Preparation method of agricultural and forestry waste porous carbon-based composite adsorption material
A technology for composite adsorption material and agricultural and forestry waste is applied in the field of preparation of agricultural and forestry waste porous carbon-based composite adsorption material, which can solve the problems of cumbersome, expensive preparation process, high cost and the like, and achieve the effect of good adsorption effect.
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Embodiment 1
[0024] In this implementation, the obtained agricultural and forestry waste porous carbon-based composite adsorption material C-CuO-MgO-Ag 2 O, C, CuO, MgO and Ag 2 The doping molar ratio of O is 7:2:1:1. The preparation method steps are as follows:
[0025] 1) Agricultural and forestry wastes such as bark, straw, sawdust, bagasse, orange peel, grapefruit peel, coconut shell, rice bran, etc. are pickled, deashed, and activated in an inert atmosphere to form pores to obtain porous carbon from agricultural and forestry waste Material.
[0026] 2), weigh copper nitrate, magnesium oxide, and silver nitrate into a beaker, dissolve with distilled water and dilute nitric acid, then add porous carbon from agricultural and forestry waste, and add ammonia water to adjust the pH value of the solution to 11, and stir thoroughly;
[0027] 3) Put the solution in a combined ultrasonic and microwave reactor for reaction, using ultrasonic 1000W + microwave 800W dual-functional reaction for ...
Embodiment 2
[0030] In this example, the obtained agricultural and forestry waste porous carbon-based composite adsorption material C-CuO-MgO-Ag 2 O, C, CuO, MgO and Ag 2 The doping molar ratio of O is 7:2:2:1, and the preparation method is the same as that in Example 1 to obtain the porous carbon-based composite adsorption material C-CuO-MgO-Ag for agricultural and forestry waste. 2 O(7:2:2:1).
Embodiment 3
[0032] In this example, the obtained agricultural and forestry waste porous carbon-based composite adsorption material C-CuO-MgO-Ag 2 O, C, CuO, MgO and Ag 2 The doping molar ratio of O is 7:1:2:1, and the preparation method is the same as that in Example 1 to obtain the porous carbon-based composite adsorption material C-CuO-MgO-Ag for agricultural and forestry waste. 2 O(7:1:2:1).
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