Temperature-responsive well cementation cement slurry and preparation method thereof
A cementing slurry, temperature responsive technology, applied in chemical instruments and methods, materials for heat exchange, composition of drilling holes, etc. Application value and other issues, to avoid thermal decomposition, timely and efficient control, and promote the development of low-temperature mechanical properties
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[0042] A method for preparing a temperature-responsive cementing cement slurry of the present invention is specifically implemented according to the following steps:
[0043] Step 1, preparing bidirectional intelligent temperature control materials, specifically:
[0044] Step 1.1, first, weigh respectively according to mass percentage: urea 10-12%, melamine 3-5%, formaldehyde 34-38%, deionized water 45-50%, triethanolamine 0.5-1.0%, the mass percentage of the above components The sum is 100%; secondly, urea, melamine and formaldehyde are dissolved in deionized water and placed in a three-necked flask with a stirring and condensing reflux device, and triethanolamine is used to adjust the pH of the system to 8-9; finally, the constant temperature Raise the temperature of the water bath to 60-65°C and react for 1.5 hours at a speed of 200-300r / min to obtain the organic resin prepolymer;
[0045] Step 1.2, weighing according to mass percentage: organic resin prepolymer 10-15%, m...
Embodiment 1
[0057] A method for preparing a temperature-responsive cementing cement slurry of the present invention is specifically implemented according to the following steps:
[0058] Step 1.1, at first, weigh respectively according to mass percentage: urea 10%, melamine 3%, formaldehyde 34%, deionized water balance, triethanolamine 0.5%, the sum of above component mass percentage is 100%; Secondly, urea , melamine and formaldehyde were dissolved in deionized water and placed in a three-necked flask with a stirring and condensing reflux device, and the pH of the system was adjusted to 8 with triethanolamine; finally, the temperature of the constant temperature water bath was raised to 60°C, and the speed of 200r / min After reacting for 1.5h, the organic resin prepolymer can be obtained;
[0059] Step 1.2, weighed according to mass percentage: organic resin prepolymer 15%, silicon nitride 0.2%, low melting point paraffin 26%, graphene oxide (GO) 0.05, deionized water balance styrene-male...
Embodiment 2
[0067] A method for preparing a temperature-responsive cementing cement slurry of the present invention is specifically implemented according to the following steps:
[0068] Step 1.1, at first, weigh respectively according to mass percentage: urea 12%, melamine 5%, formaldehyde 38%, deionized water balance, triethanolamine 1.0%, the sum of above component mass percentage is 100%; Secondly, urea , melamine and formaldehyde were dissolved in deionized water and placed in a three-necked flask with a stirring and condensing reflux device, and the pH of the system was adjusted to 9 with triethanolamine; finally, the temperature of the constant temperature water bath was raised to 65°C, and the speed of 300r / min The organic resin prepolymer can be obtained after 1.5 hours of reaction;
[0069] Step 1.2, weighed according to mass percentage: organic resin prepolymer 15%, silicon nitride 0.2%, low melting point paraffin 26%, graphene oxide (GO) agent 0.05%, deionized water 47%, styre...
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