A kind of alloy powder preparation method of recycling copper chromium alloy

A kind of alloy powder, copper-chromium alloy technology

Active Publication Date: 2020-12-15
SHAANXI SIRUI ADVANCED MATERIALS CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The existing technology has the following disadvantages. First, during the cutting and grinding process, the alloy chips are easily oxidized, and the impurities in the alloy chips will increase due to the wear of tools and other materials during the process. It consumes a lot of energy and causes waste; secondly, due to its high strength, copper-chromium alloy chips are difficult to densify during the pressing process and require extremely high pressing force, so extremely stringent requirements are put forward for equipment and molds; thirdly, electrode Inductive gas atomization powder making, the material cannot be fully smelted, the impurity and gas content of the electrode material itself cannot be reduced, and the electrode densification degree is low, and it is easy to deflate and short circuit during the electrode induction gas atomization process, resulting in the inability to continue production; Fourth, the electrode induction gas atomization pulverization needs to consume a lot of energy and protective gas, and the production cost is much higher than the cost of raw materials, which makes this method unable to be applied in batches

Method used

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  • A kind of alloy powder preparation method of recycling copper chromium alloy

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] Embodiment 1: a kind of copper-chromium alloy reclaims the alloy powder preparation method of recycling, comprises the following steps:

[0027] S1: Washing and drying

[0028] First use high-pressure water to wash the impurities adhered to the surface of CuCr alloy scraps, then use ultrasonic cleaning to remove surface oil and oxide layers, and finally dry them;

[0029] S2: vacuum induction melting

[0030] The CuCr alloy scrap that step S1 obtains is put into the crucible of smelting chamber, and wherein crucible material is magnesium oxide; Wait until vacuum degree reaches 10 -1 Pa, start heating; the heating power gradient increases, 40kW for 3 minutes, 60kW for 3 minutes, and finally rise to 80kW. When the CuCr alloy in the crucible starts to melt, turn off the vacuum system, reduce the heating power to 20kW, and then fill it with argon to the standard Atmospheric pressure; preheat the tundish, keep the power of the heating device at 7kW, and then increase the h...

Embodiment 2

[0037] Embodiment 2: a method for preparing copper-chromium alloy reclaimed alloy powder, comprising the following steps:

[0038] S1: Washing and drying

[0039] First use high-pressure water to wash the impurities adhered to the surface of CuCr alloy scraps, then use ultrasonic cleaning to remove surface oil and oxide layers, and finally dry them;

[0040] S2: vacuum induction melting

[0041] Put the CuCr alloy scraps obtained in step S1 into the crucible of the smelting chamber, wherein the material of the crucible is calcium oxide; until the vacuum degree reaches 10 -1 Pa, start heating; the heating power gradient increases, 40kW for 4min, 60kW for 4min, and finally rise to 80kW, when the CuCr alloy in the crucible starts to melt, turn off the vacuum system, reduce the heating power to 20kW, and then fill it with argon to the standard Atmospheric pressure; preheat the tundish, keep the power of the heating device at 18kW, and then increase the heating power to 125kW to ...

Embodiment 3

[0048] Embodiment 3: a kind of alloy powder preparation method of copper-chromium alloy recycling, comprises the following steps:

[0049] S1: Washing and drying

[0050] First use high-pressure water to wash the impurities adhered to the surface of CuCr alloy scraps, then use ultrasonic cleaning to remove surface oil and oxide layers, and finally dry them;

[0051] S2: vacuum induction melting

[0052] Put the CuCr alloy scraps obtained in step S1 into the crucible of the smelting chamber, wherein the material of the crucible is zirconia; until the degree of vacuum reaches 10 -1 Pa, start heating; the heating power gradient increases, 40kW for 5min, 60kW for 5min, and finally rise to 80kW, when the CuCr alloy in the crucible starts to melt, turn off the vacuum system, reduce the heating power to 20kW, and then fill it with argon to the standard Atmospheric pressure; preheat the tundish, keep the power of the heating device at 30kW, and then increase the heating power to 150...

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Abstract

The invention provides a preparation method of alloy powder for recycling copper-chromium alloy. The preparation method specifically comprises the following steps of cleaning and drying; vacuum induction melting, specifically, putting CuCr alloy leftovers into a crucible of a melting chamber, and starting to heat when the vacuum degree reaches 10 <-1 > Pa or below; increasing the heating power ina gradient mode, keeping at 40 kW for 3-5 min, keeping at 60 kW for 3-5 min, finally raising to 80 kW, when the CuCr alloy in the crucible starts to be molten, closing a vacuum system, and then introducing argon to reach the standard atmospheric pressure; then increasing the power to 100-150 kW, melting the CuCr alloy, and obtaining the completely molten CuCr alloy molten liquid; refining and removing impurities; atomizing to prepare powder; and screening to obtain CuCr alloy powder with different particle sizes. The method provided by the invention is simple in process and low in manufacturing cost, the copper-chromium alloy waste can be efficiently recycled, and the CuCr alloy powder low in gas content and high in purity is prepared.

Description

technical field [0001] The invention relates to the technical field of alloy powder production, in particular to a method for preparing alloy powder for copper-chromium alloy recovery and reuse. Background technique [0002] Copper-chromium alloy is a series of alloys formed by adding chromium and other trace alloy elements on the basis of copper. Because of its high strength and hardness after heat treatment, as well as good electrical and thermal conductivity and corrosion resistance, it is widely used in many industries. Has been widely used. [0003] Existing copper-chromium alloy recycling usually cuts and grinds copper-chromium alloy scraps first, then presses the obtained copper-chromium alloy chips into consumable electrodes, and then uses electrode induction gas atomization to make powder; the prefabricated The bar is refined in the area, and the metal liquid flows down through the nozzle continuously and vertically. When passing through the nozzle, the metal liqui...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B22F9/08C22B7/00
CPCB22F9/082B22F2009/001B22F2009/0824B22F2009/0848C22B7/001Y02P10/20
Inventor 张石松王小军刘凯李鹏杨斌姚培建师晓云王文斌李刚
Owner SHAANXI SIRUI ADVANCED MATERIALS CO LTD
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