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A kind of concrete hydration temperature rise inhibitor and preparation method thereof

A technology for concrete and inhibitor, applied in the field of concrete admixtures, can solve the problems of uncertainty of concrete performance, reduce the total amount of heat of hydration, inconvenient use, etc., achieve low product quality control requirements, large economic benefit potential, and reduce environmental The effect of pollution

Active Publication Date: 2022-04-22
中建西部建设西南有限公司 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In terms of concrete admixtures, it is common to use dextrin-based concrete hydration heat control materials to control the cement hydration rate by controlling its solubility in water, but the effect of reducing the hydration rate is limited and cannot be reduced. The total amount of heat of hydration as a whole is difficult to reduce the temperature peak because the internal heat of large-volume concrete is not easy to dissipate; in addition, the phase change energy storage material is used to absorb the heat of cement hydration to reduce the highest temperature peak, but there is a large amount Large, inconvenient use and other defects, and there are uncertainties in the impact on other properties of concrete, which limits its application to a certain extent

Method used

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  • A kind of concrete hydration temperature rise inhibitor and preparation method thereof
  • A kind of concrete hydration temperature rise inhibitor and preparation method thereof
  • A kind of concrete hydration temperature rise inhibitor and preparation method thereof

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Embodiment 1

[0028] The preparation process of the present embodiment concrete hydration temperature rise inhibitor comprises:

[0029] Preparation of modified waste concrete hydration products: Mix 80 parts of 300-mesh waste concrete cement stone powder, 5 parts of nano-zinc oxide, 10 parts of sodium acetate, and 5 parts of hydroxyethylidene diphosphonic acid in a high-speed mixer at 800 r / min Stir for 3 hours, and finally dry it at 105°C for 40 minutes; wherein, the particle size of nano-zinc oxide is 80nm, sodium acetate is anhydrous sodium acetate, AR, 96%; hydroxyethylidene diphosphonic acid is a 60% aqueous solution .

[0030] Preparation of modified metakaolin: kaolin was calcined at 900°C for 2 hours, then poured into 5% pyrophosphoric acid solution at 23°C for water quenching to obtain water quenched slag of modified metakaolin.

[0031] Preparation of concrete hydration temperature rise inhibitor: pour 5 parts of modified waste concrete hydration products, 40 parts of modified m...

Embodiment 2

[0033] The preparation process of the present embodiment concrete hydration temperature rise inhibitor comprises:

[0034] Preparation of modified waste concrete hydration products: Mix 85 parts of 350-mesh waste concrete cement stone powder, 5 parts of nano-zinc oxide, 5 parts of sodium acetate, and 5 parts of hydroxyethylidene diphosphonic acid in a high-speed mixer at 700r / min Stir for 4 hours, and finally dry it at 105°C for 40 minutes; wherein, the particle size of nano-zinc oxide is 100nm, sodium acetate is anhydrous sodium acetate, AR, 96%; hydroxyethylidene diphosphonic acid is a 60% aqueous solution .

[0035] Preparation of modified metakaolin: calcining kaolin at 880°C for 3 hours, then pouring into 5% pyrophosphoric acid solution at 20°C for water quenching to obtain water quenched slag of modified metakaolin;

[0036] Preparation of concrete hydration temperature rise inhibitor: 5 parts of modified waste concrete hydration products, 45 parts of modified metakaoli...

Embodiment 3

[0038]The preparation process of the present embodiment concrete hydration temperature rise inhibitor comprises:

[0039] Preparation of modified waste concrete hydration products: Mix 90 parts of 400-mesh waste concrete cement powder, 2 parts of nano-zinc oxide, 5 parts of sodium acetate, and 3 parts of hydroxyethylidene diphosphonic acid in a high-speed mixer at 800r / min Stir for 3.5 hours, and finally dry at 105°C for 40 minutes; wherein, the particle size of nano-zinc oxide is 60nm, sodium acetate is anhydrous sodium acetate, AR, 96%; hydroxyethylidene diphosphonic acid is 60% aqueous solution.

[0040] Preparation of modified metakaolin: calcining kaolin at 900°C for 2.5 hours, then pouring into 5% pyrophosphoric acid solution at 23°C for water quenching to obtain water quenched slag of modified metakaolin;

[0041] Preparation of concrete hydration temperature rise inhibitor: pour 10 parts of modified waste concrete hydration products, 33 parts of modified metakaolin, 2...

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Abstract

The invention provides a concrete hydration temperature rise inhibitor, which belongs to the technical field of concrete admixtures. It is prepared by grinding, sieving and drying the following components by mass: 5-10 parts of modified waste concrete hydration product, 20-45 parts of modified metakaolin, 2-10 parts of sodium metasilicate, sulfuric acid 5-10 parts of salt, 30-50 parts of fly ash. The invention also provides a preparation method of the concrete hydration temperature rise inhibitor. The raw material of the hydration temperature rise inhibitor of the present invention includes discarded concrete cement stone, which has the advantages of resource utilization of solid waste, reduces environmental pollution, and conforms to the trend of energy saving and environmental protection; the modified waste concrete hydration product and modified metakaolin have the advantages of being used in concrete water The function of slow gradual release during the hydration process ensures arbitrary adjustment within the control range to meet the control of hydration progress; the preparation process of the concrete hydration temperature rise inhibitor of the present invention is simple, only involving calcination, grinding and dispersion, and product quality control It has low requirements, high production efficiency and great potential for economic benefits.

Description

technical field [0001] The invention belongs to the technical field of concrete admixtures, in particular to a concrete hydration temperature rise inhibitor and a preparation method thereof. Background technique [0002] With the rapid development of my country's infrastructure construction, there are more and more large-scale modern technical facilities and high-rise buildings, and mass structural concrete, as an important part of its main body, has emerged in recent years. Due to the large construction volume of mass concrete, the internal heat of hydration in the concrete is not easy to be exported in a short period of time, resulting in high internal temperature of mass concrete and large temperature difference between inside and outside, which may easily cause cracks in mass concrete and affect the quality of the project. [0003] At present, the temperature and cracks of mass concrete structures are generally controlled from two aspects of material design and construct...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B22/14C04B103/22
CPCC04B40/0039C04B2103/22C04B22/0006C04B22/08C04B22/142
Inventor 兰聪张武宗王军张远刘东刘霞袁文韬杨仕海祝云
Owner 中建西部建设西南有限公司
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