Method for in-situ generating ultrafine silver particles in textile
An in-situ generation and textile technology, applied in textiles, papermaking, fiber processing, etc., can solve the problems of poor durability and high cost, and achieve the effects of good dispersion, good anti-electromagnetic radiation, and small particle size
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Embodiment 1
[0021] First use 2% sodium hydroxide solution to treat the fabric fiber to remove the dirt on the surface of the fabric, then wash it with water, dry it, and then place the fabric in 10g / l SnCl 2 In aqueous solution, Sn 2+ After being adsorbed to the fiber surface of the textile, it is dried, and with the assistance of ultrasound, the surface-treated fabric is immersed in a mixed solution of silver nitrate-dissolved ethanol and water (the water content is 5%), and the silver nitrate solution is Concentration is 3×10 -3 M. The reaction temperature is room temperature, and the silver grows and deposits on the fiber surface.
Embodiment 2
[0023] First use 2% sodium hydroxide solution to treat the fabric fiber to remove the dirt on the surface of the fabric, then wash it with water, dry it, and then place the fabric in 15g / l SnCl 2 In aqueous solution, Sn 2+ Adsorbed to the fiber surface of the textile and then dried, under the action of ultrasound, the adsorbed Sn 2+ The fabric is immersed in the mixed solution of ethanol and water containing silver nitrate (the content of water is 5%), the reaction temperature is room temperature, silver grows and deposits on the fiber surface, utilizes Sn 2+ Metal ions are reduced to realize the link between metal and fiber. Silver nitrate is then added. The concentration of silver nitrate is 9×10 -3 M.
Embodiment 3
[0025] First use 2% sodium hydroxide solution to treat the fabric fiber to remove the dirt on the surface of the fabric, then wash it with water, dry it, and then place the fabric in 12g / l SnCl 2 In aqueous solution, Sn 2+ Adsorbed to the fiber surface of the textile and then dried, under the action of ultrasound, the adsorbed Sn 2+ The fabric is immersed in the mixed solution of ethanol and water containing silver nitrate (the content of water is 20%), the reaction temperature is room temperature, silver grows and deposits on the fiber surface, utilizes Sn 2+ Metal ions are reduced to realize the link between metal and fiber. Silver nitrate is then added. The concentration of silver nitrate is 6×10 -3 M.
[0026] Textiles can be cotton, polyester, acrylic, etc.
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