Melamine softened coating paper and production process thereof
A melamine and production process technology, which is applied in the field of melamine softened coated paper and its production process, can solve the problems of whitening of the surface of the melamine coating layer, low production efficiency, easy scratching and the like, and achieves good curing performance and high production efficiency. , reduce the effect of surface whitening
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preparation example 1
[0047] Preparation of a modifier, including the following steps:
[0048] Step A: 550g of citric acid, 120 g n-butanol and 30 g of a 55% sulfuric acid solution, placed in a reflux reaction kettle, heated to 135 ° C, constant temperature reaction for 5 h, decompression distillation, allowing excess n-butanol to volatilize, Get a mixture A;
[0049] Step B: It is weighed 450 g of acetic anhydride, 25 g of diiso-dioxionyl oxyter escene and 35 g of phthalate, adding the mixture A obtained by step A, opening reflow, heating to 90 ° C, separating funnel The separation solution was performed, and the hydroxide solution with a mass fraction of the oil was 10%, and then rinsed with water, and the decompression distillation was carried out to obtain a modifier.
preparation example 2
[0051] Preparation of a modifier, including the following steps:
[0052] Step A: 500 g of citric acid, 110 g n-butanol and 25 g of a mass fraction of 50% sulfuric acid solution, placed in a reflux reaction kettle, heated to 115 ° C, constant temperature reaction for 4 h, decompression distillation, allowing excess n-butanol to volatilize, Get a mixture A;
[0053] Step B: Weigh 400 g of acetic anhydride, 22 g of diisoleal diiso lysate and 32 g of phthalate, adding the mixture A obtained by step A, opening reflow, heating to 80 ° C, separating funnel Separation, rinse the hydroxide solution of 7% of the hydroxide solution of 7%, then rinsed with water, and then evaporated to the modifier.
preparation example 3
[0055] Preparation of a modifier, including the following steps:
[0056] Step A: 450g of citric acid, 100 g n-butanol and 20 g of a 35% sulfuric acid solution, placed in a reflux reaction kettle, heated to 100 ° C, constant temperature reaction for 3 h, distilled pressure reduction, and allowed excess n-butanol to volatilize, Get a mixture A;
[0057] Step B: 350 g of acetic anhydride, 20 g of dirabus or 30 g of phthalate diisoleyl oxide, adding the mixture A obtained by step A, opening reflow, heating to 70 ° C, separating funnel Separation, rinse the oil-based mass fraction of 5%, rinsed with water, and then evaporated, and the modifier is obtained.
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