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Rare-earth-doped optical fiber with optimized background loss and preparation method of rare-earth-doped optical fiber

A rare earth-doped, optical fiber technology, applied in lasers, gaseous chemical plating, laser parts, etc., to achieve the effect of improving stress defects, low attenuation, and optimizing background loss

Pending Publication Date: 2022-05-17
YANGTZE OPTICAL FIBRE & CABLE CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0005] Aiming at the above defects or improvement needs of the prior art, the present invention provides a rare earth-doped optical fiber and its preparation method, which can be effectively used in the preparation of optical fiber preforms by using a rare earth halide evaporation system and a plasma vapor deposition (PCVD) process. Alkali metal doping is carried out during the process, and the same alkali metal element doping is set in the core layer and the transition cladding layer; thereby improving the viscosity matching between the cladding layer and the core layer of the preform and reducing the viscosity difference during the preparation process The stress defect generated reduces the core back-to-bottom loss of the fiber

Method used

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  • Rare-earth-doped optical fiber with optimized background loss and preparation method of rare-earth-doped optical fiber
  • Rare-earth-doped optical fiber with optimized background loss and preparation method of rare-earth-doped optical fiber
  • Rare-earth-doped optical fiber with optimized background loss and preparation method of rare-earth-doped optical fiber

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preparation example Construction

[0054] The invention provides a method for preparing a rare earth-doped optical fiber with optimized background loss. The rare earth-doped optical fiber includes a core layer, a transitional cladding layer and a pure silicon cladding layer arranged in sequence from the inside to the outside, and the core layer and the transitional cladding layer are multi-component doped Miscellaneous silicon dioxide layer; Wherein, method comprises:

[0055] The core layer is prepared by using a rare earth halide evaporation system combined with PCVD process; the doping materials in the core layer include aluminum, ytterbium, phosphorus, and one or more alkali metal elements; the doping concentration of alkali metal elements is based on their oxides Formal calculation, the average concentration of alkali metal oxide doped in the core layer is 100ppm ~ 1000ppm;

[0056] The transition cladding layer is prepared by using a rare earth halide evaporation system combined with PCVD technology; the ...

Embodiment 1

[0063] The optical fiber core layer contains oxides of aluminum, ytterbium, phosphorus, and alkali metals, and they are all approximately uniformly distributed. Among them, the aluminum oxide (Al 2 o 3 ) with a doping concentration of 13000ppm, ytterbium oxide (Yb 2 o 3 ) The doping concentration is 2400ppm, phosphorus oxide (P 2 o 5 ) with a doping concentration of 20000ppm, alkali metal oxides (K 2 The content of O) is 100ppm, the fiber core layer radius R1 is 15um, the core layer relative refractive index difference is Δn1 is 0.095%, contains the oxide of aluminum, phosphorus, alkali metal in the transitional cladding, and is approximate uniform distribution, wherein Aluminum oxide in the cladding (Al 2 o 3 ) The doping concentration is 1500ppm, phosphorus oxide (P 2 o 5 ) The doping concentration is 1600ppm, the alkali metal oxide (K 2 The content of O) is 50ppm, the radius R2 of the cladding is 60um, the relative refractive index difference of the cladding is Δn2...

Embodiment 2

[0065] The optical fiber core layer contains oxides of aluminum, ytterbium, phosphorus, fluorine, and alkali metals, and they are all approximately uniformly distributed. Among them, the aluminum oxide (Al 2 o 3 ) with a doping concentration of 15000ppm, ytterbium oxide (Yb 2 o 3 ) The doping concentration is 2500ppm, phosphorus oxide (P 2 o 5 ) doping concentration is 30000ppm, alkali metal oxide (K 2 The content of O) is 50ppm, the fiber core layer radius R1 is 10um, the relative refractive index difference of the core layer is Δn1 and is 0.08%, and the oxides of aluminum, phosphorus and alkali metals are included in the transition cladding, and are approximately evenly distributed, wherein Aluminum oxide in the cladding (Al 2 o 3 ) The doping concentration is 1000ppm, phosphorus oxide (P 2 o 5 ) with a doping concentration of 1300ppm, alkali metal oxides (K 2 The content of O) is 100ppm, the radius R2 of the cladding is 40um, the relative refractive index differenc...

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Abstract

The invention provides a back-to-bottom loss optimized rare earth doped optical fiber, which comprises a core layer, a transition cladding and a pure silicon cladding which are sequentially arranged from inside to outside, and is characterized in that the core layer and the transition cladding are both multi-element doped silicon dioxide layers; doped materials in the core layer comprise aluminum, ytterbium, phosphorus and one or more alkali metal elements; the doping concentration of the alkali metal element is calculated according to the oxide form of the alkali metal element, and the average concentration of the alkali metal oxide doped in the core layer is 50ppm-1000ppm; doped materials in the transition cladding comprise fluorine, phosphorus and one or more alkali metal elements; the doping concentration of the alkali metal element is calculated according to the oxide form of the alkali metal element, and the average concentration of the alkali metal element doped in the transition cladding is 500 ppm to 300 ppm; wherein alkali metal elements doped in the core layer and the transition cladding are the same. According to the invention, the core layer and the transition cladding can form good viscosity matching through the doping of the alkali metal, thereby reducing the defects and stress loss in the preparation of the optical fiber, and further optimizing the back bottom loss of the rare earth-doped optical fiber.

Description

technical field [0001] The invention relates to the field of optical fiber technology, in particular to a rare earth-doped optical fiber with optimized background loss and a preparation method thereof. Background technique [0002] With the rapid development of optical fiber communication technology, the use of optical fiber is becoming more and more extensive. The overall situation is prosperous, in which optical fibers are not only widely used in conventional communication fields, but also in consumer electronics, material processing and other industries. Active rare earth doped fiber can not only be used as the key raw material in fiber laser, but also can be used in the production of optical fiber communication devices such as optical amplifiers, wavelength conversion and other optical fiber devices. [0003] At present, the mainstream preparation method of rare earth doped preform is modified chemical vapor phase method (MCVD). Most of the research institutions and ent...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): H01S3/067C23C16/50C23C16/40C23C16/24
CPCH01S3/06733H01S3/06716C23C16/50C23C16/402C23C16/24
Inventor 郑伟汪松雷高清钟力汪亨袁飚曹蓓蓓
Owner YANGTZE OPTICAL FIBRE & CABLE CO LTD
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