Formula of magnesium-based flame retardant and preparation method
A flame retardant and inorganic flame retardant technology, applied in the field of magnesium-based flame retardant formulation and preparation, can solve the problems of high preparation cost, increased cost, large dosage, etc., and achieves good high temperature resistance and thermal stability, and improves thermal stability. The effect of high performance and low preparation cost
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[0047] A preparation method of magnesium-based flame retardant, said method comprising the following steps:
[0048] 1) Preparation of magnesium-based suspension:
[0049] (a) Take an appropriate amount of magnesium oxide and an organosilane coupling agent into the reaction tank, add a sodium silicate solution into the reaction tank and heat and stir to obtain a magnesium-based suspension;
[0050] (b) filtering the magnesium-based suspension to remove impurities to obtain a pure magnesium-based suspension;
[0051] 2) Preparation of inorganic flame retardant:
[0052] (c) After the diatomite and hydrated silica are pulverized by a ball mill, soaked in water to remove impurities, dehydrated and dried, and then ground into a powder mixture;
[0053] (d) adding an acidic solution to the powder mixture, stirring for 2.5 hours, filtering, removing the precipitate, retaining the acidic solution, adjusting the pH value to 6-6.5, and obtaining a weakly acidic mixed liquid;
[0054...
Embodiment 1
[0068] By the above-mentioned method, according to the weight part of composition preparation:
[0069] 5 parts of magnesium oxide, 3 parts of organic silane coupling agent;
[0070] 15 parts of hydrated silica, 20 parts of diatomaceous earth, 5 parts of aluminum hydroxide particles, 6 parts of silicon dioxide particles, and 45 parts of sodium silicate.
Embodiment 2
[0072] By the above-mentioned method, according to the weight part of composition preparation:
[0073] 7 parts of magnesium oxide, 3.5 parts of organosilane coupling agent;
[0074] 20 parts of hydrated silica, 24 parts of diatomaceous earth, 7.5 parts of aluminum hydroxide particles, 8.5 parts of silicon dioxide particles, and 50 parts of sodium silicate.
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