Long-acting sunscreen mosquito-repellent emulsion and preparation method thereof
A mosquito repellent and long-acting technology is applied in the field of long-acting sunscreen mosquito repellent lotion and its preparation, which can solve the problems of transdermal absorption and unsustainable repellent effect, so as to prolong the effective protection time, prevent the acne-causing effect, and improve the sunscreen effect. Effect
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Embodiment 1
[0035] To prepare long-lasting sunscreen and mosquito repellent particles:
[0036] S1. Add isopropyl tris (dioctyl pyrophosphate acyloxy) titanate into deionized water, disperse evenly, immediately add nanoporous zinc oxide, stir for 30min, suction filtration, and vacuum dry; The mass ratio of zinc, titanate and deionized water is 15:0.5:100;
[0037] S2. Heat and melt 3-(4-methylbenzylidene) camphor, add it together with cinnamon oil and ethyl butylacetamidopropionate into a circulating pneumatic mixer, mix at 75°C for 5 minutes, and then add surface modification nanoporous zinc oxide, continue to mix for 20min, discharge, and cool to obtain a core layer;
[0038] S3. Dissolve lignin in acetone, spray and deposit it on the surface of the core layer to form a shell layer, and dry in vacuum.
[0039] In the long-acting sunscreen and mosquito repellent particles, the mass ratio of nanoporous zinc oxide, 3-(4-methylbenzylidene) camphor, cinnamon oil, ethyl butylacetaminopropio...
Embodiment 2
[0046] To prepare long-lasting sunscreen and mosquito repellent particles:
[0047] S1. Add isopropyl tris (dioctyl pyrophosphate acyloxy) titanate into deionized water, disperse evenly, immediately add nanoporous zinc oxide, stir for 30min, suction filtration, and vacuum dry; The mass ratio of zinc, titanate and deionized water is 20:0.7:100;
[0048] S2. Heat and melt 3-(4-methylbenzylidene) camphor, add cinnamon oil and ethyl 10-undecenoylamino methyl propionate into a circulating pneumatic mixer, and mix at 72°C for 5min , then add the surface modified nanoporous zinc oxide, continue to mix for 30min, discharge and cool to obtain the core layer;
[0049] S3. Dissolve lignin in acetone, spray and deposit it on the surface of the core layer to form a shell layer, and dry in vacuum.
[0050] In the long-acting sunscreen and mosquito repellent particles, the mass ratio of nanoporous zinc oxide, 3-(4-methylbenzylidene) camphor, cinnamon oil, ethyl 10-undecenoylaminomethylprop...
Embodiment 3
[0057] To prepare long-lasting sunscreen and mosquito repellent particles:
[0058] S1. Add isopropyl tris (dioctyl pyrophosphate acyloxy) titanate into deionized water, disperse evenly, immediately add nanoporous alumina, stir for 40min, suction filtration, and vacuum dry, then the nanoporous oxidation The mass ratio of aluminum, titanate and deionized water is 18:0.6:100;
[0059] S2. Heat and melt 3-(4-methylbenzylidene) camphor, add it to a circulating pneumatic mixer together with cinnamon oil and ethyl butylacetamidopropionate, mix at 75°C for 4 minutes, and then add surface modification nanoporous alumina, continued to mix for 25min, discharged, cooled to obtain a core layer;
[0060] S3. Dissolve lignin in acetone, spray and deposit it on the surface of the core layer to form a shell layer, and dry in vacuum.
[0061] In the long-acting sunscreen and mosquito repellent particles, the mass ratio of nanoporous alumina, 3-(4-methylbenzylidene) camphor, cinnamon oil, eth...
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