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Silver nanowire antibacterial layer and silver nanowire mask

A technology of nano-silver wire and anti-bacterial layer, applied in coatings, clothing, protective clothing, etc., can solve the problems of limiting the anti-bacterial and anti-virus capabilities of nano-silver masks, poor adhesion, etc., and achieve high hydrophobicity, high safety, and comfortable wearing Effect

Pending Publication Date: 2020-07-24
SHENZHEN HUAKE COMM TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Nano-silver has antibacterial and anti-virus effects. In order to improve the antibacterial performance of masks, nano-silver ions or nano-silver particles are often added in the process of preparing masks. However, the traditional nano-silver materials have poor adhesion to the fiber matrix, and there are nano-silver particles. The risk of precipitation has a certain degree of danger, and limits the antibacterial and antiviral capabilities of nano silver masks

Method used

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  • Silver nanowire antibacterial layer and silver nanowire mask
  • Silver nanowire antibacterial layer and silver nanowire mask
  • Silver nanowire antibacterial layer and silver nanowire mask

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] A nano silver wire antibacterial layer, its preparation method comprises the steps:

[0031] (1) Mixing silver nanowires with a diameter of 8-12nm and a length of 30-40 μm and an organic silicon modifier in ethylene glycol to obtain a reaction stock solution, the mass fraction of the silver nanowires in the reaction stock solution is 0.01%, so The organosilicon modifier mass fraction is 1%, reacted for 2 hours at 120°C and 300r / min mechanical stirring to obtain a reaction solution, cleaned with acetone and blown with nitrogen to obtain a modified nano-silver wire with a low-thickness protective layer. Wire;

[0032] (2) Adding the modified silver nanowires into a mixture of water: ethanol: isopropanol = 1:5:4 by mass percentage to obtain a suspension of silver nanowires with a mass fraction of 0.01%;

[0033] (3) Spray the nano-silver wire suspension evenly on a polytetrafluoroethylene film (PTFE film) with a pore size of 300 nm with an air spray gun, and sinter at a l...

Embodiment 2

[0035] A nano silver wire antibacterial layer, its preparation method comprises the steps:

[0036] (1) Mixing silver nanowires with a diameter of 8-12nm and a length of 30-40 μm and an organic silicon modifier in ethylene glycol to obtain a reaction stock solution, the mass fraction of the silver nanowires in the reaction stock solution is 0.01%, so The mass fraction of the organic silicon modifier is 2%, reacted at 120° C. and 300 r / min under mechanical stirring for 2 hours to obtain a reaction solution, cleaned with acetone and blown with nitrogen to obtain a modified nano-silver wire with a low-thickness protective layer. Wire;;

[0037] (2) Adding the modified silver nanowires into a mixture of water: ethanol: isopropanol = 1:4:4 by mass percentage to obtain a suspension of silver nanowires with a mass fraction of 0.005%;

[0038] (3) Spray the nano-silver wire suspension evenly on a PTFE film with a pore size of 200 nm with an air spray gun, and sinter at a low temperat...

Embodiment 3

[0040] A nano silver wire antibacterial layer, its preparation method comprises the steps:

[0041] (1) Mixing silver nanowires with a diameter of 8-12nm and a length of 30-40 μm and an organic silicon modifier in ethylene glycol to obtain a reaction stock solution, the mass fraction of the silver nanowires in the reaction stock solution is 0.01%, so The mass fraction of the organic silicon modifier is 1%, reacted at 100° C. and 300 r / min under mechanical stirring for 2 hours to obtain a reaction solution, cleaned with acetone and blown with nitrogen to obtain a modified nano-silver wire with a low-thickness protective layer. Wire;

[0042] (2) Adding a mass percentage of water: ethanol: isopropanol = 1:5:4 to the modified silver nanowires to obtain a suspension of silver nanowires with a mass fraction of 0.1%;

[0043] (3) Spray the nano-silver wire suspension evenly on a PTFE film with a pore size of 200 nm with an air spray gun, and sinter at a low temperature of 85° C. to...

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Abstract

The invention discloses a silver nanowire antibacterial layer and a silver nanowire mask. The preparation method of the silver nanowire antibacterial layer comprises the following steps: (1) mixing silver nanowires and an organic silicon modifier in ethylene glycol to obtain a reaction stock solution with the mass fraction of the silver nanowires being 0.01-0.05% and the mass fraction of the organic silicon modifier being 1-3%, carrying out a mechanical stirring reaction to obtain a reaction solution, and cleaning and blow-drying the reaction solution to obtain modified silver nanowires; (2) adding a mixed solution composed of water, ethyl alcohol and isopropyl alcohol into the modified silver nanowires so as to obtain 0.005%-0.1% of silver nanowire turbid liquid; and (3) uniformly spraying or dipping the silver nanowire turbid liquid on a PTFE film, and sintering at low temperature to obtain the silver nanowire antibacterial layer. The silver nanowires modified by ethylene glycol andthe organic silicon modifier so that the silver nanowires have higher adhesive force on the PTFE film and are easier to sinter at low temperature, and the silver nanowire particles on the prepared nano antibacterial layer are more uniformly distributed.

Description

technical field [0001] The invention relates to the field of nano-silver wires, in particular to a nano-silver wire antibacterial layer and a nano-silver wire anti-mask. Background technique [0002] During the period when the virus is raging, the clearest known transmission method is saliva transmission, and frequent wearing of masks has become one of the most important anti-corrosion measures. With the development of the situation, mask resources are extremely scarce, especially medical masks with significant antibacterial and antibacterial effects. [0003] The new type of coronavirus pneumonia is extremely contagious. In addition to the substantial increase in the production capacity of antibacterial masks, higher requirements are also placed on the antibacterial properties of masks. Nano-silver has antibacterial and anti-virus effects. In order to improve the antibacterial performance of masks, nano-silver ions or nano-silver particles are often added in the process of...

Claims

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Application Information

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IPC IPC(8): C08J7/06C09D5/14A41D13/11C08L27/18
CPCC08J7/06C09D5/14A41D13/1192C08J2327/18Y02A50/30
Inventor 詹世治曾西平靳世东肖谢林仪珊
Owner SHENZHEN HUAKE COMM TECH CO LTD
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