Electrode slurry composition and its preparation method, pole piece coated with it and lithium ion battery comprising the pole piece
A lithium-ion battery and electrode slurry technology, applied in the field of lithium-ion batteries, can solve problems such as active lithium consumption, affecting battery power and low-temperature discharge performance, and serious polarization problems, so as to improve cycle stability and cycle life, improve Battery kinetic performance, good film-forming protective effect
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[0038] In one embodiment of the method for preparing the electrode slurry composition according to the present invention, based on the weight of the electrode active material, the added amount of the phosphate ester additive is 0.2-5%, preferably 0.5-5%.
[0039] In another embodiment of the method for preparing the electrode slurry composition according to the present invention, the phosphate ester additive is a phosphate ester additive shown in the following formula II, III or IV:
[0040] Formula II
[0041] Formula III
[0042] Formula IV
[0043] In another embodiment of the method for preparing the electrode slurry composition according to the present invention, the electrode active material is a positive electrode active material or a negative electrode active material, preferably a positive electrode active material; the conductive agent is selected from conductive carbon black , conductive graphite, Ketjen black, carbon nanotubes, carbon fiber (VGCF), one or m...
Embodiment 1
[0067] Step 1: The positive electrode active material LiNi 6 co 2 mn 2 o 2 The conductive agent Super P and the binder PVDF are added to the NMP at a weight ratio of 97.6:1.3:1.1 for slurry mixing, and then a phosphate ester additive is added during the high-speed dispersion process to obtain a positive electrode slurry composition.
[0068] The addition amount of phosphoric acid ester additive is 0.2wt% of positive electrode active material, and described phosphoric acid ester additive has the structure shown in following formula II:
[0069] Formula II
[0070] Step 2: The positive electrode slurry composition prepared in step 1 is evenly coated on a 12 μm aluminum foil current collector, and after drying, it is rolled and cut by a roller press to obtain a positive electrode sheet with a thickness of 100 μm;
[0071] Step 3: Assemble the positive electrode sheet prepared in step 2 with a suitable negative electrode sheet, separator and electrolyte to form a battery; th...
Embodiment 2
[0074] According to the method of Example 1, the positive electrode sheet is made, assembled into a battery for testing, the difference is that, based on the weight of the positive active material, the amount of the phosphoric acid ester additive added is 0.5wt%, and the phosphoric acid ester additive has Structure shown in following formula III:
[0075] Formula III
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