Compound preservative as well as preparation method and application thereof
A technology for compounding preservatives and compounds, used in additives, lubricating compositions, petroleum industry and other directions, can solve the problems of poor environmental friendliness, poor viscosity-temperature performance, and difficult to remove odors, and achieves improved water solubility, wear resistance, and Good corrosion and anti-corrosion effect, improve the effect of anti-freezing performance
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Embodiment 1
[0071] This embodiment provides a composite preservative, including alkanolamide phosphate, benzotriazole, monoethanolamine, diethanolamine, monoisopropanolamine and diglycolamine.
[0072] Its preparation method is as follows:
[0073] (1) 17 parts of caprylic acid, 10 parts of n-dodecanedioic acid, 10 parts of oleic acid, 10 parts of 21 carbon dimer acid, 6 parts of monoethanolamine, 8 parts of diethanolamine, 5 parts of monoisopropanolamine, Mix 4 parts of diglycolamine and react at 150°C for 100 minutes to obtain alkanolamide.
[0074] (2) Add phosphorus pentoxide in an equimolar amount to the alkanolamide to the reaction system, and react at 90° C. for 2 hours to obtain the alkanolamide phosphate.
[0075] (3) Mix alkanolamide phosphate, 6 parts of monoethanolamine, 4 parts of diethanolamine, 5 parts of monoisopropanolamine, 6 parts of diglycolamine and 3 parts of benzotriazole at 90°C, and cool to Room temperature (25 ℃), that is.
Embodiment 2
[0077] This embodiment provides a composite preservative, including alkanolamide phosphate, 2,5-dimercaptothiadiazole disodium salt, monoethanolamine, diethanolamine, monoisopropanolamine and diglycolamine.
[0078] Its preparation method is as follows:
[0079] (1) Mix 20 parts of sebacic acid, 15 parts of oleic acid, 12 parts of behenic dimer acid, 10 parts of diethanolamine, 10 parts of monoisopropanolamine, and 5 parts of diglycolamine, and react at 120°C for 120 minutes , to give alkanolamides.
[0080] (2) Add phosphorus pentoxide in an equimolar amount to the alkanolamide to the reaction system, and react at 60° C. for 2.5 hours to obtain the alkanolamide phosphate.
[0081] (3) Mix alkanolamide phosphate, 5 parts of diethanolamine, 5 parts of monoisopropanolamine, 10 parts of diglycolamine and 5 parts of 2,5-dimercaptothiadiazole disodium salt at 60°C, Cool to room temperature (25 ° C), that is, too.
Embodiment 3
[0083] This embodiment provides a composite preservative, including alkanolamide phosphate, tolyltriazole, monoethanolamine, diethanolamine, monoisopropanolamine and diglycolamine.
[0084] Its preparation method is as follows:
[0085] (1) Mix 18 parts of capric acid, 18 parts of oleic acid, 8 parts of behenic acid dimer acid, 10 parts of monoethanolamine, 8 parts of monoisopropanolamine, and 5 parts of diglycolamine, and react at 180°C for 90 minutes. Alkanolamides are obtained.
[0086] (2) Add phosphorus pentoxide in an equimolar amount to the alkanolamide to the reaction system, and react at 100° C. for 1.5 h to obtain the alkanolamide phosphate.
[0087] (3) Mix alkanolamide phosphate, 8 parts of monoethanolamine, 4 parts of monoisopropanolamine, 10 parts of diglycolamine and 3 parts of methylbenzotriazole at 100°C, and cool to room temperature (25 ℃), that is.
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