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Method for jointly extracting flavone and pectin from passion fruit peel

A combined extraction and passion fruit technology, applied in skin care preparations, food ingredients containing natural extracts, pharmaceutical formulations, etc., can solve environmental pollution, waste of resources and other problems, to improve dissolution rate, reduce oxidation, and increase extraction rate Effect

Pending Publication Date: 2021-09-24
GUANGXI NORMAL UNIV FOR NATITIES
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Passion fruit in my country is mainly cultivated in Guangxi, Guangdong, Hainan and other southern provinces of China and Taiwan. Among them, Guangxi is the largest passion fruit producing area in my country. Passion fruit is generally used for the production of fruit juice, jelly, fruit dew, and jam. And other products, and its peel is often discarded as waste, which causes a waste of resources and may also cause related problems such as environmental pollution

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] A method for jointly extracting flavonoids and pectin from passion fruit peel, comprising the following steps:

[0033] S1. Clean the passion fruit peel, dry at 45°C, and pulverize to obtain passion fruit peel powder;

[0034] S2. Add 1kg of passion fruit peel powder into the extraction tank, and add ethanol with a volume fraction of 80% according to the solid-to-liquid ratio of 1:48g / mL, and simultaneously add solubilizers triethanolamine and dimethyl carbonate, ethanol, triethanolamine and The volume ratio of dimethyl carbonate is 1000:3:8, and the pH is adjusted to 8.5 with sodium hydroxide. Ultrasonic extraction is performed for 30 minutes. The power of the ultrasonic wave is 230W, and the temperature is 52°C. Extract twice, filter, and separate the filtrate A and filter residue A ;

[0035] S3. Concentrate the filtrate A to 1 / 8 of the original volume under reduced pressure, adjust the pH to 7.2 with hydrochloric acid, pass the filtrate through a D101 macroporous r...

Embodiment 2

[0040] A method for jointly extracting flavonoids and pectin from passion fruit peel, comprising the following steps:

[0041] S1. Clean the passion fruit peel, dry at 45°C, and pulverize to obtain passion fruit peel powder;

[0042] S2. Add 1kg of passion fruit peel powder into the extraction tank, and according to the solid-to-liquid ratio of 1:40g / mL, add ethanol with a volume fraction of 75%, and simultaneously add solubilizer triethanolamine and dimethyl carbonate, ethanol, triethanolamine and The volume ratio of dimethyl carbonate is 1000:3:5, and the pH is adjusted to 8.0 with sodium hydroxide. Ultrasonic extraction is performed for 30 minutes. The power of the ultrasonic wave is 250W, and the temperature is 50°C. Extract twice, filter, and separate the filtrate A and filter residue A ;

[0043] S3. Concentrate the filtrate A to 1 / 10 of the original volume under reduced pressure, adjust the pH to 6.8 with hydrochloric acid, pass the filtrate through a D101 macroporous ...

Embodiment 3

[0048] A method for jointly extracting flavonoids and pectin from passion fruit peel, comprising the following steps:

[0049] S1. Clean the passion fruit peel, dry at 45°C, and pulverize to obtain passion fruit peel powder;

[0050] S2. Add 1kg of passion fruit peel powder into the extraction tank, and according to the solid-to-liquid ratio of 1:60g / mL, add ethanol with a volume fraction of 75%, and simultaneously add solubilizer triethanolamine and dimethyl carbonate, ethanol, triethanolamine and The volume ratio of dimethyl carbonate is 1000:6:5, adjust the pH to 8.5 with sodium hydroxide, extract by ultrasonic wave for 30 minutes, the power of ultrasonic wave is 220W, the temperature is 55°C, extract twice, filter, and separate filtrate A and filter residue A ;

[0051] S3. Concentrate the filtrate A to 1 / 10 of the original volume under reduced pressure, adjust the pH to 7.5 with hydrochloric acid, pass the filtrate through a D101 macroporous resin column, elute with 70% ...

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PUM

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Abstract

The invention discloses a method for jointly extracting flavone and pectin from passion fruit peel. The method comprises the following steps: cleaning, drying and crushing to obtain passion fruit peel powder; adding passion fruit peel powder into an extraction tank, adding ethanol, solubilizer triethanolamine and dimethyl carbonate, adjusting the pH value to 8.0-8.5 by using alkali, carrying out ultrasonic extraction, filtering, and separating filtrate A and filter residue A; passing the filtrate A through a column, and performing reduced pressure distillation to obtain passion fruit peel total flavonoids; taking the filter residue A, inactivating enzyme, adding water, Tween-80 and cellulase, soaking, carrying out ultrasonic extraction for 5-15 minutes, filtering, and separating filtrate B and filter residue B; and concentrating the filtrate B under reduced pressure, decolorizing, carrying out alcohol precipitation, filtering, taking a precipitate, and drying the precipitate to obtain the pectin. According to the method of the invention, the flavone and the pectin can be jointly extracted from the passion fruit peel, and comprehensive utilization of the passion fruit peel is realized.

Description

technical field [0001] The invention relates to the technical field of extraction technology, in particular to a method for jointly extracting flavonoids and pectin from passion fruit peel. Background technique [0002] Passion fruit is native to South America and is a perennial vine of the genus Passiflora in the Passiflora family. It is known for its rich aroma of bananas, pineapples, lemons, strawberries, peaches, pomegranates and other fruits from its juice. Known as "Passion Fruit", it is also a transliteration of its English name "Passionfruit". It is also known as "King of Juice" and "Money Tree" abroad. [0003] Passion fruit juice has excellent color, fragrance, taste and nutrition. It is rich in more than 160 beneficial ingredients such as 17 kinds of amino acids necessary for the human body, multivitamins, and trace elements. , skin care and beauty and other magical effects. [0004] Passion fruit in my country is mainly cultivated in Guangxi, Guangdong, Hainan ...

Claims

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Application Information

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IPC IPC(8): A61K36/185C08B37/00A61K31/732A61K8/9789A61K8/73A61Q19/00A23L33/105A23L33/125A61K131/00
CPCA61K36/185C08B37/0048A61K31/732A61K8/9789A61K8/73A61Q19/00A23L33/105A23L33/125A61K2236/13A61K2236/17A61K2236/15A61K2236/333A61K2236/39A61K2236/51A61K2236/55A61K2800/10A61K2800/82A23V2002/00A23V2200/30A23V2250/2116A23V2250/21A23V2250/5072
Inventor 卢珍兰李致宝余森艳袁芳陈永
Owner GUANGXI NORMAL UNIV FOR NATITIES
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