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Trithiocyanuric acid trisodium salt rapid detection test paper as well as preparation method and detection method thereof

A technology of trisodium thiocyanate and trisodium polythiocyanate is applied in the field of rapid detection test paper and preparation of trisodium thiocyanate, which can solve the problems of expensive instruments, high cost, long time consumption and the like

Pending Publication Date: 2020-10-23
HENAN PROVINCE PROD QUALITY SUPERVISION & INSPECTION CENT
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The invention provides a rapid detection test paper for trisodium thiocyanate and its preparation method and detection method to solve the problems of high cost, long time consumption, Problems such as expensive equipment

Method used

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  • Trithiocyanuric acid trisodium salt rapid detection test paper as well as preparation method and detection method thereof
  • Trithiocyanuric acid trisodium salt rapid detection test paper as well as preparation method and detection method thereof
  • Trithiocyanuric acid trisodium salt rapid detection test paper as well as preparation method and detection method thereof

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preparation example Construction

[0043] The second invention of the present invention provides a kind of preparation method of trisodium thiocyanate rapid detection test paper, at least comprises the following steps:

[0044] S1: Preparation of chromogenic agent: add inorganic metal salt reagent to distilled water (the distilled water described in the present invention is water that meets the requirements of GB / T 6682-1992) several times, and stir until the inorganic metal salt reagent no longer After continuing to dissolve, a mixed solution is obtained, and the mixed solution is filtered through a rapid chromatography qualitative filter paper to obtain a saturated inorganic metal salt solution;

[0045] S2: Preparation of color test paper: Soak uncut filter paper or rice paper in a color developer at room temperature, soak for 10 seconds at room temperature, take it out to dry and cut it into a suitable shape to obtain a color test paper.

[0046] Further, in order to improve the color developing effect, the...

Embodiment 1

[0057] A rapid detection test paper for trisodium thiocyanate, the test paper includes a standard color comparison card and a color test paper, the color test paper is made by soaking a color developer, and the color developer includes saturated CuSO 4 The solution and mass fraction are 0.5% sodium carboxymethyl cellulose, and the color test paper is selected from slow chromatography qualitative analysis filter paper.

[0058] The preparation method of trisodium thiocyanate rapid detection test paper at least comprises the following steps:

[0059] S1: Preparation of chromogen: add CuSO to 100ml distilled water several times 4 reagents, stir well until the CuSO 4 After the reagent no longer dissolves, a mixed solution is obtained, and the mixed solution is filtered through a fast chromatography qualitative filter paper to obtain saturated CuSO 4 solution; to saturated CuSO 4 Add the corresponding sodium carboxymethylcellulose into the solution, heat and stir until the sodiu...

Embodiment 2

[0069] A rapid detection test paper for trisodium thiocyanate, the test paper includes a standard color comparison card and a color test paper, the color test paper is made by soaking a color developer, and the color developer includes saturated FeCl 2 Solution, color test paper as filter paper.

[0070] The preparation method of trisodium thiocyanate rapid detection test paper at least comprises the following steps:

[0071] S1: Preparation of chromogen: Add FeCl to 100ml distilled water several times 2 Reagent, stir well until FeCl 2 After the reagents no longer continue to dissolve, a mixed solution is obtained, and the mixed solution is filtered through a fast chromatography qualitative filter paper to obtain saturated FeCl 2 solution;

[0072] S2: Preparation of color test paper: Soak the uncut filter paper in the color developer at room temperature for 10 seconds at room temperature, take it out to dry and cut it into a suitable shape to obtain the color test paper. ...

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Abstract

The invention relates to trithiocyanuric acid trisodium salt rapid detection test paper as well as a preparation method and a detection method thereof. The detection test paper comprises a standard colorimetric card and color developing test paper, wherein the color developing test paper is prepared through soaking treatment of a color developing agent; the color developing agent comprises a saturated inorganic metal salt solution, wherein metal ions of the saturated inorganic metal salt solution are selected from any one of Cu<2+>, Fe<2+>, Sn<2+> and Ni<2+>; and the color developing agent further comprises a thickening agent with the mass fraction of 0.1-2%. The preparation method comprises preparation of the color developing agent and preparation of the color developing test paper. The trithiocyanuric acid trisodium salt rapid detection test paper prepared by the invention is simple in preparation method, low in cost, capable of rapidly detecting trithiocyanuric acid trisodium salt in a sample with high sensitivity, suitable for rapid screening of a large number of samples, convenient to carry, transport, store and use, convenient for on-site detection, and also convenient for civil self-inspection.

Description

technical field [0001] The invention relates to the technical field of food detection, in particular to a rapid detection test paper for trisodium thiocyanate, a preparation method and a detection method thereof. Background technique [0002] Trisodium thiocyanate (TMT-Na) is a high-efficiency and rapid rubber vulcanizing agent, which is widely used in vulcanizing agents for acrylate rubber, polychloroether elastomer, neoprene, etc. In addition, TMT-Na is an environmentally friendly heavy metal ion remover, which can chelate with most monovalent and divalent heavy metal ions in aqueous solution to form stable, insoluble compounds with good chemical stability , Widely used in the removal of heavy metal ions in sewage and wastewater. TMT-Na has active sulfhydryl groups and can participate in the formation of disulfide bonds between gluten proteins. In recent years, unscrupulous traders have used TMT-Na to prepare compound flour treatment agents and added them to flour in ord...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/78G01N33/10
CPCG01N21/78G01N33/10G01N2021/7759G01N2021/775
Inventor 巩凡郝莉花冯波杨智灵赵芳王克林葛静静王振旭李晓明乔青青贾利平陈蕾曹硕周博金峻节罗莉赵喜梅李旭樊云霄仝莹莹
Owner HENAN PROVINCE PROD QUALITY SUPERVISION & INSPECTION CENT