based on li 2 o Lithium secondary battery with positive electrode and negative electrode without active material and preparation method thereof
A lithium secondary battery, inactive technology, applied in the field of electrochemistry, can solve problems such as hindering the effective utilization of lithium metal batteries, difficulties in practical use, and restrictions on the production and preparation of lithium metal batteries, so as to prolong life, reduce negative electrode costs, and increase capacity. and the effect of specific energy
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[0030] The following methods were used to prepare the Li-containing 2 Lithium secondary battery with O positive electrode and active material-free negative electrode:
[0031] S1. Preparation of cathode material lithium oxide
[0032] Lithium oxide by thermal decomposition of lithium peroxide Li 2 O 2 get. First, the lithium peroxide Li 2 O 2 The powder is transferred to the inside of the tube furnace cavity, and argon Ar protective gas is quickly introduced at normal temperature to prevent it from being deteriorated in contact with air. After 5 hours of argon gas Ar, the tube furnace was heated (heating rate: 10 degrees per minute) and kept at 350 degrees for 5 hours. After that, stop heating and cool with the furnace. After the powder temperature reached room temperature, the samples were placed in the transfer chamber and transferred to an Ar glove box for storage. During the whole process, the influence of deterioration caused by contact with air is eliminated.
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