Tire pyrolysis carbon black modification method, modified pyrolysis carbon black and tire
A carbon black and modification technology, applied in chemical instruments and methods, inorganic pigment treatment, dyeing physical treatment, etc., can solve the problem of poor reinforcement performance of cracked carbon black
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Embodiment 1
[0043] (1) Grinding, grinding tire pyrolysis carbon black to ensure that the 45um water washing sieve residue of pyrolysis carbon black is less than or equal to 500mg / kg;
[0044] (2) Sizing, mix the ground tire pyrolysis carbon black with water to make a water dispersion with a concentration of 80g / L; add absolute ethanol, anhydrous ethanol: pyrolysis carbon black mass ratio 1:10, mechanical stirring 100r / min, stirring for 3 minutes to obtain carbon black slurry;
[0045] (3) Ultrasonic dispersion, the carbon black slurry is placed in an ultrasonic disperser for ultrasonic dispersion to obtain a dispersed carbon black slurry; the dispersion power of the ultrasonic dispersion machine is 3000W, and the dispersion time of the ultrasonic dispersion machine is 10min;
[0046] (4) Aging modification, dispersing carbon black slurry in a 60℃ water bath, adding 30% H 2 O 2 , 30% H 2 O 2 :Pyrolysis carbon black, mass ratio 1:1, aging for 1h;
[0047] (5) Vacuum filtration, after aging and mod...
Embodiment 2
[0051] (1) Grinding: grind the tire pyrolysis carbon black to ensure that the 45um water washing sieve residue of the pyrolysis carbon black is less than or equal to 500mg / kg;
[0052] (2) Sizing, mix the ground pyrolysis carbon black with water to make an aqueous dispersion with a concentration of 100g / L; add anhydrous ethanol, anhydrous ethanol: pyrolysis carbon black mass ratio 1:8, mechanical stirring 100r / min, stirring for 3 minutes to obtain carbon black slurry;
[0053] (3) Ultrasonic dispersion, the carbon black slurry is placed in an ultrasonic disperser for ultrasonic dispersion to obtain a dispersed carbon black slurry; the dispersion power of the ultrasonic dispersion machine is 4000W, and the dispersion time of the ultrasonic dispersion machine is 20min;
[0054] (4) Aging modification, dispersing carbon black pulp in a 60℃ water bath, adding 20% H 2 O 2 , 20% H 2 O 2 :Pyrolysis carbon black, mass ratio 1:1, aging for 1h;
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