Tobacco shreds containing aquilaria agallocha extract, cigarette and preparation method thereof
A technology of extracting and extracting Chinese agarwood, applied in the direction of preparing tobacco, tobacco, processing tobacco, etc.
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Embodiment 1
[0029] Example 1 Shredded Tobacco and Cigarettes Containing the Extract of Agarwood Aloes
[0030] S1: Take Qinan agarwood (obtained from Reke No. 2 Jiexiang for 2 years), crush it, pass through a 100-mesh sieve, and then extract it by simultaneous distillation and extraction. The heating temperature is 100°C, the distillation time is 6 hours, and the extraction solvent is dichloromethane. , the extract was concentrated under reduced pressure to a solid-to-liquid ratio of 1 g: 1 mL to obtain Fraction 1 of Agarwood chinensis. The residue powder after distillation was heated and extracted with 75% ethanol under reflux, the heating temperature was 75°C, the heating time was 2h, and the extraction was repeated twice. Mix Fraction 1 and Fraction 2 to obtain the extract of Agarwood chinensis.
[0031] S2: Spray the extract of Agarwood chinensis evenly on the surface of shredded tobacco (the content of Agarwood chinensis extract is 6% of the mass of shredded tobacco), and place the ...
Embodiment 2
[0032] Example 2 Shredded Tobacco and Cigarettes Containing the Extract of Aloes chinensis
[0033] S1: Take Qinan agarwood (obtained from Reke No. 2 Jiexiang for 2 years), crush it, pass through a 100-mesh sieve, and extract by simultaneous distillation and extraction. The heating temperature is 90°C, the distillation time is 3 hours, the extraction solvent is diethyl ether, and the extract Concentrate under reduced pressure to a solid-to-liquid ratio of 1 g: 1 mL to obtain Fraction 1 of Qinan Agarwood. The residue powder after distillation was extracted by heating under reflux with 90% ethanol, the heating temperature was 85°C, the heating time was 3h, and the extraction was repeated twice. Mix Fraction 1 and Fraction 2 to obtain the extract of Agarwood chinensis.
[0034] S2: Spray the extract of Agarwood chinensis evenly on the surface of shredded tobacco (the content of Agarwood chinensis extract is 10% of the mass of shredded tobacco), and place the shredded tobacco at ...
Embodiment 3
[0035] Example 3 Shredded Tobacco and Cigarettes Containing Agarwood Extract
[0036] S1: Take Qinan agarwood (obtained from Reke No. 2 Jiexiang for 2 years), crush it, pass through a 50-mesh sieve, and extract by simultaneous distillation and extraction. The heating temperature is 95°C, the distillation time is 8 hours, the extraction solvent is ether, and the extract is Concentrate under reduced pressure to a solid-to-liquid ratio of 1 g: 1 mL to obtain Fraction 1 of Agarwood Agarwood. The residue powder after distillation was heated and extracted with 95% ethanol under reflux, the heating temperature was 80°C, and the heating time was 3 hours, and the extraction was repeated three times.
[0037] S2: Mix Fraction 1 and Fraction 2 to obtain the extract of Agarwood chinensis, spray the extract of Agarwood chinensis evenly on the surface of cut tobacco (the content of Agarwood chinensis extract is 0.1% of the mass of shredded tobacco), and place the shredded tobacco in Equili...
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