Kelp antioxidant additive and preparation method thereof
An anti-oxidant additive, kelp technology, which is applied in the field of food additives, can solve the problems of harming human health and inability to provide nutrients to the human body, achieve non-toxic side effects, improve the activity of glutathione peroxidase, and enhance immune cells Effect
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Embodiment 1
[0013] A preparation method of kelp antioxidant additive, comprising the steps of:
[0014] (1) According to the mass parts, add 120 parts of kelp powder, 10 parts of magnesium chloride, 1.0 parts of zinc sulfate and 1000 parts of distilled water into the mixer, keep stirring, then replace the air in the mixer with nitrogen, repeat After three times, nitrogen gas was filled, and the temperature of the reaction system was raised to 70°C under the protection of nitrogen gas, and the reaction was carried out for 6 hours; after the reaction was completed, it was cooled to room temperature, and 40 parts of sodium hydroxide solution was added. The concentration of the sodium hydroxide solution was 16%, and the reaction was carried out at room temperature 60min, then extracted three times with ethyl acetate, combined organic phases were recrystallized with ethanol and then dried to obtain the kelp extract;
[0015] (2) 1 part by weight of the above kelp extract, 3 parts by weight of ...
Embodiment 2
[0017] A preparation method of kelp antioxidant additive, comprising the steps of:
[0018] (1) According to the mass parts, add 125 parts of kelp powder, 15 parts of magnesium chloride, 1.2 parts of zinc sulfate and 1000 parts of distilled water into the mixer, keep stirring, then replace the air in the mixer with nitrogen, repeat After three times, nitrogen gas was filled, and the temperature of the reaction system was raised to 80°C under the protection of nitrogen gas, and the reaction was carried out for 8 hours; after the reaction was completed, it was cooled to room temperature, and 45 parts of sodium hydroxide solution was added. The concentration of the sodium hydroxide solution was 18%, and the reaction was carried out at room temperature 90min, then extracted three times with ethyl acetate, combined organic phases were recrystallized with ethanol and then dried to obtain the kelp extract;
[0019] (2) 3 parts by weight of the above-mentioned kelp extract, 4 parts by...
Embodiment 3
[0021] A preparation method of kelp antioxidant additive, comprising the steps of:
[0022] (1) According to the mass parts, add 130 parts of kelp powder, 20 parts of magnesium chloride, 1.5 parts of zinc sulfate and 1000 parts of distilled water into the agitator, stir continuously, and then replace the air in the agitator with nitrogen, repeat After three times, nitrogen was filled, and the reaction system was heated to 90°C under the protection of nitrogen, and reacted for 10 hours; after the reaction was completed, it was cooled to room temperature, and 50 parts of sodium hydroxide solution was added. The concentration of the sodium hydroxide solution was 20%, and the reaction was carried out at room temperature 120min, then extracted three times with ethyl acetate, combined organic phases were recrystallized with ethanol and then dried to obtain the kelp extract;
[0023] (2) 5 parts by weight of the above-mentioned kelp extract, 5 parts by weight of sodium bicarbonate, 0...
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