Viscose large biological fiber containing ginseng/ganoderma lucidum/lycium barbarum/saffron crocus and preparation method of viscose large biological fiber
A technology of biological fiber and saffron, which is applied in the field of fiber to achieve the effect of promoting circulation, antibacterial effect, and prolonging the action period
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preparation example Construction
[0050] Preparation of temperature sensitive phase change agent
[0051] Step 1, prepare the wall:
[0052] Step 11, 1 of 3 parts of melamine powder and 1 formaldehyde solution were weighed according to weight.
[0053] Step 12, the melamine powder and formaldehyde solution weigh in step 11 were added to 100 ml of distilled water, and the stirring rate was 200 m in at a temperature of 78 ° C, stirred well, and the solution A was obtained.
[0054] Step 13, adding urea in the solution A obtained in step 12, and then stirred at a temperature of 78 ° C for 20 min, stirred well, stir well, to obtain a solution B, that is, the sac. wall;
[0055] Step 2, prepare the cystic:
[0056] Step 21, 30 parts of 0.5 wt% SDS solution, 30 parts of 6 wt% polyethylene glycol solution, 500 parts of the node octadecyl solution according to the weight parts.
[0057] Step 22, 0.5 wt% SDS solution as used in step 21 and 6 wt% polyethylene glycol solution were added to the n-octadecytic liquid, and the r...
preparation example 1
[0065] Step 1, 3 parts of the ginseng extract, 16 parts of Ganoderma lucidum extract, 6 columi extract, 28 red flowers extract, 90 parts of the porous adsorbent, 200 parts of the temperature sensitive phase change agent, coupling agent 1 Copy;
[0066] Step 2, mix the ginseng extract, Ganoderma extract, 枸杞 extract, saffron extract, and porous adsorbent, at a closed condition of 60 ° C, stirring at a rotational speed of 200R / min for 24 h, resulting in a load active ingredient Active adsorbent;
[0067] Step three, the temperature-sensitive phase change agent weigh in step one is added to 100 parts of distilled water, and the ultrasonic dispersion (controlling the power of up to 300 W) is 20 min, and the dispersion is obtained.
[0068] Step 4. Add the active adsorbent prepared in step II to the dispersion produced in step three, and the coupling agent is added to a shear force at a temperature of 50 ° C. The shear force is 5000 IPS. A modified raw liquid containing joint particle...
preparation example 2
[0072] Step 1, 4 parts of the ginseng extract, 18 serum extract, 7.5 枸 提 extracts, 30 cases of safflower extract, 95 parts of the porous adsorbent, 220 parts of the temperature sensitive phase, 220 parts, coupling agent 2 Copy;
[0073] Step 2, a ginseng extract, ganoderma extract, 杞 extract, safflower extract, and porous adsorbent, at a closed condition of 60 ° C, stirring at a rotational speed of 200R / min for 26 h, resulting in a load-loaded active ingredient Active adsorbent;
[0074] Step three, adding the temperature sensitive phase degraded in step one to 100 parts of distilled water, ultrasonic dispersion (control of ultrasonic waves of 300 W and 40 kHz) 30 min, resulting in dispersion;
[0075] Step 4. Add the active adsorbent prepared in step II to the dispersion made in the step three, and the coupling agent is added to the shear force at a temperature of 50 ° C. 40 min, A modified raw liquid containing joint particles is obtained;
[0076] Step 5, the modified raw liq...
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