Preparation method of carrier transport film and preparation method of quantum dot light-emitting diode
A quantum dot luminescence and carrier technology, which is applied in semiconductor/solid-state device manufacturing, semiconductor devices, electrical components, etc., can solve the problem of low carrier mobility, reduce roughness, improve microscopic appearance, film The effect of layer crystallinity improvement
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[0028] A first aspect of the embodiments of the present application provides a method for preparing a carrier transport film, such as figure 1 shown, including the following steps:
[0029] S01: Provide substrate;
[0030] S02: prepare a carrier transport film composed of N-layer stacked metal oxide semiconductor layers on the substrate;
[0031] Wherein, the preparation steps of each metal oxide semiconductor layer include: first depositing metal oxide semiconductor material, and then scanning annealing with electron beam;
[0032] N is a positive integer, N≥2.
[0033] The preparation method of the carrier transport film provided by the present application adopts the technology of N-layer metal oxide semiconductor layer stacking and layering preparation, that is, each metal oxide semiconductor layer is firstly deposited metal oxide semiconductor material, and then electron beam Scanning annealing; such a preparation method can improve the microscopic morphology of the car...
Embodiment 1
[0090] An upright quantum dot light-emitting diode, from bottom to top, comprises: an ITO substrate (anode), a hole injection layer, a hole transport layer, a quantum dot light-emitting layer, an electron transport layer, and a cathode. Its preparation process includes the following steps:
[0091] Step S1: on the ITO substrate (anode), spin-coating PEDOT:PSS at a rotational speed of 5000 rpm and a time of 30 seconds, followed by heating at 150° C. for 15 minutes, and standing to cool for 5 minutes to obtain a hole injection layer.
[0092] Step S2: spin-coating TFB (8 mg / mL) on the above hole injection layer with a rotational speed of 3000 rpm and a time of 30 seconds, followed by heating at 80° C. for 10 minutes, and standing to cool for 5 minutes to obtain hole transport Floor.
[0093] Step S3: spin-coating quantum dots (20 mg / mL) on the hole transport layer under the conditions of a rotational speed of 2000 rpm and a time of 30 seconds to obtain a quantum dot light-emitt...
Embodiment 2
[0102] An upright quantum dot light-emitting diode, from bottom to top, comprises: an ITO substrate (anode), a hole injection layer, a hole transport layer, a quantum dot light-emitting layer, an electron transport layer, and a cathode. Its preparation process includes the following steps:
[0103] Step S1: on the ITO substrate (anode), spin-coating PEDOT:PSS at a rotational speed of 5000 rpm and a time of 30 seconds, followed by heating at 150° C. for 15 minutes, and standing to cool for 5 minutes to obtain a hole injection layer.
[0104] Step S2: spin-coating TFB (8 mg / mL) on the above hole injection layer with a rotational speed of 3000 rpm and a time of 30 seconds, followed by heating at 80° C. for 10 minutes, and standing to cool for 5 minutes to obtain hole transport Floor.
[0105] Step S3: spin-coating quantum dots (20 mg / mL) on the hole transport layer under the conditions of a rotational speed of 2000 rpm and a time of 30 seconds to obtain a quantum dot light-emitt...
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