Preparation method of monolithic interlayer through hole

A single-layer, silicon wafer technology, applied in chemical instruments and methods, semiconductor/solid-state device manufacturing, electrical components, etc., can solve the problems of residual contamination of reactive gases, different etching rates, non-uniformity, etc., and achieve good through holes. Etching quality, the effect of eliminating the inclination problem

Pending Publication Date: 2021-10-12
SOUTH UNIVERSITY OF SCIENCE AND TECHNOLOGY OF CHINA
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0005] However, at present, ion beam etching (IBE), deep silicon etching (DRIE), reactive ion etching (RIE), focused ion beam etching (FIB), and inductive coupling (ICP) are commonly used for monolithic interlayer vias. Plasma etching usually has a certain inclination problem in the processing of micro-nano through holes; the etching rate will also be different in different grain regions, causing non-uniform etching surface problems; residual pollution of reactive gases after etching, etc.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

preparation example 1

[0063] This preparation example provides a kind of etching solution containing bacillus licheniformis, described etching solution containing bacillus licheniformis is prepared by following preparation method:

[0064] (a) Inoculate Bacillus licheniformis into NA medium and culture at 37°C for 24h, centrifuge at 2000rpm for 10min to remove the secretion of Bacillus licheniformis, aggregate and purify to obtain Bacillus licheniformis;

[0065] (b) Get 300mL of Bacillus licheniformis obtained by aggregation and purification, add 700mL of phosphate buffer solution with a pH value of 7.4, and then cultivate for 4 hours in an environment with a temperature of 37°C to obtain 300,000 live bacteria containing Bacillus licheniformis etchant.

preparation example 2

[0067] This preparation example provides a kind of etching solution containing Bacillus cereus, and the etching solution containing Bacillus cereus is prepared by the following preparation method:

[0068] (a) Inoculate Bacillus cereus into Chua's medium and culture at 37°C for 24 hours, centrifuge at 1800 rpm for 8 minutes to remove the secretion of Bacillus cereus, aggregate and purify to obtain Bacillus cereus;

[0069] (b) Take 300mL of aggregated and purified Bacillus cereus and add 700mL of phosphate buffer solution with a pH value of 7.4, and then culture in an environment with a temperature of 37°C for another 6 hours to obtain a viable count of 320,000 cereus-containing spores Bacillus etchant.

preparation example 3

[0071] This preparation example provides a kind of etching solution containing Alcaligenes faecalis, and the etching solution containing Alcaligenes faecalis is prepared by the following preparation method:

[0072] (a) inoculate Alcaligenes faecalis in Chua's medium and cultivate at 30°C for 24h, remove the excretion of Alcaligenes faecalis by centrifuging at 1500rpm for 10min, gather and purify to obtain Alcaligenes faecalis;

[0073] (b) Add 300mL of Alcaligenes faecalis obtained by aggregation and purification into 700mL of phosphate buffer with a pH value of 7.4, and then culture for another 5 hours in an environment with a temperature of 30°C to obtain 350,000 viable bacteria containing Alcaligenes faecalis bacteria etchant.

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PUM

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Abstract

The invention provides a preparation method of a monolithic interlayer through hole. The preparation method of the monolithic interlayer through hole comprises the following steps of (1) preparing a mask pattern, namely sequentially carrying out spin coating, pre-baking, exposure, development and hardening on a silicon wafer; (2) pre-treating a deoxidation layer, namely soaking the silicon wafer on which a mask pattern is formed in an acid solution, and removing an oxidized SiO2 film on the surface of the silicon wafer; (3) carrying out biochemical variable-temperature etching, namely soaking the silicon wafer of the deoxidation layer in biochemical etching liquid, and performing biochemical variable-temperature etching to form the monolithic interlayer through hole, wherein the biochemical etching solution is an etching solution containing alkali-producing anaerobic bacteria. According to the method for manufacturing the monolithic interlayer through hole based on a biochemical mode, on the premise that the good etching effect and the etching quality of the through hole can be guaranteed, various problems occurring in an existing etching method can be effectively eradicated.

Description

technical field [0001] The invention relates to the technical field of integrated circuit packaging, in particular to a method for preparing through holes between monolithic layers. Background technique [0002] With the continuous breakthrough of integrated semiconductor manufacturing process technology, the performance of integrated circuit devices has developed rapidly, and the corresponding microelectronic packaging technology has gradually become an important factor restricting the development of semiconductor technology. In order to achieve smaller size, faster processing speed and lower manufacturing cost of semiconductor devices. More and more advanced packaging technologies that go beyond traditional packaging concepts have been proposed. Among them, the three-dimensional packaging technology realizes interconnection and communication through interlayer interconnection, which effectively shortens the interconnection length, reduces the parasitic parameters of the i...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): H01L21/768C09K13/00
CPCH01L21/76898C09K13/00
Inventor 叶怀宇王少刚高宸山杨荟茹刘起鹏张国旗
Owner SOUTH UNIVERSITY OF SCIENCE AND TECHNOLOGY OF CHINA
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