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High-temperature device for preparing lithium ion battery negative electrode material and preparation method of material

A technology for lithium-ion batteries and high-temperature devices, which is applied to battery electrodes, negative electrodes, and methods for chemically changing substances by using atmospheric pressure. It can solve problems such as poor batch stability, excessively large particles, and uneven material quality. , to achieve batch stability

Active Publication Date: 2021-01-12
JIANGXI IAMETAL NEW ENERGY TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] In the existing silicon oxide negative electrode preparation technology, not only high energy consumption, low yield, but also poor batch stability and uneven material quality levels severely limit the large-scale preparation of silicon oxide negative electrode materials
In addition, when C-SiOx formed after pulverization and coating is mechanically mixed with other negative electrode materials, there are still problems such as excessive particle size and pulverization during the cycle, which leads to rapid deterioration of battery performance and seriously affects the performance of silicon oxide. Negative electrode industrial application

Method used

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  • High-temperature device for preparing lithium ion battery negative electrode material and preparation method of material
  • High-temperature device for preparing lithium ion battery negative electrode material and preparation method of material

Examples

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Embodiment 1

[0052] This embodiment provides a high-temperature device for preparing negative electrode materials for lithium-ion batteries. The high-temperature device includes a bin body 1 and a vacuum device 4 connected to the bin body, a transmission device 5, a gas mixing device 6, and an exhaust gas treatment device 7; The bin body 1 includes a vacuum reaction chamber 2 and a rotary collection chamber 3. The front end of the rotary collection chamber 3 is connected to the vacuum reaction chamber 2, and the rear end of the rotary collection chamber 3 is respectively connected to the vacuum device, the transmission device and the gas mixing device. The processing device 7 is connected to the vacuum reaction chamber; the vacuum reaction chamber 2 and the rotary collection chamber 3 are respectively equipped with independent heating devices, which can independently control the temperature of the vacuum reaction chamber and the rotary collection chamber.

[0053] The vacuum reaction chambe...

Embodiment 2

[0081] This embodiment provides a method for preparing a negative electrode material of a lithium ion battery. The method is specifically to prepare a negative electrode material for a lithium ion battery by compounding silicon oxide and other negative electrode materials. Using the high temperature device, the vacuum reaction chamber 2 The silicon oxide raw material is placed inside, and other negative electrode materials are placed in the rotary collection chamber 3 as the core material, and the reaction temperatures of the vacuum reaction chamber and the rotary collection chamber are respectively controlled, so that silicon oxide is deposited on the surface of the core material to form nano Level coating layer, after carbon coating in the high temperature device, the negative electrode material of lithium ion battery can be obtained.

[0082] The preparation method uses the above-mentioned high temperature device, comprising the following steps:

[0083] (1) Keep the vacuum...

Embodiment 3

[0090] This embodiment provides a method for preparing a lithium-ion battery negative electrode material, using the above-mentioned high-temperature device, comprising the following steps:

[0091] (1) Keep the vacuum tightness of the gas quick-connection pipeline 602 and the tail gas quick-connection pipeline 702, put silicon oxide raw material in the reaction chamber 201 of the vacuum reaction chamber, and install Enter the core material (metal germanium), and the mass ratio of the silicon oxide raw material to the core material is 1:1;

[0092] (2) Seal the first sealing flange 102, the fixing flange 3012, and the second sealing flange 103, and open the vacuum device 4 for vacuuming; when the degree of vacuum reaches 50-100Pa, open the transmission device 5 , the rotary collection chamber 3 rotates at a speed of 50r / min;

[0093] (3) The heating layer of the vacuum reaction chamber 2 is heated to 1400° C. to fully vaporize the silicon oxide raw material to obtain silicon o...

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Abstract

The invention relates to a high-temperature device for preparing a lithium ion battery negative electrode material and a preparation method of the material. The high-temperature device comprises a binbody, and a vacuum device, a transmission device, a gas mixing device and a tail gas treatment device which are connected with the bin body, wherein the bin body comprises a vacuum reaction chamber and a rotary collection chamber, the front end of the rotary collection chamber communicates with the vacuum reaction chamber, the rear end of the rotary collection chamber is respectively connected with the vacuum device, the transmission device and the gas mixing device, and the tail gas treatment device is connected with the vacuum reaction chamber; and the vacuum reaction chamber and the rotarycollection chamber are each provided with an independent heating device, and the temperature of the vacuum reaction chamber and the temperature of the rotary collection chamber can be independently controlled. The preparation method comprises the following steps: respectively placing a silicon monoxide raw material and an inner core material in the vacuum reaction chamber and the rotary collection chamber, respectively controlling the reaction temperatures of the vacuum reaction chamber and the rotary collection chamber, depositing gas-phase silicon monoxide on the surface of the inner core material to form a nano-scale coating layer, and carrying out carbon coating to obtain the lithium ion battery negative electrode material.

Description

technical field [0001] The invention belongs to the technical field of preparation of lithium-ion battery negative electrode materials, and in particular relates to a high-temperature device for preparing lithium-ion battery negative electrode materials and a preparation method thereof. Background technique [0002] With the rapid development of modern consumption, electronics, and electric vehicle industries, the research and industrialization of lithium-ion batteries as energy sources are becoming more and more important. As an important indicator to measure battery performance, the energy density of lithium-ion batteries still needs to be further improved. However, the energy density improvement of traditional carbon-based anode materials has reached the limit, which cannot meet the needs of high energy density lithium-ion batteries. In order to promote the further development of lithium-ion batteries and related industries and meet the market demand for lithium-ion batt...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01B33/18C01B32/05H01M4/36H01M4/48H01M4/62H01M10/0525B01J3/00B01J3/03
CPCC01B33/18C01B32/05H01M4/366H01M4/483H01M4/625H01M10/0525B01J3/006B01J3/002B01J3/03H01M2004/021H01M2004/027C01P2004/80Y02E60/10
Inventor 徐泉刘柱李阁黄林波李金熠程晓彦
Owner JIANGXI IAMETAL NEW ENERGY TECH CO LTD
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