A class of iridium complexes for oxygen sensing and preparation method thereof
An iridium complex, oxygen sensing technology, applied in indium organic compounds, chemical instruments and methods, platinum group organic compounds, etc., can solve problems such as difficult detection routes, need to be further improved, etc. The effect of excellent photobleaching resistance and good application prospects
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[0039] Example 1: Preparation of ligands and complexes
[0040] (1) Synthesis method of ligand
[0041]The synthesis method of the main ligand: 3-bromocarbazole and bromoethane are dissolved in tetrahydrofuran, heated to reflux under magnetic stirring, cooled to room temperature, extracted with dichloromethane, the organic phase is dehydrated by anhydrous magnesium sulfate, and then reduced. Spin to dry, and silica gel column chromatography obtains 9-ethyl-3-bromocarbazole (compound 1); Phenylphosphino)ferrocene]palladium dichloride was added to the eggplant-shaped flask, deoxygenated, injected with dioxane, heated to reflux under nitrogen protection, cooled to room temperature after the reaction was completed, and extracted with dichloromethane , the organic phase was dewatered by anhydrous magnesium sulfate, then spin-dried under reduced pressure, and silica gel column chromatography was used to obtain compound 2; compound 2, 2-bromopyridine and tetrakis(triphenylphosphine)...
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