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Rice hull silicon slow-release porous material for air purification and preparation method thereof

A technology for air purification, porous materials, applied in the fields of botanical equipment and methods, air quality improvement, chemicals for biological control, etc., can solve the problem of short duration, high concentration of released gas, slow release time and slow release The amount cannot be precisely controlled, etc., to achieve the effects of low cost, prolonged sustained release time, and accurate and controllable sustained release amount and time.

Active Publication Date: 2021-05-11
苏州北美国际高级中学
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Air purification refers to providing overall solutions for various indoor environmental problems such as sterilization and disinfection, dust reduction and haze removal, removal of harmful decoration residues and peculiar smells, so as to improve living and office conditions and improve physical and mental health; however, the existing purification materials for sterilization and disinfection , such as a negative oxygen ion purifier, which uses its own negative ions to purify, remove dust, deodorize, and sterilize the air. However, the service life of negative ions in the air is very short, so it needs to be continuously injected into the air. sustained release;
[0003] Secondly, chlorine dioxide is recognized by the World Health Organization as an A1-level high-efficiency bacteriostatic agent due to its strong oxidizing properties and reactivity. Long-term defects;
[0004] And the existing air purification materials generally adopt chlorine dioxide air purification gel, but the preparation process of this air purification gel is complicated, and the cost is high, and the slow release time and slow release amount cannot be accurately controlled, and the final product The material cannot be degraded naturally, and it is easy to cause secondary pollution;
[0005] There is also the existing air purification gel, which realizes the slow release of chlorine dioxide by dispersing chlorite and acid into the hydrogel. The control of slow release mainly controls the gas diffusion stage of chlorine dioxide. The hole prolongs the diffusion period, the service period is short, generally less than two months, the release is unstable, the concentration of the released gas is high at the beginning, and the subsequent release is unstable
[0006] Therefore, for the above-mentioned purification materials, due to the short reaction time between the sterilizing media, the use time is shortened, resulting in a low purification effect, and it is necessary to continuously replace new purification materials, which leads to problems such as increased costs. The invention provides A rice husk silicon slow-release air-purifying porous material and its preparation method to solve the problems raised in the above-mentioned background technology

Method used

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  • Rice hull silicon slow-release porous material for air purification and preparation method thereof

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preparation example Construction

[0022] The present invention provides a technical solution: a rice husk silicon slow-release air-purifying porous material and its preparation method. The specific preparation steps of the rice husk silicon slow-release air-purifying porous material are as follows:

[0023] A, first get a certain equal portion of chlorite and dissolve it in paraffin to obtain a powder mixture, then press it through a powder tablet machine, and form a chlorite reaction layer after tableting;

[0024] B, get a certain equal portion of the acid and dissolve it in paraffin to make a powder mixture, then press it through a powder tablet machine, after the tableting, the acid-containing layer reaction layer is formed;

[0025] C, the chlorite reaction layer obtained in step A, and the acid-containing layer reaction layer obtained in step B, add rice husk silica between them, and then use a powder tablet press to perform tabletting together, and finally form The upper reaction layer is a chlorite rea...

Embodiment 1

[0030] Mix 1g of sodium chlorite and 2g of paraffin wax powder, heat to 65°C, stir to completely dissolve the chlorite in the paraffin wax, and compress the above mixture cooled to room temperature with a powder tablet machine at 2MPa; 0.5g of oxalic acid Mix it with 1g of paraffin wax powder, heat it to 65°C, stir evenly, and compress the mixture of oxalic acid and paraffin wax powder cooled to room temperature with a powder tablet press at 2MPa; Pressing tablets to form a sandwich structure micro-reaction slow-release space purification tablet;

[0031] The microscopic scanning electron microscope picture of rice husk silica is shown in the appendix Figure 1 The particle diameter of nano-silica is about 10-40 nanometers, and the nano-particles are covered with worm-like channels. The pore diameter of the pores is 4 nanometers tested by nitrogen adsorption, and the specific surface area of ​​rice husk silica is about 200m2 / g. The micro-reaction space purification tablet has...

Embodiment 2

[0033] Mix 3g of sodium chlorite and 8g of paraffin wax powder, heat to 65°C, stir to completely dissolve the chlorite in the paraffin wax, and compress the above mixture cooled to room temperature with a powder tablet machine at 9MPa; 2g of citric acid Mix it with 3g of paraffin wax powder and heat it to 65°C, stir evenly, and compress the mixture of oxalic acid and paraffin wax powder cooled to room temperature with a powder tablet press at 9MPa; add 2g of rice husk silica between the above two pieces, together at 9MPa Press into tablets to form a sandwich structure micro-reaction slow-release space purification tablet. The micro-reaction space purification tablet has a sterilization rate of over 99.9% at 25°C, an effective volume of 12 cubic meters, and an effective time of 120 days.

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Abstract

The invention discloses a rice hull silicon slow-release porous material for air purification and a preparation method. The porous material is composed of an outer reactant diffusion layer and an inner micro-reaction layer. The rice hull silicon slow-release porous material for air purification is prepared from 1-8 g of chlorite, 1-16 g of paraffin, 0.5-4 g of acid and 1-5 g of rice hull silicon dioxide. According to the invention, by implementing control in two stages, namely reaction and diffusion, the slow release time of chlorine dioxide gas is effectively prolonged to three months or more, and stable release of the chlorine dioxide gas is realized; and air slow release is utilized for sterilization, a slow release amount and slow release time are accurate and controllable, cost is as low as several cents, the material is very green and environmentally friendly, and finally generated substances can safely return to the environment.

Description

technical field [0001] The invention relates to the technical field of environmental protection, in particular to a rice husk silicon slow-release air-purifying porous material and a preparation method thereof. Background technique [0002] Air purification refers to providing overall solutions for various indoor environmental problems such as sterilization and disinfection, dust reduction and haze removal, removal of harmful decoration residues and peculiar smells, so as to improve living and office conditions and improve physical and mental health; however, the existing purification materials for sterilization and disinfection , such as a negative oxygen ion purifier, which uses its own negative ions to purify, remove dust, deodorize, and sterilize the air. However, the service life of negative ions in the air is very short, so it needs to be continuously injected into the air. sustained release; [0003] Secondly, chlorine dioxide is recognized by the World Health Organi...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A01N25/08A01N25/18A01N25/34A01N59/00A01P1/00A01P3/00
CPCA01N25/08A01N25/18A01N25/34A01N59/00Y02A50/20
Inventor 董雷邱皓
Owner 苏州北美国际高级中学
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