Boron-doped diamond film and preparation method thereof, oil-water separation element, water treatment electrode and preparation method thereof and water treatment device

A boron-doped diamond, water treatment technology, applied in water/sewage treatment, oxidized water/sewage treatment, water/sludge/sewage treatment, etc. Strong wear and impact capability, reduced organic waste content, and strong corrosion resistance

Active Publication Date: 2020-06-26
SHENZHEN INST OF ADVANCED TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] At present, the existing small portable water purifiers available in the market in our country have the following defects: the water purification device and the water storage device are set separately, and the equipment is complicated; the water purification pot is too large and heavy, so it is not easy to carry; As the core filter element, the filter element is relatively large, it is not easy to replace, and the water purification effect is not good, and the impurities and pollutants in the water cannot be completely removed, which poses a threat to human health, etc.
Although these methods can improve the efficiency of water purification and the service life of the water purifier to a certain extent, the composition of the sewage in the harsh environment is complex, the chemical oxygen demand is high, and it often has strong acidity or strong alkalinity, which leads to the separation of ordinary separation membranes. There are fatal shortcomings such as poor corrosion resistance, poor thermal stability, easy pollution, difficult to clean and cannot be reused, which limits its application in sewage treatment

Method used

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  • Boron-doped diamond film and preparation method thereof, oil-water separation element, water treatment electrode and preparation method thereof and water treatment device
  • Boron-doped diamond film and preparation method thereof, oil-water separation element, water treatment electrode and preparation method thereof and water treatment device

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preparation example Construction

[0040] In a second aspect, the present invention provides a method for preparing a boron-doped diamond film, comprising the following steps:

[0041] A substrate is provided, first a boron-doped diamond micro-layer is prepared on the substrate, and after a boron-doped diamond nano-layer is prepared on the surface of the boron-doped diamond micro-layer, the boron-doped diamond film is obtained on the substrate.

[0042] The boron-doped diamond thin film obtained by this preparation method has all the advantages of the above-mentioned boron-doped diamond thin film, and will not be repeated here.

[0043] In some embodiments of the present invention, the preparation method of boron-doped diamond film comprises the following steps:

[0044] S1) Provide a substrate, first perform low-density crystal planting on the substrate, and then grow a boron-doped diamond micron layer by chemical vapor deposition;

[0045] S2) performing high-density planting on the surface of the boron-dope...

Embodiment 1

[0105] like figure 1 As shown, the present embodiment is a water treatment electrode, including a stainless steel metal mesh as the electrode substrate 10, a boron-doped diamond micro-layer 20 formed on the surface of the electrode substrate 10, and a raised boron-doped diamond micro-layer 20 is provided on the surface of the electrode substrate. Micron particles 21, and boron-doped diamond nano-layer 30 formed on the surface of boron-doped diamond micro-layer 20, boron-doped diamond nano-layer 30 surface has raised nanoparticles 31, boron-doped diamond micro-layer 20 and boron-doped diamond nano-layer 30 A lotus leaf-like multi-level micro-nano structure is formed.

[0106] The preparation method of the water treatment electrode comprises the following steps:

[0107] S1) Perform sandblasting treatment on the surface of the stainless steel metal mesh to activate the surface of the substrate, increase the surface roughness microscopically, and make the surface uniform macrosc...

Embodiment 2

[0114] This embodiment is a water treatment electrode, which is different from Embodiment 1 in that the electrode substrate in this embodiment is a copper alloy metal mesh, and the others are the same as Embodiment 1.

[0115] The preparation method of the water treatment electrode comprises the following steps:

[0116]S1) Sandblasting is performed on the surface of the copper alloy metal mesh to activate the surface of the substrate, increase the surface roughness microscopically, and make the surface uniform macroscopically. The sandblasting time is 2 minutes;

[0117] S2) Clean the metal mesh after the blasting treatment, first ultrasonic cleaning with deionized water for 2 times, each time for 5 minutes, and then ultrasonic cleaning with alcohol for 5 minutes;

[0118] S3) The cleaned metal mesh sample was subjected to ultrasonic crystallization treatment in diamond suspension I. The ultrasonic implantation time was 30 min. The formula of diamond suspension I was: diamond...

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Abstract

The invention provides a boron-doped diamond film and a preparation method thereof, an oil-water separation element, a water treatment electrode and a preparation method thereof and a water treatmentdevice, and relates to the technical field of diamond films. The boron-doped diamond film comprise a boron-doped diamond micrometer layer and a boron-doped diamond nanometer layer; the surface of theboron-doped diamond micrometer layer is provided with convex micrometer particles; the boron-doped diamond nanometer layer is formed on the surface of the boron-doped diamond micrometer layer, and thesurface of the boron-doped diamond nanometer layer is provided with nanometer particles; and the boron-doped diamond micrometer layer and the boron-doped diamond nanometer layer form a lotus leaf-like multilevel micro-nano structure. The boron-doped diamond film has the lotus leaf-like multilevel micro-nano structure, a bionic superhydrophobic surface is formed, the filtering function and the electrocatalytic water purification function are taken into account concurrently, and a foundation is laid for development of a new-generation field living water supply system.

Description

technical field [0001] The invention relates to the technical field of diamond films, in particular to a boron-doped diamond film and a preparation method thereof, an oil-water separation element, a water treatment electrode and a preparation method thereof, and a water treatment device. Background technique [0002] During battlefield or disaster rescue, due to the constraints of transportation and other factors, it is often difficult to guarantee the drinking water supply and sanitation of the troops. When the supply in the rear is insufficient, the drinking water mainly depends on the local water source and takes water locally. Water sources that can be used as drinking water in the wild mainly include mountain springs, streams, lakes, and natural rainfall. However, these water sources often contain a large number of germs, organic waste and other harmful substances to the human body. They must be purified before drinking, otherwise they will cause many diseases. , affect...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C23C16/27C23C16/02C02F1/46C02F1/72B01D17/022
CPCC23C16/278C23C16/271C23C16/0272C02F1/4606C02F1/72C02F1/722B01D17/02C02F2305/023C23C16/27C02F1/46C23C16/02
Inventor 唐永炳王陶黄磊李星星
Owner SHENZHEN INST OF ADVANCED TECH
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