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174results about How to "High batch stability" patented technology

Preparation method of titanium alloy bars

The invention discloses a preparation method of titanium alloy bars. The finished titanium alloy bars are prepared through the following steps: heating prepared TC4-DT titanium alloy ingots to 1150 to 1200 DEG C; cogging and forging a beta phase zone of the ingots with a fast forging press; heating forging stocks to Tbeta-50 to Tbeta-20 DEG C through a resistance furnace; carrying out repeated upsetting and extension forging by the fast forging press; forging forged stocks to required dimensions at a forging temperature of Tbeta-70 to Tbeta-40 DEG C to obtain titanium alloy bars with uniform tissues; and carrying out duplex annealing on the obtained titanium alloy bars with the uniform tissues. The preparation method has the advantages of convenient operation, strong controllable technology, high stability of batches of prepared bars, and good repeatability. The titanium alloy bars prepared through the method of the present invention has the advantages of strong plasticity, qualified macrostructure, high strength and fracture toughness, and low fatigue crack growth rate.
Owner:西安大富宇航科技有限公司

Preparation method of TC4ELI titanium alloy bar

The invention provides a preparation method of a TC4ELI titanium alloy bar. The preparation method comprises the following steps of: (1) carrying out cogging forging; (2) carrying out upsetting forging; (3) carrying out precise forging; (4) carrying out shearing, straightening and annealing treatment in sequence, thereby obtaining the cylindrical TC4ELI titanium alloy bar with the cross-section diameter of 15mm-90mm. The invention also provides a preparation method of the TC4ELI titanium alloy bar. The preparation method comprises the following steps of: (1) carrying out cogging forging; (2) carrying out upsetting forging; (3) carrying out precise forging; (4) rolling; (5) carrying out shearing, straightening and annealing treatment in sequence, thereby obtaining the cylindrical TC4ELI titanium alloy bar with the cross-section diameter of 8mm-15mm. The preparation method is simple in process, strong in repeatability and suitable for large-scale industrial production; the TC4ELI titanium alloy bar prepared by adopting the preparation method is uniform and fine in structure, high in microscopic structure level and excellent in mechanical property.
Owner:NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH

Preparation method for inverted LED white-light chip of chip scale package

The invention discloses a preparation method for an inverted LED white-light chip of chip scale package, and the method comprises the following steps: temporarily fixing an UV solidifying adhesive tape (2-1) on the upper surface of a die bonding positioning light cover (1); setting flip chips (3) on the upper surface of the UV solidified adhesive tape (2-1) according to the position of the die bonding positioning light cover (1); employing a fluorescent glue film (4) to cover the flip chips (3); carrying out vacuumizing and heating, and enabling the fluorescent glue film (4) to be solidified and packaged on the flip chips (3); carrying out cutting along gaps among the all packaged flip chips (3); removing the die bonding positioning light cover (1); carrying out UV irradiation and enabling the UV solidified adhesive tape (2-1) to be solidified, and obtaining the inverted LED white-light chip (5) of chip scale package. The method simplifies the technological flow, avoids glue mixing and dispensing in the original technology, improves the production efficiency and yield, and greatly reduces the production cost. The method completely avoids the sinking of phosphor, enables the batch stability of the inverted LED white-light chips (5) to be high, and enabling the color temperature of the inverted LED white-light chips (5) to be consistent.
Owner:TECORE SYNCHEM

Direct-throwing type sour dough fermenting agent as well as preparation method and application thereof

The invention relates to a direct-throwing type plant lactobacillus sour dough fermenting agent as well as a preparation method and an application thereof. The preparation method of the direct-throwing type plant lactobacillus sour dough fermenting agent comprises the following steps of: activating plant lactobacillus, preparing the direct-throwing type plant lactobacillus sour dough fermenting agent and the like. The sour dough fermenting agent disclosed by the invention can be used for producing flour foods including breads, steamed breads and the like; the sour dough fermenting agent can be used for delaying the ageing of the foods including the breads and the like, the flavor is very obviously improved and the use is convenient; and the direct-throwing type plant lactobacillus sour dough fermenting agent has a lead reducing function, is very suitable for industrial production and has a very good application prospect.
Owner:JIANGNAN UNIV

Preparation method of lithium ion battery cathode material

The invention discloses a preparation method of a lithium ion battery cathode material, belonging to the technical field of preparation of lithium ion battery cathode materials. The lithium ion battery cathode material is a nickel manganese lithium aluminate three-component cathode material and has the chemical formula of LiNi0.5-xMn0.5-xAl2xO2, wherein x=0.01-0.075. The three components of nickel, manganese and aluminum are precipitated at the same time by using a complete coprecipitation method so that the three elements are evenly mixed on the molecular level, and the solid-phase reaction is performed on the three elements and lithium salt, thereby the uniform degree of a product is greatly improved; spherical nickel manganese lithium aluminate particles are prepared by using mechanical ball milling and spray pelleting technologies, thereby the stacking density of the materials is improved and the volume energy density of the battery is further increased. Besides, the method realizes that a nickel manganese aluminum precursor is fully mixed with the lithium salt, therefore, the batch stability of the products is improved and large-scale production is facilitated.
Owner:王志勇

Silicon embedded redox graphene/graphite phase carbon nitride composite material, preparation and application thereof

The invention discloses a silicon embedded redox graphene / graphite phase carbon nitride composite material, preparation and application thereof. The silicon embedded redox graphene / graphite phase carbon nitride composite material comprises a redox graphene / graphite phase carbon nitride composite matrix serving as the base material, nano-silicon spheres that act as the active centre and are evenlydispersed and embedded in the lamellar gap of the redox graphene / graphite phase carbon nitride composite matrix, and a carbon layer that is located on the surfaces of the nano-silicon spheres and canstrengthen the chemical bonding force between the active centre and the base material. The silicon embedded redox graphene / graphite phase carbon nitride composite material provided by the invention has good electrochemical cycle performance, excellent compatibility and structural stability, can give play to good synergistic effect between the components, also has high batch stability, and is easyfor large-scale production.
Owner:DALIAN MARITIME UNIVERSITY

Method for treatment on high-voltage Ni-Co-Mn ternary positive electrode material by surface drying method

InactiveCN105374996AReduce the amount of residual lithium on the surfaceImprove adaptabilityCell electrodesSecondary cellsAir atmosphereManganese
A method for treatment on a high-voltage Ni-Co-Mn ternary positive electrode material by a surface drying method comprises the following steps of firstly, sieving and dispersing a lithium salt, weighing and adding the lithium salt and a Ni-Co-Mn hydroxide into a blending mixer for mixing according to a mole ratio of (1.0-1.2):1, mixing the lithium salt and the Ni-Co-Mn hydroxide to obtain mixed raw powder; secondly, loading and compacting the mixed raw powder in a pot, carrying out sintering in a high-temperature air atmosphere, cooling until the tapping temperature is less than or equal to 80 DEG C, taking a powder body out, and carrying out weak breaking, dispersing and sieving on the powder body in a drying room to obtain a high-dispersion Ni-Co-Mn ternary material substrate; thirdly, weighing and adding the high-dispersion Ni-Co-Mn ternary material substrate and a cladding agent A into a grinding blending mixer for mixing according to a mole ratio of 1:(0.1-0.001), and allowing the high-dispersion Ni-Co-Mn ternary material substrate and the cladding agent to be in mixed contact, thereby obtaining a mixed material; loading the mixed material in the pot, cooling after sintering the mixed material in the high-temperature air atmosphere to a solid phase until the tapping temperature is less than or equal to 80 DEG C, taking the powder body out, and carrying out sieving to obtain the high-voltage Ni-Co-Mn ternary material. According to the method, the high-voltage Ni-Co-Mn ternary positive electrode material which has the characteristics of high capacity, high cycle, high temperature and favorable safety can be prepared.
Owner:CAIHONG GRP ELECTRONICS CO LTD

Novel process for preparing battery-grade iron phosphate material by using iron hydroxide

The invention discloses a novel process for preparing a low-cost battery-grade iron phosphate material by using iron hydroxide. The process comprises the following steps: mixing a zero-valent iron source and corrosive acid in a molar ratio, and adding a certain amount of primary water and ammonia water; stirring to react for 0 to 24 hours, and slowly adding hydrogen peroxide until the iron source disappears and the solution turns to orange; adding surfactant which is 1 to 5 percent that of the mass of the iron source into the solution; adding a reagent containing phosphate radicals into the solution according to a certain molar ratio of iron element to phosphor element under a stirring condition to obtain iron phosphate precipitate; filtering and washing the product 3 to 5 times with the primary water which is 3 to 7 times the weight of the iron phosphate; drying in vacuum for 4 to 12 hours at 50 and 80 DEG C to obtain FePO4.2H2O. The process for preparing battery grade iron phosphate is simple and easy to carry out and low in cost; and the prepared product has good product crystal structure, few impurities and uniform granularity and is suitable for industrial scale production; moreover, the lithium iron phosphate prepared by the process has high specific capacity, low self-discharge, high tap density, stable product performance and good processing performance.
Owner:ZHEJIANG NARADA POWER SOURCE CO LTD +2

Preparation method of TC17 titanium alloy flat square section bar

The invention provides a preparation method of a TC17 titanium alloy flat square section bar. The preparation method comprises the following steps that (1) a riser and an ingot bottom of a TC17 titanium alloy cast ingot are cut off, and surface defects are removed; (2) billet forging is performed on the TC17 titanium alloy cast ingot, and primary forging stocks are obtained; (3) first middle forging is performed on the primary forging stocks, and first middle forging stocks are obtained; (4) second middle forging is performed on the first middle forging stocks, and second middle forging stocks are obtained; (5) sawing is performed on the second middle forging stocks, then forming forging is performed, and a semi-finished flat square section bar is obtained; and (6) heat treatment is performed on the semi-finished flat square section bar, and the TC17 titanium alloy flat square section bar with the length of 850 mm to 1600 mm, the width of 132 mm and the thickness of 65 mm to 100 mm is obtained. The preparation method has the advantages of integral technical scheme, strong process controllability, uniformity in product texture and shape, excellent overall performance, high batch stability and high yield and is suitable for large-scale industrial production.
Owner:WESTERN TITANIUM TECH

Secondary sintering synthesis method for lithium iron phosphate

The invention discloses a secondary sintering synthesis method for lithium iron phosphate, which comprises the following process steps of: 1, preparing materials in a molar ratio of lithium to iron to phosphorus element of (0.98-1.02): 1: 1, and mixing the materials uniformly; 2, heating the obtained mixture to between 350 and 550 DEG C, preserving the heat for 5 to 15 hours, then cooling the mixture along with a furnace to room temperature, and crushing the obtained material to obtain lithium iron phosphate powder; 3, mixing the obtained lithium iron phosphate powder, a carbon source and a solvent uniformly, drying the mixture and then heating the mixture to between 650 and 850 DEG C, preserving the heat for 10 to 20 hours, then cooling the mixture along with the furnace to room temperature, and crushing, screening and grading the mixture to obtain a screened product which is a lithium iron phosphate product produced by the method. The method is simple; the operation is convenient; the prepared lithium iron phosphate has high electric conductivity, good storage performance, good low-temperature performance and good batch consistency; and the method greatly improves the electric conductivity, low-temperature performance, storage performance and batch stability of the lithium iron phosphate. The method is suitable for industrialized production and can replace the conventional one-time high temperature sintering process.
Owner:谢朝华 +3

Working electrolyte for ultrahigh-voltage aluminium electrolytic capacitor and manufacturing method thereof

Disclosed in the invention is a working electrolyte for an ultrahigh-voltage aluminium electrolytic capacitor. The working electrolyte comprises the following raw materials, by mass percent: 49 to 76% of a main solvent, 5 to 20% of a secondary solvent, 6 to 25% of a solute, and 3 to 10% of a property-modifying additive. According to the manufacturing method, the main solvent and the secondary solvent are mixed; the solute is added at the temperature of 100 to 115 DEG C, and stirring is carried out and the temperature rises 130 to 135 DEG C; heat-preservation stirring is carried out and reaction is also carried out for 10 to 40 minutes; and cooling is carried out until the temperature is reduced to 70 to 90 DEG C and then the property-modifying additive is added, thereby completing preparation. According to the invention, with application of special materials, the special preparation process is used; and on the basis of optimized formulas, the combined effect of the materials is realized. The prepared working electrolyte having advantages of reasonable cost, long service life, high high-temperature stability, and high batch stability can meet the urgent need of factories in the country, especially the need of the high-end manufacturers.
Owner:上海洪微电子科技有限公司

Preparation method of GH4169 alloy bars

The invention relates to a preparation method of GH4169 alloy bars, and belongs to the technical field of high-temperature alloy hot machining. The problems that the grain sizes of GH4169 alloy bars in the prior art are not uniform, and batch-to-batch production is not stable are solved. The preparation method includes the following steps that 1, a free forging press is used for upsetting cast ingots in a closed upsetting or free forging upsetting manner, wherein the upsetting deformation temperature is 1,110+ / -20 DEG C; 2, forging blanks obtained after upsetting are subjected to surface machining, black skin and defects are removed, and cylindrical forging blanks are obtained; and 3, the machined blanks are heated, the heating temperature is 980 DEG C-1,060 DEG C, the forging blanks continue to be subjected to heat preservation for 60 min-480 min after being fully heated, then the forging blanks are discharged out of a furnace to be subjected to hot extrusion, the time between furnacedischarging and extrusion starting is controlled within 5 min, the surfaces of the forging blanks are coated with a lubricant before the forging blanks are extruded, and a glass cushion is arranged between an extrusion die and the forging blanks. High-stability manufacturing that the structures of the sections, the heads and the tails of the GH4169 alloy bars with the diameters larger than or equal to 250 mm are uniform and fine, and the grain sizes are smaller than the level 4 or even the level 6 is achieved.
Owner:TIANJIN HEAVY EQUIP ENG RES +1

Method for making steamed buns through utilizing Lactobacillus plantarum

The invention relates to a method for making steamed buns. The method comprises the following steps: activating Lactobacillus plantarum, making a sour dough containing Lactobacillus plantarum, fermenting by utilizing Lactobacillus plantarum to make a steamed bun dough, fermenting small doughs obtained after dividing the steamed bun dough, and steaming the small doughs. The method uses the Lactobacillus plantarum CCFM8661 to ferment in order to make steamed breads and uses no commercial yeasts, the steamed buns made through the method have a rich flavor, and an insufficient flavor disadvantage caused by the use of a single yeast to ferment of products mode in the present market is overcome; and the steamed buns made through the method have the advantages of fine construction structure, good batch stability, and high safety.
Owner:JIANGNAN UNIV

Environment-friendly stable polyamide acid solution and preparation method thereof

The invention relates to a polyamide acid solution and a preparation method thereof, in particular to an environment-friendly stable polyamide acid solution and a preparation method thereof. The environment-friendly stable polyamide acid solution and the preparation method thereof aim at solving the problems of difficultly of large-scale preparation of a polyamide acid aqueous solution, wide molecular weight distribution and poor batch stability in the prior art. The environment-friendly stable polyamide acid solution is prepared from tertiary amine, aromatic primary amine, aromatic dianhydride, aromatic diamine and water, wherein repetitive units of polyamide acid in the polyamide acid aqueous solution are shown in the specification. The preparation method includes the steps that tertiary amine, aromatic primary amine, aromatic dianhydride, aromatic diamine and water are taken, and weighed tertiary amine is divided into tertiary amine A and tertiary amine B; water and aromatic primary amine are added into a three-necked bottle under certain conditions for a reaction; weighed tertiary amine A and weighed aromatic diamine are added into the three-necked bottle for a reaction, reaction liquid is heated, then weighed aromatic dianhydride is added into the three-necked bottle and stirred for a reaction, then the reaction liquid is cooled, weighed tertiary amine B is added and stirred for a reaction, and the reaction liquid is cooled and subjected to standing.
Owner:INST OF PETROCHEM HEILONGJIANG ACADEMY OF SCI

Preparation method of Mg-contained hydrogen storage alloy

The invention belongs to the technical field of functional metal alloy materials and relates to a smelting method applicable to La-Mg-Ni series and Mg2Ni type hydrogen storage alloys, which comprises the following concrete steps of: weighing the components of the La-Mg-Ni series hydrogen storage alloy as ABy according to a stoichiometric proportion, wherein the A is LaxMg1-x, the B is Niy-zCz, and the C is Mn, Fe, Mo, Co, Al, Ti, Si, V, Cr, Cu, Zn, Zr, Nb, W, Hf, Ta, B, P or / and Sn, La, Mg and Ni, adding into a crucible of a medium-frequency induction smelting furnace, and placing on a feeding device in the furnace after carrying out surface processing on Mg blocks; carrying out vacuum pumping until the vacuum degree is 10-2 Pa, introducing He and Ar protective gases mixed according to a certain proportion until the air pressure in the furnace reaches 0.01-0.1MPa, regulating the power range to be 15-35kW, and controlling the temperature at 600-1300 DEG C until metals are molten; and stopping electrifying for 1-10 minutes, adding the Mg into the crucible through the feeding device in the furnace, regulating the power range to be 15-35kW, controlling the temperature at 600-1300 DEG C and casting after smelting for 1-10 minutes. The process has simple operation, good controllability, stable components of the prepared hydrogen storage alloy and lower cost and can realize low-cost and large-scale production.
Owner:UNIV OF SCI & TECH BEIJING

Preparing method for titanium alloy panel

The invention relates to a preparing method for a titanium alloy panel. An alloy comprises, by mass percentage, 4%-5% of Al, 1%-2% of Ni, 0.7%-0.8% of Cu, 0.5%-0.7% of V, 0.1%-0.2% of Bi, 0.1%-0.2% of Si, 0.07%-0.09% of In, 0.05%-0.06% of Ni, 0.03%-0.04% of Pd, 0.03%-0.04% of Pr, 0.01%-0.02% of Y and the balance titanium and titanium non-metallic inclusion; and the titanium alloy panel is obtained through ingot casting, annealing treatment, forging, hot rolling, cold rolling, quenching treatment and heat preservation. The intensity of the titanium alloy panel reaches more than 1200 MPa.
Owner:WUXI QINGYANG MACHINERY MFG

Porous polyimide composite retainer tube blank pre-heating, limiting and pressing process

ActiveCN103507193AAvoid loose textureLow tensile strengthPorosityPre treatment
The invention discloses a porous polyimide composite retainer tube blank pre-heating, limiting and pressing process. The process comprises the following eight steps: 1, performing pretreating of vacuum drying on a raw material of polyimide; 2, weighing according to the weight percentage, and preparing a porous polyimide composite material; 3, forming the size of a retainer mould; 4, screening the porous polyimide composite material to remove small particles or impurities which are not mixed uniformly; 5, filling the porous polyimide composite material into the mould; 6, putting the mould filled with the material into a constant-temperature drying box, and preserving heat for 20-40 minutes; 7, taking out the mould, and limiting and pressing the mould; and 8, after demoulding, putting into a programmable sintering furnace for sintering and shaping. By the porous polyimide composite retainer tube blank pre-heating, limiting and pressing process, in a free sintering process, phenomena such as loose texture, low tensile strength and large pore size and porosity of a product due to a small forming pressure as well as stress cracking and poor consistency of material properties between tube blanks due to a large forming pressure can be avoided.
Owner:LUOYANG BEARING RES INST CO LTD

Polytetrafluoroethylene composite, polytetrafluoroethylene composite holder for bearing and preparation method of polytetrafluoroethylene composite holder for bearing

The invention discloses a polytetrafluoroethylene composite, a polytetrafluoroethylene composite holder for a bearing and a preparation method of the polytetrafluoroethylene composite holder for the bearing. The polytetrafluoroethylene composite is prepared from, by mass, 3%-8% of coupling agent modified nano aluminum oxide, 2%-5% of molybdenum disulfide and 90%-95% of polytetrafluoroethylene. The polytetrafluoroethylene composite is prepared by compounding polytetrafluoroethylene, coupling agent modified nano aluminum oxide and molybdenum disulfide. Nano aluminum oxide is large in heat conductivity and small in grain size, the crushing resistance, heat conductivity and wear resistance of the composite can be remarkably improved, the material surface activity can be improved after nano aluminum oxide is modified with a coupling agent, and surface binding force is increased. The friction and wear resistance of the composite can be enhanced through molybdenum disulfide; the composite has excellent self-lubricating performance and high tensile strength, crushing resistance, heat conductivity and friction and wear resistance are obviously improved, and the requirement of the ultralow-temperature high-speed bearing on the holder is met.
Owner:LUOYANG BEARING RES INST CO LTD

Short carbon fiber reinforced phenol formaldehyde resin-based composite material and preparation method thereof

The invention discloses a short carbon fiber reinforced phenol formaldehyde resin-based composite material and a preparation method thereof. The preparation method comprises: carrying out high-temperature heat treatment on a continuous carbon fiber bundle to remove surface metal ions and impurities, washing until the surface is free of glue, and drying to obtain a pre-treated continuous carbon fiber bundle; preparing a short carbon fiber bundle coated with a phenol formaldehyde resin layer on the surface from the pre-treated continuous carbon fiber bundle by using equipment for preparing a short carbon fiber bundle coated with a phenol formaldehyde resin layer on the surface; mixing the short carbon fiber bundle coated with the phenol formaldehyde resin layer on the surface and phenol formaldehyde resin powder according to a certain ratio to obtain a mixture; pre-treating the mixture, and carrying out cold pressing pre-molding to prepare a pre-molded plate material; and loading the pre-molded plate material in a hot pressing mold, carrying out curing molding, and carrying out post-treatment to obtain the short carbon fiber reinforced phenol formaldehyde resin-based composite material.
Owner:ZHEJIANG ASIA PACIFIC MECHANICAL & ELECTRONICS

Method for preparing aluminum-titanium alloy impeller

The invention discloses a method for preparing an Al-Ti alloy impeller. The method is characterized in that the alloy comprises the following components by mass percent: 7% to 8% of Al, 0.7% to 0.8% of Ni, 0.7% to 0.8% of Co, 0.8% to 0.9% of V, 0.3% to 0.4% of Cr, 0.3% to 0.4% of Sn, 0.07% to 0.09% of Fe, 0.03% to 0.04% of Cu, 0.05% to 0.06% of Pr, 0.01% to 0.02% of Ce, 0.5% to 0.6% of Mg, 0.5% to 0.7% of Mo, 0.7% to 0.9% of Si and the balance of Ti and inevitable nonmetallic inclusions. The strength of a Ti alloy board can reach more than 1200MPa.
Owner:TONGSHAN COUNTY FENGHUA IND & TRADE

Preparation method of silver powder with low heat shrinkage rate

The invention provides a preparation method of silver powder with low heat shrinkage rate. The preparation method comprises the steps that a silver nitrate water solution and a reducing agent solutionare simultaneously added into a dispersing agent water solution to obtain silver powder particles, then after the surface of the silver powder is coated with a surfactant, the silver powder particlesproduce mutual impact, collision and friction shearing by jet stream, so as to achieve the surface smoothness and dispersion treatment of the silver powder, finally a high-energy pulse current is utilized to provide high energy in a very short time to promote the recrystallization of the silver powder in a faster way at a lower temperature, the crystal defects of the silver powder is improved, and the silver powder particles are prevented from agglomerating. The heat shrinkage rate of the prepared silver powder is less than 5% at 700 DEG C, good degree of sphericity and dispersity are achieved, the particle size D100 is not more than 5 [mu]m, the tap density is not less than 4 g / cm<3>, and a broad application prospect in the field of miniaturization and high-reliability circuits is achieved.
Owner:西安宏星电子浆料科技股份有限公司

Titanium alloy plate

The invention discloses a titanium alloy plate, relating to the technical field of formulas for the titanium alloy plate. The titanium alloy plate is prepared from the following ingredients in percentage by mass: 0.16% of Ni, 6% of Al, 0.6% of Zn, 0.5% of Nb, 0.100% of V, 0.45% of Mo, 0.08% of Bi, 0.45% of Mg, 0.85% of Si, 0.02% of Sn, 0.06% of Co, 0.06% of Cr, 0.03% of Ta, 0.07% of Ca, 0.05% of Y, 0.8% of Mn, 0.30% of Pb, 0.06% of Zr, 0.06% of Te, 0.06% of Fe, 0.15% of Cu, 0.35% of W and the balance of titanium and non-metallic inclusion. In the formula, a proper amount of elements such as silicon, iron, aluminum and magnesium are added, the high-temperature creep resistance of alloy is improved, and the stability of plate performance is improved.
Owner:TIANGONG AIHE SPECIAL STEEL

Preparation method of lithium ion battery positive electrode material

The invention provides a preparation method of a lithium ion battery positive electrode material. The preparation method comprises the steps of mixing a lithium source, an iron source and a phosphatesource according to a mole ratio of Li, Fe and P being (1-1.02):(0.955-1):1, and performing pre-sintering in air to obtain a mixture of Li3Fe2(PO4)3 and Fe2O3, wherein the sintering time is 4-5 hours,and the sintering temperature is 500-700 DEG C; and mixing the mixture and a carbon source of which the mass accounts for 3-10% of Li3Fe2(PO4)3, grinding in a grinding medium, and performing secondary sintering under a non-oxidization or reduction atmosphere after drying to obtain an LFP / C positive electrode material, wherein the sintering time is 5-6 hours, and the sintering temperature is 600-800 DEG C. By the method, the smoothness of synthesis particle and the batch stability and the cycle stability of a product can be effectively improved.
Owner:PULEAD TECH IND

Silicide/oxide composite negative electrode material with lithium silicate interface layer and preparation method

The invention provides a silicide / oxide composite negative electrode material with a lithium silicate interface layer and a preparation method, and belongs to the field of lithium ion batteries. The silicide / oxide composite negative electrode material with the lithium silicate interface layer comprises a silicon active center, an oxide substrate and the lithium silicate interface layer, wherein the lithium silicate interface layer is positioned between the silicon active center and the oxide substrate. By adopting a method that chemical deposition is combined with high-temperature solid-phase reaction, excessive lithium ions are adsorbed by virtue of good adsorption properties of deposition reaction products, so that the lithium silicate interface layer is formed in situ between the silicon active center and the oxide substrate through high-temperature solid-phase reaction of the lithium ions and trace silicon oxide on a silicon surface, not only is a continuous channel for lithium ion transmission provided, but also the lithium silicate interface layer can be used as an effective protection interface to reduce the reaction property of the active center and the oxide substrate, and therefore, good electrochemical circulation properties can be achieved. The processes related to the silicide / oxide composite negative electrode material are very simple, and the composite material prepared by using the method is excellent in interfacial compatibility.
Owner:DALIAN MARITIME UNIVERSITY

Lithium niobite/niobium-base oxide/silicon compound cathode material, preparation method and application thereof

The invention discloses a lithium niobite / niobium-base oxide / silicon compound cathode material, a preparation method and an application thereof. The lithium niobite / niobium-base oxide / silicon compoundcathode material comprises a silicon active center and a lithium niobite / niobium-base oxide mixed shell layer uniformly coated on the surface of the silicon active center. The lithium niobite / niobium-base oxide / silicon compound cathode material provided by the invention takes lithium niobite as a fast ion conductor, so that the rapid transferring of lithium ions under room temperature and even high temperature can be effectively guaranteed; the synergic alloying effect of the lithium niobite and the niobium-base oxide is beneficial to the structure and surface stability of the silicon duringan electrochemical reaction process, so that the lithium niobite / niobium-base oxide mixed shell layer can be used as a stress buffer layer, an ionic conduction layer and a surface stabilizing layer; the lithium niobite / niobium-base oxide / silicon compound cathode material has high initial coulombic efficiency and excellent electrochemical circling stability performance.
Owner:DALIAN MARITIME UNIVERSITY

Matte ABS resin composition and preparation method thereof

ActiveCN105440562AEven and fine matteHigh batch stabilityPolymer sciencePolyamide
The invention discloses a matte ABS resin composition and a preparation method thereof. The composition comprises, in parts by weight, 100 parts of ABS resin, 0.5-10 parts of a polymer micropowder, 0.5-5 parts of a compatibilizer, 0.05-1 part of an anti-oxidant, and 0.1-2 parts of a lubricant. The polymer micropowder is a semicrystalline polyamide micropowder, the molecular main chain contains a repeated amide group -[NHCO]-, the melting point is 245-390 DEG C, the glass-transition temperature is 55-185 DEG C, and the particle size is 1-50 mu m. The matte ABS resin composition is obtained by pre-mixing the above raw materials in a high-speed mixer for 3-10 min and then performing extrusion granulation on the premix through a double-screw extruder. Compared with the prior art, the ABS resin composition with excellent matte effect is directly prepared through a one-step process, the preparation method is simple in technology, the prepared ABS resin composition is super low in luster, and the problems that luster distribution is not uniform, physical and mechanical performances are deteriorated and technology is complex are solved.
Owner:SHANGHAI KUMHO SUNNY PLASTICS

Method for controlling homogeneity of structure properties of high-strength and high-plasticity TB6 titanium alloy wires

ActiveCN108893691AOptimizing the preparation process parametersHigh room temperature tensile strengthStructure propertyRoom temperature
The invention belongs to the technical field of preparation of titanium alloy wires, and particularly relates to a method for controlling homogeneity of structure properties of high-strength and high-plasticity TB6 titanium alloy wires. The method comprises the following steps: carrying out multi-pass large deformation hot rolling on a TB6 titanium alloy bar with the specification of phi 40mm- phi45mm* 800mm-1200mm at first to obtain a bar with the specification of phi 9 mm-phi 10 mm; then carrying out single-phase region solid-solution treatment and then carrying out cold rolling, and controlling total deformation of cold rolling to be 15-36% to obtain a wire with the specification of phi 6 mm-phi 7 mm; and finally, carrying out ageing treatment on the wire at the temperature of 520-560 DEG C. The method is simple in process parameter setting, convenient to operate and high in process controllability, and the tensile strength sigma b of the wire in an aged state at the room temperature is greater than or equal to 1050 MPa, the yield strength sigma 0.2 is greater than or equal to 1000 MPa, the elongation delta 5 is greater than or equal to 15%, the percentage reduction of area psiis greater than or equal to 50%, the batch stability is high, and the repeatability is good.
Owner:AVIC BEIJING INST OF AERONAUTICAL MATERIALS
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