamate pesticide residues

A technology for carbamates and pesticide residues, applied in color/spectral characteristic measurement, material analysis by observing the impact on chemical indicators, and analysis by making materials react chemically, it can solve carcinogenicity and low detection accuracy , complex operation process and other issues, to achieve the effect of fast and accurate detection, high detection efficiency and high measurement accuracy

Inactive Publication Date: 2020-06-02
上海尚湾信息技术有限公司
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  • Abstract
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  • Claims
  • Application Information

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Problems solved by technology

However, studies have shown that carbamate pesticides have certain carcinogenic, teratogenic and mutagenic effects, and long-term exposure to such pesticides through diet will have an impact on human health. Therefore, monitoring of carbamate pesticide residues is carried out on agricultural products extra important
[0003] In the existing market, most of the kits and simple pesticide residue quick test cards are used to quickly detect pesticide residues through the cholinesterase inhibition method, which has high cost and low detection accuracy; while large-scale instruments such as gas phase or liquid chromatography , although the accuracy and sensitivity are high, this kind of instrument is expensive, the operation process is complicated, the detection time is long, and it needs professionals to carry out it, which cannot meet the needs of a large number of rapid detection of daily food safety

Method used

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  • Rapid detection device for carbamate pesticide residues
  • Rapid detection device for carbamate pesticide residues
  • Rapid detection device for carbamate pesticide residues

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Embodiment Construction

[0024] The reagent preparation method used in the embodiment of the present invention is as follows:

[0025] Sample solution: Grind and filter agricultural products such as vegetables and fruits to be tested, and dissolve 20mL of vegetable and fruit juices in 80mL of water;

[0026] Ammonia-ammonium chloride buffer solution with a pH of 10: Weigh 20g of ammonium chloride and dissolve in 100mL of concentrated ammonia water, store at 3-5°C;

[0027] The first chromogenic agent (2g / L 4-aminoantipyrine aqueous solution): absorb 10mL of 20g / L potassium ferricyanide solution and dissolve it in water, add water to dilute to 100mL, and prepare it immediately;

[0028] Second developer (8g / L potassium ferricyanide solution): Dissolve 10mL of 80g / L potassium ferricyanide solution in water, add water to dilute to 100mL, store at 3-5°C, and use for one week;

[0029] Such as figure 1 As shown, the present invention provides a rapid detection device for carbamate pesticide residues, inc...

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Abstract

The invention discloses a rapid detection device for carbamate pesticide residues. The device comprises a primary mixing pool, a color developing pool, a waste liquid pool, a sample liquid supply device, a buffer solution supply device, a first color developing agent supply device, a second color developing agent supply device, a cleaning liquid supply device, a spectrum testing device, a temperature control module, a valve pump module, a liquid flow control module, a testing module, a display module and a control unit. According to the present invention, the use amounts of a sample solution,a buffer solution and a 4-aminoantipyrine solution entering the primary mixing pool are accurately controlled, carbamate in the sample solution is hydrolyzed in an alkaline environment to generate phenolic compounds, then, the mixed solution enters the color developing pool, and a second color developing agent enters the color developing pool and reacts with phenolic compounds in the mixed solution to generate a red complex, and then, the liquid in the developing pool is controlled to enter the spectrum testing device, and the pesticide residue in the sample solution is tested. The device is simple to operate, and is high in detection speed and accurate in detection result.

Description

technical field [0001] The invention relates to the technical field of analysis and detection of pesticide residues, in particular to a rapid detection device for carbamate pesticide residues. Background technique [0002] Exogenous substances such as pesticides, antibiotics and hormones are widely used in the production process of agricultural products. The earliest pesticides used were organochlorine and organophosphorus pesticides. Although they can eliminate pests in large quantities, this type of pesticide has good stability, can exist in the environment for a long time, and accumulate continuously in animals, plants and humans, so it is gradually used. disuse. Now widely used carbamate pesticides have the advantages of strong selectivity, high efficiency, low toxicity to humans and animals, easy decomposition, and less residue. Therefore, they have been widely used. However, studies have shown that carbamate pesticides have certain carcinogenic, teratogenic and mutag...

Claims

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Application Information

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IPC IPC(8): G01N21/78G01N21/27
CPCG01N21/27G01N21/78
Inventor 袁文美
Owner 上海尚湾信息技术有限公司
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