Preparation process of nano thermal insulation coating
A preparation process, nanotechnology, applied in the direction of nanotechnology, fireproof coatings, coatings, etc., can solve the problems of not having heat preservation, heat insulation, flame retardancy, etc., and achieve the effect of ensuring the preparation effect
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Embodiment 1
[0013] Embodiment 1: a kind of preparation technology of nanometer thermal insulation coating, comprises the following steps:
[0014] 1) Preparation of nano antimony pentoxide: Put 14 parts of antimony trioxide and 19 parts of deionized water into the inside of the stirred reactor and stir for 10 minutes to make the two fully mixed into a slurry, and then mix the slurry Heating the material to a temperature of 90°C. After heating, add water into it and stir for 5 minutes. After stirring, slowly add 11 parts of hydrogen peroxide with a concentration of 28% into it. During the process of adding hydrogen peroxide , the temperature shall not exceed 95°C. After the hydrogen peroxide is added, continue to stir for 2 minutes to fully mix the slurry with hydrogen peroxide. After mixing, heat the obtained mixture to reflux for 43 minutes to obtain a white thick slurry. After the white thick slurry is cooled slightly, it is filtered to remove the internal aggregates or lumps. After the...
Embodiment 2
[0016] Embodiment two: a kind of preparation technology of nanometer thermal insulation coating, comprises the following steps:
[0017] 1) Preparation of nano antimony pentoxide: put 15 parts of antimony trioxide and 20 parts of deionized water into the inside of the stirred reactor and stir for 25 minutes to make the two fully mixed into a slurry, and then mix the slurry Heating the material, the temperature is 95°C, after the heating is completed, add water into it and stir for 7 minutes, after stirring, slowly add 12 parts of hydrogen peroxide with a concentration of 28% into it, during the process of adding hydrogen peroxide , the temperature must not exceed 95°C. After the hydrogen peroxide is added, continue to stir for 4 minutes to fully mix the slurry with hydrogen peroxide. After mixing, heat the obtained mixture to reflux for 48 minutes to obtain a white thick slurry. After the white thick slurry is cooled slightly, filter it to remove the internal aggregates or lum...
Embodiment 3
[0019] Embodiment 3: A preparation process of a nanometer thermal insulation coating, comprising the following steps:
[0020] 1) Preparation of nano antimony pentoxide: put 14.1 parts of antimony trioxide and 19.2 parts of deionized water into the inside of the stirred reactor and stir for 11 minutes to make the two fully mixed into a slurry, and then mix the slurry Heating the material to a temperature of 91°C. After heating, add water into it and stir for 5 minutes. After stirring, slowly add 11 parts of hydrogen peroxide with a concentration of 28% into it. During the process of adding hydrogen peroxide , the temperature must not exceed 95°C. After the hydrogen peroxide is added, continue to stir for 2 minutes to fully mix the slurry with hydrogen peroxide. After mixing, heat the obtained mixture to reflux for 44 minutes to obtain a white thick slurry. After the white thick slurry is cooled slightly, filter it to remove the internal aggregates or lumps. After filtering, pl...
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