Method for preparing aminonitrile organic matter by gas phase method
A technology of aminonitriles and organics, which is applied in the field of preparation of aminonitriles organics by gas phase method, can solve the problems of low molar ratio of organic amides, high conversion rate of organic amides, high selectivity of aminonitriles organics, etc., and achieve high conversion rate of organic amides, The effect of improving the purity and selectivity of high amino nitrile organic substances
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[0174] The preparation method of catalyst A1 is carried out according to CN111659463A, except that in the molding step, a mold matching with catalyst A1 is used for molding to form catalyst A1 with a specific structure, other preparation methods are carried out according to CN111659463A.
[0175] Catalyst A2 to Catalyst A4 have the same structure and preparation method as Catalyst A1, except that the molar ratios of silicon, aluminum and phosphorus are 1:0.8:0.4, 1:0.8:0.8 and 1:0.8:1.6.
[0176] Catalyst B1
[0177] Catalyst B1 is a clover-shaped cylindrical catalyst, which includes a cylindrical body 1 and a protrusion 2, wherein the height of the cylinder is 4.5mm, and the lobes outside the clover circle intersection are the protrusions 2 , specifically as figure 1 As shown, the inside of the dotted line is marked as the main part of the catalyst, and the part outside the dotted circle is marked as the protrusion 2. The diameter of the dotted circle is 3mm, and a marked in...
Embodiment 1
[0202] The present embodiment provides a method for preparing 6-aminocapronitrile by a gas phase method, said method comprising the steps of:
[0203] (1') trimethyl phosphate (accounting for ammonia weight 10ppm) is mixed with ammonia and carried out preheating treatment at 500 DEG C to make ammonia superheated to obtain mixed gas.
[0204](2') The mixed gas and the i-th part of the organic amide in the liquid phase state at 120°C are mixed and gasified at 350°C in the Venturi gasification device and then passed into the first stage of the fixed-bed reactor (a total of 4 in series) The fixed-bed reactor is counted as 4 sections of fixed-bed reactors, and the catalyst of the same weight is filled in each section of fixed-bed reactor), reacts under the first reaction temperature, the first reaction pressure and the first catalyst effect, obtains the first Reaction discharge;
[0205] (3') The i-th reaction output and the i+1 part of the organic amide are passed into the i+1 se...
Embodiment 2
[0212] The present embodiment provides a method for preparing 6-aminocapronitrile by a gas phase method, said method comprising the steps of:
[0213] (1') isopropyl distearoyloxyaluminate (accounting for ammonia weight 20ppm) is mixed with ammonia and then preheated at 600°C to make ammonia superheated to obtain mixed gas.
[0214] (2') The mixed gas and the i-th part of the organic amide in the liquid phase state at 220°C are mixed and gasified at 500°C in the Venturi gasification device and then passed into the first stage of the fixed-bed reactor (a total of 4 in series) The fixed-bed reactor is counted as 4 sections of fixed-bed reactors, and the catalyst of the same weight is filled in each section of fixed-bed reactor), reacts under the first reaction temperature, the first reaction pressure and the first catalyst effect, obtains the first Reaction discharge;
[0215] (3') The i-th reaction output and the i+1 part of the organic amide are passed into the i+1 section fi...
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