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A kind of quartz wafer etching additive and preparation method thereof

A technology for etching additives and quartz wafers, applied in chemical instruments and methods, surface etching compositions, etc., can solve the problems of uneven etching powder slag, scratches, etc., and achieve the purpose of inhibiting acid volatilization and etching acid loss, reducing volatilization, The effect of suppressing the diffusion of odor

Active Publication Date: 2022-07-01
深圳市科玺化工有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] In order to overcome the defects of the above-mentioned prior art, the present invention needs to provide high removal rate and stable rate, long life, easy water cleaning of the wafer after etching, and an etching solution additive that can complete the etching operation after soaking at normal temperature, and the microscopic appearance of the wafer surface after etching Flat and smooth, thickness tolerance less than or equal to 0.2um, etch rate greater than or equal to 4.00um / min, with good dispersion, wetting and sedimentation functions, which can solve the problem of uneven etching powder residue, suspension in the solution, and adsorption on the surface of the wafer after etching. It can effectively inhibit the volatilization of acid and the loss of etching acid, and the smell is mild and non-irritating.

Method used

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  • A kind of quartz wafer etching additive and preparation method thereof
  • A kind of quartz wafer etching additive and preparation method thereof
  • A kind of quartz wafer etching additive and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1~10

[0037] Embodiments 1 to 10: use the No. 1 temperature-controlled stirring liquid tank according to the formula in Table 1, weigh the specified amount of phase-stable solvent according to the mass percentage, add it to the No. 1 tank, set the temperature to normal temperature, and follow the stirring speed of 60 r / min. Weigh the dispersant and the chelating corrosion inhibitor in mass percentage and stir for 20 minutes; under the condition of continuous stirring, the temperature is raised to 50 °C, then stirred at a constant temperature, the rotation speed is set to 200 r / min, and the penetrating agent and wetting agent are added in turn and stirred for 2 hours, until the Completely dissolve evenly, adjust the stirring speed to 120r / min, and set the temperature to 25°C. After the temperature drops to 25°C, add the concave and convex point inhibitor, foam breaker, and sedimentation agent, and stir for 30 minutes to dissolve evenly, which is the finished product of the quartz wafer...

Embodiment 11

[0060] In Example 11, the phase-stable solvent was removed, and the prepared additive solution itself had sediment, was easy to delaminate, and was difficult to use.

Embodiment 12

[0061] In Example 12, the penetrant was removed, and the flatness of the wafer surface after treatment was slightly worse, and the amount of treatment was reduced.

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Abstract

A quartz wafer etching additive is composed of the following components according to weight percentage: 12% to 25% of a phase stable solvent, 1% to 5% of a penetrant, 4% to 8% of a dispersant, and 20% of a chelating corrosion inhibitor. ~30%, wetting agent 15%~25%, foam breaker 8~12%, bump inhibitor 10%~20%, sedimentation agent 1%~2%. The etching solution prepared with the additive of the invention has high removal rate, stable rate and long service life, the etching operation can be completed by soaking at room temperature, and the wafer can be easily washed with water after etching; the etching solution with the additive of the invention is added, and the microscopic appearance of the etched wafer surface is smooth Smooth, thickness tolerance is less than or equal to 0.2um, good dispersion, wetting and sedimentation functions of the additive can reduce the unevenness of etching slag after etching, suspension in solution, and adsorption on the wafer surface. Inhibit acid volatilization and etching acid loss, mild and non-irritating odor.

Description

technical field [0001] The invention relates to the technical field of semiconductor material processing, in particular to a quartz wafer etching additive and a preparation method thereof. Background technique [0002] Quartz crystal is an electronic material second only to monocrystalline silicon. It is used to manufacture electronic components that select and control frequency. It is widely used in various fields of the electronic information industry, such as color TVs, air conditioners, computers, DVDs, wireless communications, etc., especially The application in high-performance electronic equipment and digital equipment is expanding day by day, and low-corrosion tunnel density crystal materials are necessary materials for the production of SMD frequency chips and mobile phone frequency chips. [0003] No matter how fine the final abrasive is after the quartz wafer is ground, there is always a damage layer composed of abrasive and quartz particles on the surface of the ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09K13/08C09K13/00
CPCC09K13/08C09K13/00
Inventor 冉有仁刘三川
Owner 深圳市科玺化工有限公司
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