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Tar residue treatment method

A treatment method and tar residue technology, which is applied in the field of coal chemical industry, can solve the problems of high purchase cost and operation and maintenance cost of centrifugal equipment, insufficient mechanical centrifugal separation effect, and increased production cost of extraction agent, so as to reduce tar residue treatment Effects of equipment and materials, saving processing costs, and avoiding waste of resources

Active Publication Date: 2022-07-01
内蒙古正能化工集团有限公司
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, there are still many shortcomings in various treatment methods. For example, it is difficult to find an efficient, green and environmentally friendly organic solvent in solvent extraction and separation, and the higher cost of the extraction agent will further increase the production cost; the effect of mechanical centrifugation is not thorough enough to easily cause Subsequent processing is inconvenient, and the purchase cost and operation and maintenance cost of centrifugal equipment are high, so it is not suitable for application in most coal enterprises; resources are not fully utilized for coal blending coking or directly used as fuel, and even cause excessive pollutant emissions

Method used

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Embodiment 1

[0029] The present embodiment provides a tar residue treatment method, such as figure 1 shown, it includes:

[0030] S1, primary separation treatment: tar residue is placed in a high temperature alkaline liquid environment, stirring and separation obtains primary separation tar residue and liquid product, and the liquid product is carried out to stand for stratification, and separate primary separation tar and alkaline liquid;

[0031] S2, secondary separation treatment: carry out pressure filtration to the described primary separation tar residue, obtain secondary separation tar residue and secondary separation tar;

[0032] S3, tertiary separation treatment: carry out high-temperature dry distillation on the secondary separation tar residue to obtain crude gas and coke powder.

[0033] It should be noted that in the high temperature alkaline liquid environment, the viscosity of the tar residue is reduced, and the coal tar in it is easier to separate. At the same time, stirr...

Embodiment 2

[0044] This embodiment provides a tar residue treatment system, such as image 3 As shown, it can be used to realize the tar residue treatment method in the first embodiment. The system of this embodiment includes a high temperature alkaline liquid environment unit 10, a stirring device 20, a slag extraction device 30, a static layering device, a filter press device 40 and a first a carbonization device 50;

[0045] Both the stirring device 20 and the slag extraction device 30 are arranged in the high temperature alkaline liquid environment unit 10, the liquid outlet of the high temperature alkaline liquid environment unit 10 is communicated with the liquid inlet of the static layering device, and the slag extraction device 30 has a liquid outlet. The discharge port 302 communicates with the feed port 401 of the filter press device 40 , and the slag discharge port 402 of the filter press device 40 communicates with the feed port 501 of the first carbonization device 50 .

[0...

Embodiment 3

[0064] The present embodiment provides a tar residue treatment method, such as Figure 4 As shown, it is basically the same as a tar residue treatment method described in Example 1, which will not be repeated here. The difference is: in the initial separation treatment step, the temperature of the furnace gas in the traditional coking route is increased, and then the The collected high-temperature tar residue mixed with ammonia water after spray cooling with ammonia water is directly stirred as the tar residue placed in the high-temperature alkaline liquid environment, and the tar residue and the tar-aqueous ammonia mixture are separated to obtain the first separation. The tar-ammonia-water mixture is allowed to stand for stratification, and the primary separation tar and ammonia-water are separated.

[0065] It should be noted that the temperature of the outgoing gas in the traditional coking route can be increased by increasing the flow rate of the return gas and air. The or...

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Abstract

The invention provides a tar residue treatment method which comprises the following steps: firstly, putting tar residues in a high-temperature alkaline liquid environment to reduce the viscosity, and meanwhile, carrying out primary separation on the tar residues by utilizing a stirring effect; carrying out secondary filter pressing separation on the primarily separated tar residue, and finally carrying out high-temperature dry distillation on the secondarily separated tar residue to obtain raw gas and coke powder. According to the method, efficient and thorough recovery of the tar residues can be realized through three-step separation treatment of the tar residues, and products such as coal tar and coke powder generated in each separation process can be sold or used by themselves, so that various problems caused by improper treatment of the tar residues are avoided, and additional economic benefits are brought to enterprises; meanwhile, the treatment steps are simple and easy to implement, no high-cost and high-pollution equipment or materials are needed, the cost is low, environment friendliness is achieved, and large scale and continuity are quite easy to achieve.

Description

Technical field: [0001] The invention relates to the technical field of coal chemical industry, in particular to a tar residue treatment method. Background technique: [0002] In the traditional coking route, under the condition that the coke oven gas is cooled by ammonia water spray in the gas collector or primary cooler, the organic compounds with high boiling point will be condensed to form coal tar. Mixed with coal tar to form tar residue. Tar residue is a viscous waste residue. The main components are coal dust, coke powder, coal tar, asphaltenes, polycyclic aromatic hydrocarbons and other carbon-containing substances. They are toxic and harmful solid waste residues. Improper handling will not only cause environmental pollution, but also It will cause waste of resources. Some of the high-boiling polycyclic aromatic hydrocarbons will produce strong carcinogen benzopyrene when they are not completely burned, which will seriously pollute the atmosphere and endanger people...

Claims

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Application Information

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IPC IPC(8): C10B53/00C10B57/00C10B57/08
CPCC10B53/00C10B57/00C10B57/08
Inventor 杨瑞才李玉奎李玉广赵博李彦雄白莉苗文莉宋晓庆谢安禄高保军张勋飞吴永利王建雄刘树小苗栋
Owner 内蒙古正能化工集团有限公司