Environment-friendly fireproof coating and preparation method thereof
A fire retardant coating and environmental protection technology, applied in fire retardant coatings, anti-corrosion coatings, coatings, etc., can solve the problems of complex raw materials and environmental pollution, and achieve the effects of short process flow, good comprehensive performance, high production efficiency and high yield rate
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Embodiment 1
[0030] An environmentally friendly fireproof coating is characterized in that it is made of the following components in parts by weight: 10 parts of vinyl modified hyperbranched polyphosphate, 5 parts of acrylate modified p-aminophenyl calixyrrole, 1 ,3-bis(oxiranylmethyl)-5-(2-propenyl)-1,3,5-triazine-2,4,6(1H,3H,5H)-trione / 3, 50 parts of 3'-diamino-4,4'-difluorodiphenylsulfone polycondensate, 0.5 part of azobisisobutyronitrile, 15 parts of attapulgite, 1 part of tributyl phosphate, and 1 part of sodium hexametaphosphate.
[0031] The 1,3-bis(oxiranylmethyl)-5-(2-propenyl)-1,3,5-triazine-2,4,6(1H,3H,5H)-trione / The preparation method of 3,3'-diamino-4,4'-difluorodiphenylsulfone polycondensate comprises the following steps: 1,3-bis(oxiranylmethyl)-5-(2- propenyl)-1,3,5-triazine-2,4,6(1H,3H,5H)-trione, 3,3'-diamino-4,4'-difluorodiphenylsulfone polycondensate, Sodium hydroxide and 1,4-naphthoquinone were added to dimethyl sulfoxide, stirred and reacted at 80°C for 6 hours, th...
Embodiment 2
[0036] An environmentally friendly fireproof coating is characterized in that it is made of the following components in parts by weight: 13 parts of vinyl modified hyperbranched polyphosphate, 6 parts of acrylate modified p-aminophenyl calixyrrole, 1 ,3-bis(oxiranylmethyl)-5-(2-propenyl)-1,3,5-triazine-2,4,6(1H,3H,5H)-trione / 3, 55 parts of 3'-diamino-4,4'-difluorodiphenylsulfone polycondensate, 0.7 parts of azobisisoheptanonitrile, 17 parts of pozzolan, 1.5 parts of Deqian 3100 defoamer, and 1.5 parts of sodium polycarboxylate.
[0037] The 1,3-bis(oxiranylmethyl)-5-(2-propenyl)-1,3,5-triazine-2,4,6(1H,3H,5H)-trione / The preparation method of 3,3'-diamino-4,4'-difluorodiphenylsulfone polycondensate comprises the following steps: 1,3-bis(oxiranylmethyl)-5-(2- propenyl)-1,3,5-triazine-2,4,6(1H,3H,5H)-trione, 3,3'-diamino-4,4'-difluorodiphenylsulfone polycondensate, Potassium hydroxide and chlorobenzoquinone were added to N,N-dimethylformamide, stirred and reacted at 82°C for ...
Embodiment 3
[0042] An environmentally friendly fireproof coating is characterized in that it is made of the following components in parts by weight: 15 parts of vinyl modified hyperbranched polyphosphate, 7.5 parts of acrylate modified p-aminophenyl calixyrrole, 1 ,3-bis(oxiranylmethyl)-5-(2-propenyl)-1,3,5-triazine-2,4,6(1H,3H,5H)-trione / 3, 60 parts of 3'-diamino-4,4'-difluorodiphenylsulfone polycondensate, 1 part of azobisisoheptanonitrile, 20 parts of talc, 2 parts of defoamer BYK0882, and 2 parts of sodium hexametaphosphate.
[0043] The 1,3-bis(oxiranylmethyl)-5-(2-propenyl)-1,3,5-triazine-2,4,6(1H,3H,5H)-trione / The preparation method of 3,3'-diamino-4,4'-difluorodiphenylsulfone polycondensate comprises the following steps: 1,3-bis(oxiranylmethyl)-5-(2- propenyl)-1,3,5-triazine-2,4,6(1H,3H,5H)-trione, 3,3'-diamino-4,4'-difluorodiphenylsulfone polycondensate, Sodium carbonate and 1,4-naphthoquinone were added to N,N-dimethylacetamide, stirred and reacted at 85°C for 7 hours, then ...
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