Preparation method and application of high-efficiency dispersing agent for water-based automobile coating
A dispersant, automotive technology, applied in the coating and other directions, can solve the problems of large pigment agglomerates and easy flocculation, and achieve the effect of strong dispersing ability, good fullness, and excellent pigment wetting and dispersing.
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Embodiment 1
[0034] Embodiment 1: Preparation of high-efficiency dispersant for water-based automotive coatings
[0035] Step S1: Add 12 parts by weight of cyclohexanone, 1.5 parts by weight of macromolecular initiator PSt-C1, and 4 parts by weight of component A to the reactor, and stir evenly; in this example, component A is tertiary acrylic acid For butyl ester, the reactor is equipped with auxiliary reaction equipment such as stirring paddles, thermometers, and condensers;
[0036] Step S2: Add the catalytic system formed by mixing cuprous bromide and bipyridine into the reaction kettle of step S1 under nitrogen environment, stir evenly, heat up to 120°C for polymerization reaction, and continue the reaction for 15 hours;
[0037] Step S3: Add 30 parts by weight of amine acrylate to the reaction kettle of step S2, fully react for 3.5 hours and then cool to room temperature, wherein the amine acrylate in this embodiment is dimethylaminoethyl methacrylate;
[0038] Step S4: discharging ...
Embodiment 2
[0041] Embodiment 2: the use of product application embodiment (taking black as example) the preparation of water-based environment-friendly high-performance high-pigment automotive paint and its performance index.
[0042] The high-efficiency dispersant for water-based automotive coatings prepared in Example 1 is a wetting and dispersing agent, and a resin-free grinding system is adopted. Quantitative water-based high-pigment pigments, deionized water, and wetting and dispersing agents are weighed and mixed evenly, and then put into a sand mill for further preparation. After grinding until the fineness meets the requirements, select functional additives and water-based dispersions, configure them under dispersion conditions, and stir evenly to obtain component B, wherein the addition amount of each component (by weight) is as follows:
[0043] The following formulas are proportioned according to parts by weight:
[0044]
[0045] Hydrophilic modified polyisocyanate as comp...
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