Supercapacitor electrode powder material and preparation method thereof
A supercapacitor and electrode powder technology, which is applied in the manufacture of hybrid capacitor electrodes and hybrid/electric double layer capacitors, etc., can solve the problems of poor fluidity of positive electrode materials, difficult electrolyte penetration and unfavorable electrode coating tap density, etc., to achieve Good porosity, good sphericity, high dispersion effect
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Embodiment 1
[0073] The embodiment of the present invention also provides a method for preparing a supercapacitor electrode powder material, which is specifically implemented according to the following steps:
[0074] Step 1, using Co(NO 3 ) 2 , Fe(NO 3 ) 3 , and Na 2 SeO 4 For cobalt source, iron source and selenium source, respectively weigh Co(NO 3 ) 2 , Fe(NO 3 ) 3 , and Na 2 SeO 4 ;
[0075] Step 2, ethanol and deionized water are configured according to the volume ratio of 2:1;
[0076] Step 3, the Co(NO 3 ) 2 , Fe(NO 3 ) 3 , and Na 2 SeO 4 Dissolve in a mixed solution of 500ml ethanol and deionized water, stir magnetically for 30 minutes to form a red transparent solution;
[0077] Step 4, taking a certain amount of polyethylene glycol as a binder, and the mass ratio of polyethylene glycol and cobalt nitrate is 5:1.
[0078] Step 5, adding polyethylene glycol dropwise to the solution in step 1.3, the dropping rate is 10 drops / min, while maintaining strong magnetic...
Embodiment 2
[0093] The embodiment of the present invention also provides a supercapacitor electrode powder material Co 0.9 Fe 0.1 The preparation method of Se is specifically implemented according to the following steps:
[0094] Step 1, using Co(NO 3 ) 2 , Fe(NO 3 ) 3 , and Na 2 SeO 4 For cobalt source, iron source and selenium source, respectively weigh Co(NO 3 ) 2 , Fe(NO 3 ) 3 , and Na 2 SeO 4 ;
[0095] Step 2, ethanol and deionized water are configured according to the volume ratio of 2:1;
[0096] Step 3, the Co(NO 3 ) 2 , Fe(NO 3 ) 3 , and Na 2 SeO 4 Dissolve in a mixed solution of 500ml ethanol and deionized water, stir magnetically for 20 minutes to form a red transparent solution;
[0097] Step 4, taking a certain amount of polyethylene glycol as a binder, and the mass ratio of polyethylene glycol and cobalt nitrate is 3:1.
[0098] Step 5, adding polyethylene glycol dropwise to the solution in step 1.3, the dropping rate is 7 drops / min, while maintaining s...
Embodiment 3
[0113] The embodiment of the present invention also provides a supercapacitor electrode powder material Co 0.8 Fe 0.2 The preparation method of Se is specifically implemented according to the following steps:
[0114] Step 1, using Co(NO 3 ) 2 , Fe(NO 3 ) 3 , and Na 2 SeO 4 Cobalt source, iron source and selenium source, according to the molar ratio of 1.15:0.3:1.1 respectively weigh Co(NO 3 ) 2 , Fe(NO 3 ) 3 , and Na 2 SeO 4 ;
[0115] Step 2, ethanol and deionized water are configured according to the volume ratio of 2:1;
[0116] Step 3, the Co(NO 3 ) 2 , Fe(NO 3 ) 3 , and Na 2 SeO 4 Dissolve in a mixed solution of 500ml ethanol and deionized water, stir magnetically for 20 minutes to form a red transparent solution;
[0117] Step 4, taking a certain amount of polyethylene glycol as a binder, and the mass ratio of polyethylene glycol and cobalt nitrate is 6:1.
[0118] Step 5, adding polyethylene glycol dropwise to the solution in step 1.3, the dropping...
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