Three-dimensional graphene antenna and preparation method thereof
A graphene, three-dimensional technology, applied in the direction of graphene, antenna, resonant antenna, etc., can solve the problems of three-dimensional graphene physical and chemical properties, difficult to operate, complex methods, etc.
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Embodiment 3
[0033] The specific preparation process of the three-dimensional graphene antenna in this embodiment is as follows:
[0034] 1. Preparation of graphene dispersion.
[0035] Such as figure 2 As shown, weigh 5g of natural graphite flakes and 2.5g of NaNO 3 , was added to 130 mL of 98 wt% H 2 SO 4 , put the three together, mix well and continue to stir for 2h under ice bath conditions. Then weigh KMnO 4 15g, put it into the reaction beaker, and continue to react for 2h. Then the reaction beaker was transferred to a water bath at 37° C. for 1 h. Then the temperature was raised to 98°C, and 230 mL of deionized water was measured and added into the reaction beaker, and the reaction was continued for 30 minutes. Then add 400 mL of deionized water and 10 mL of H 2 o 2 , placed on a magnetic stirrer and stirred for 1 hour. After the reaction, wash with HCL to remove sulfate radicals, and then repeatedly wash with deionized water until pH = 7 to obtain a graphene oxide soluti...
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