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A method for strengthening and toughening magnesium alloy strips

A magnesium alloy and strip technology, applied in the field of metal materials, can solve problems such as local overburning, coarse alloy grains, and demanding processing technology

Active Publication Date: 2021-07-06
CENT SOUTH UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The strength and plasticity of magnesium alloys can be improved at the same time through grain refinement, but the degree of grain refinement to improve the strength of magnesium alloys is limited. Distributed strengthening phase realization
[0004] At present, heat-treatable magnesium alloys are basically prepared by deformation heat treatment process, that is, "solution → processing → aging" process, in which solution treatment is annealed at a higher temperature for a long time, and there are the following problems: 1) The heating temperature is high (above 400°C), long holding time (depending on the batch size in the furnace, usually several hours), and high energy consumption; 2) Surface oxide layer is easy to form during heat treatment, which is difficult to remove in subsequent processes, affecting product quality; 3) It is easy to cause abnormal grain growth, resulting in coarse grains and uneven size distribution inside the alloy, which seriously damages the mechanical properties of the alloy; 4) The processing technology is demanding, and it is easy to cause uneven internal temperature of the material and local overburning, resulting in solid solution Poor uniformity, consistency and stability of alloy structure and properties after treatment
In addition, the magnesium alloy after solution treatment undergoes plastic forming and aging treatment, and the aging temperature is generally lower than the recrystallization temperature. Although strengthening phases can be precipitated in the magnesium matrix to improve the strength of the alloy, the magnesium matrix crystals produced by solution treatment Coarse particles and uneven size distribution still exist, and the prepared alloy has poor plasticity and limited strengthening degree.

Method used

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  • A method for strengthening and toughening magnesium alloy strips
  • A method for strengthening and toughening magnesium alloy strips
  • A method for strengthening and toughening magnesium alloy strips

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0045] Embodiment 1: Preparation of AZ61 magnesium alloy strip

[0046] (1) Rapid solid solution and water spray cooling and quenching are carried out on the extruded AZ61 magnesium alloy (Cu-6wt%Al-1wt%Zn) billet by electric pulse, so that the precipitated phase in the alloy is solid-dissolved in the magnesium matrix . The parameters of the electric pulse input to the energized region of the magnesium alloy strip blank are: frequency 1200Hz, pulse width 100μs, current density amplitude 2200A / mm 2 , effective current density 250A / mm 2 , the maximum heating temperature is 340°C, the heating time is 10s; the cooling water flow rate of spray water is 12L / min.

[0047] (2) Carry out a cold rolling to the magnesium alloy strip material of the electric pulse solution treatment in the step (1), the pass reduction rate is 25%, the total reduction rate is 50%, and the rolling speed is 5m / min;

[0048] (3) Aging treatment is carried out to the primary cold-rolled magnesium alloy stri...

Embodiment 2

[0062] Embodiment 2: Preparation of AZ91 magnesium alloy strip

[0063] (1) Rapid solid solution and water spray cooling and quenching are carried out on the extruded AZ91 magnesium alloy (Cu-9wt%Al-1wt%Zn) billet by electric pulse, so that the precipitated phase in the alloy is solid-dissolved in the magnesium matrix . The parameters of the electric pulse input to the energized region of the magnesium alloy strip blank are: frequency 1500Hz, pulse width 120μs, current density amplitude 2500A / mm 2 , effective current density 400A / mm 2 , the maximum heating temperature is 350°C, the heating time is 10s; the flow rate of water spray cooling water is 20L / min

[0064] (2) Carry out one-time cold rolling to the magnesium alloy strip material of electric pulse solution treatment in step (1), pass reduction ratio 18%, total reduction ratio 50%, rolling speed 3m / min;

[0065] (3) aging treatment is carried out to the primary cold-rolled magnesium alloy strip in step (2), the aging ...

Embodiment 3

[0076] Embodiment 3: the preparation of ZK60 magnesium alloy strip

[0077](1) Rapid solid solution and water spray cooling and quenching treatment of the hot-rolled ZK60 magnesium alloy (Cu-5.8wt%Zn-0.7wt%Zr) strip blank by electric pulse, so that the precipitated phase in the alloy is solid-dissolved in the magnesium matrix middle. The parameters of the electric pulse input to the energized region of the magnesium alloy strip blank are: frequency 1800Hz, pulse width 150μs, current density amplitude 2700A / mm 2 , effective current density 450A / mm 2 , the maximum heating temperature is 370°C, the heating time is 15s; the flow rate of water spray cooling water is 25L / min

[0078] (2) Carry out a cold rolling to the magnesium alloy strip material of the electric pulse solution treatment in the step (1), the pass reduction rate is 20%, the total reduction rate is 50%, and the rolling speed is 4m / min;

[0079] (3) aging treatment is carried out to the primary cold-rolled magnesi...

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Abstract

The invention discloses a method for strengthening and toughening magnesium alloy strips. Aiming at the problems of easy oxidation, coarse crystal grains, limited improvement of strength and plasticity, and high energy consumption in the traditional heat treatment process of magnesium alloys, the invention first uses electric pulses to treat magnesium alloys. The alloy strip is subjected to rapid solution treatment, and then processed by rolling, the primary cold-rolled strip is subjected to aging treatment, the aging-treated strip is subjected to secondary cold-rolling, and finally the secondary cold-rolled strip is subjected to electric pulse induction. Recrystallization treatment uses electric pulses to quickly refine the matrix grains and precipitated phases to hinder the growth of grains, so as to obtain a structure with fine and uniform matrix grains and a dispersed distribution of strengthening phases. Through the synergistic toughness of fine grains and precipitated phases Chemical reaction to prepare high-strength and high-toughness magnesium alloy strips. Compared with the magnesium alloy strip in the prior art, the strength and elongation after fracture of the magnesium alloy strip prepared by the process of the invention are respectively increased by more than 10% and 30%.

Description

technical field [0001] The invention belongs to the technical field of metal materials, and in particular relates to a method for strengthening and toughening magnesium alloy strips. Background technique [0002] As the lightest engineering metal structure material, magnesium alloy has the advantages of light specific gravity, high specific strength and specific stiffness, good thermal conductivity, strong electromagnetic shielding ability, good damping and shock absorption, easy cutting and recycling, etc. Information, transportation and other industries have a wide range of applications, and are known as "the most promising green engineering materials in the 21st century". [0003] With the development of transportation tools (such as automobiles, high-speed rail, etc.) towards light weight and electronic devices towards miniaturization, light weight, and multi-function, higher and higher requirements are put forward for the performance and processing performance of magnes...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22F1/06C22F3/00
CPCC22F1/06C22F3/00
Inventor 姜雁斌王檬李周唐国翌肖柱龚深
Owner CENT SOUTH UNIV
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