Boron-doped diamond film and preparation method thereof, oil-water separation element, water treatment electrode and preparation method thereof and water treatment device
A boron-doped diamond, water treatment technology, applied in water/sewage treatment, oxidized water/sewage treatment, water/sludge/sewage treatment, etc. Strong wear and impact capability, reduced organic waste content, and strong corrosion resistance
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[0040] In a second aspect, the present invention provides a method for preparing a boron-doped diamond film, comprising the following steps:
[0041] A substrate is provided, first a boron-doped diamond micro-layer is prepared on the substrate, and after a boron-doped diamond nano-layer is prepared on the surface of the boron-doped diamond micro-layer, the boron-doped diamond film is obtained on the substrate.
[0042] The boron-doped diamond thin film obtained by this preparation method has all the advantages of the above-mentioned boron-doped diamond thin film, and will not be repeated here.
[0043] In some embodiments of the present invention, the preparation method of boron-doped diamond film comprises the following steps:
[0044] S1) Provide a substrate, first perform low-density crystal planting on the substrate, and then grow a boron-doped diamond micron layer by chemical vapor deposition;
[0045] S2) performing high-density planting on the surface of the boron-dope...
Embodiment 1
[0105] like figure 1 As shown, the present embodiment is a water treatment electrode, including a stainless steel metal mesh as the electrode substrate 10, a boron-doped diamond micro-layer 20 formed on the surface of the electrode substrate 10, and a raised boron-doped diamond micro-layer 20 is provided on the surface of the electrode substrate. Micron particles 21, and boron-doped diamond nano-layer 30 formed on the surface of boron-doped diamond micro-layer 20, boron-doped diamond nano-layer 30 surface has raised nanoparticles 31, boron-doped diamond micro-layer 20 and boron-doped diamond nano-layer 30 A lotus leaf-like multi-level micro-nano structure is formed.
[0106] The preparation method of the water treatment electrode comprises the following steps:
[0107] S1) Perform sandblasting treatment on the surface of the stainless steel metal mesh to activate the surface of the substrate, increase the surface roughness microscopically, and make the surface uniform macrosc...
Embodiment 2
[0114] This embodiment is a water treatment electrode, which is different from Embodiment 1 in that the electrode substrate in this embodiment is a copper alloy metal mesh, and the others are the same as Embodiment 1.
[0115] The preparation method of the water treatment electrode comprises the following steps:
[0116]S1) Sandblasting is performed on the surface of the copper alloy metal mesh to activate the surface of the substrate, increase the surface roughness microscopically, and make the surface uniform macroscopically. The sandblasting time is 2 minutes;
[0117] S2) Clean the metal mesh after the blasting treatment, first ultrasonic cleaning with deionized water for 2 times, each time for 5 minutes, and then ultrasonic cleaning with alcohol for 5 minutes;
[0118] S3) The cleaned metal mesh sample was subjected to ultrasonic crystallization treatment in diamond suspension I. The ultrasonic implantation time was 30 min. The formula of diamond suspension I was: diamond...
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