Method for jointly extracting flavone and pectin from passion fruit peel
A combined extraction and passion fruit technology, applied in skin care preparations, food ingredients containing natural extracts, pharmaceutical formulations, etc., can solve environmental pollution, waste of resources and other problems, to improve dissolution rate, reduce oxidation, and increase extraction rate Effect
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Embodiment 1
[0032] A method for jointly extracting flavonoids and pectin from passion fruit peel, comprising the following steps:
[0033] S1. Clean the passion fruit peel, dry at 45°C, and pulverize to obtain passion fruit peel powder;
[0034] S2. Add 1kg of passion fruit peel powder into the extraction tank, and add ethanol with a volume fraction of 80% according to the solid-to-liquid ratio of 1:48g / mL, and simultaneously add solubilizers triethanolamine and dimethyl carbonate, ethanol, triethanolamine and The volume ratio of dimethyl carbonate is 1000:3:8, and the pH is adjusted to 8.5 with sodium hydroxide. Ultrasonic extraction is performed for 30 minutes. The power of the ultrasonic wave is 230W, and the temperature is 52°C. Extract twice, filter, and separate the filtrate A and filter residue A ;
[0035] S3. Concentrate the filtrate A to 1 / 8 of the original volume under reduced pressure, adjust the pH to 7.2 with hydrochloric acid, pass the filtrate through a D101 macroporous r...
Embodiment 2
[0040] A method for jointly extracting flavonoids and pectin from passion fruit peel, comprising the following steps:
[0041] S1. Clean the passion fruit peel, dry at 45°C, and pulverize to obtain passion fruit peel powder;
[0042] S2. Add 1kg of passion fruit peel powder into the extraction tank, and according to the solid-to-liquid ratio of 1:40g / mL, add ethanol with a volume fraction of 75%, and simultaneously add solubilizer triethanolamine and dimethyl carbonate, ethanol, triethanolamine and The volume ratio of dimethyl carbonate is 1000:3:5, and the pH is adjusted to 8.0 with sodium hydroxide. Ultrasonic extraction is performed for 30 minutes. The power of the ultrasonic wave is 250W, and the temperature is 50°C. Extract twice, filter, and separate the filtrate A and filter residue A ;
[0043] S3. Concentrate the filtrate A to 1 / 10 of the original volume under reduced pressure, adjust the pH to 6.8 with hydrochloric acid, pass the filtrate through a D101 macroporous ...
Embodiment 3
[0048] A method for jointly extracting flavonoids and pectin from passion fruit peel, comprising the following steps:
[0049] S1. Clean the passion fruit peel, dry at 45°C, and pulverize to obtain passion fruit peel powder;
[0050] S2. Add 1kg of passion fruit peel powder into the extraction tank, and according to the solid-to-liquid ratio of 1:60g / mL, add ethanol with a volume fraction of 75%, and simultaneously add solubilizer triethanolamine and dimethyl carbonate, ethanol, triethanolamine and The volume ratio of dimethyl carbonate is 1000:6:5, adjust the pH to 8.5 with sodium hydroxide, extract by ultrasonic wave for 30 minutes, the power of ultrasonic wave is 220W, the temperature is 55°C, extract twice, filter, and separate filtrate A and filter residue A ;
[0051] S3. Concentrate the filtrate A to 1 / 10 of the original volume under reduced pressure, adjust the pH to 7.5 with hydrochloric acid, pass the filtrate through a D101 macroporous resin column, elute with 70% ...
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