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Chinese medicine composition and its prepn process and quality control method

A quality control method and composition technology, which is applied in the direction of drug combination, testing of pharmaceutical preparations, pharmaceutical formulations, etc., and can solve problems such as toxic side effects and insignificant effects

Inactive Publication Date: 2007-01-03
吴逸芳
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, most of the chemical drugs for the treatment of such diseases have relatively large toxic and side effects, and there are many types of traditional Chinese medicines for the treatment of such diseases, but most of them have insignificant effects

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0064] Prescription: 30kg of horse money seed powder, 5kg of soil beetle

[0065] Sichuan Achyranthes 5kg Licorice 5kg

[0066] Ephedra 5kg Frankincense 5kg

[0067] Myrrh 5kg Scorpion 5kg

[0068] Stiff silkworm 5kg Cangzhu 5kg

[0069] Preparation method: the above ten flavors, crushed into fine powder, sieved through a 100 mesh sieve, add 1200g of microcrystalline cellulose, mix well, use 1% hypromellose 60% ethanol solution as a binder, granulate (20 mesh ), dry at 60°C, granulate, add 50g magnesium stearate to the dry granules, and add an appropriate amount of starch to adjust the total amount to 80kg, mix well, and compress into tablets, each 0.3g, and coating, ready to get.

Embodiment 2

[0071] Prescription: Horse Money Seed Powder 400g Soil Turtle Worm 80g

[0072] Sichuan Achyranthes 80g Licorice 80g

[0073] Ephedra 80g Frankincense 80g

[0074] Myrrh 80g Whole Scorpion 80g

[0075] Stiff silkworm 80g Cangzhu 80g

[0076] Preparation method: crush the above ten medicines, add 110g of microcrystalline cellulose, mix well, and pan into pills, ready to be obtained.

Embodiment 3

[0078] Quality inspection of the tablets made in Example 1:

[0079] Quantitative:

[0080] (1) High performance liquid chromatography

[0081] Chromatographic conditions and system suitability tests use octadecylsilane bonded silica gel as filler; 10:90-85 acetonitrile-0.2% phosphoric acid as mobile phase, detection wavelength 254±2nm, flow rate 1.0±0.2ml / min. The number of theoretical plates calculated by Strychnine should not be less than 1500.

[0082] Preparation of the reference substance solution Accurately weigh the strychnine reference substance, add methanol, acetonitrile or mobile phase to make a solution containing strychnine at 20 μg / ml, which is obtained.

[0083] Preparation of the test solution: Take 0.6g of this product, which is equivalent to the medicinal material of Strychnoides powder, accurately weigh it, place it in a stoppered Erlenmeyer flask, add lye, place it, accurately add 50ml of chloroform, close the stopper, and weigh it. Let stand or reflux or extr...

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Abstract

The present invention discloses one kind of Chinese medicine composition, and belongs to the field of Chinese medicine technology. The Chinese medicine composition is prepared with nux vomica, ground beetle, cyathula root, licorice, Chinese ephedra and other Chinese medicinal materials, and through a certain technological process. The Chinese medicine composition has obvious lumbago treating effect. The present invention also discloses the preparation process and quality control method of the Chinese medicine composition.

Description

Invention field [0001] The invention relates to a traditional Chinese medicine composition, in particular to a traditional Chinese medicine composition for treating low back pain, belonging to the field of traditional Chinese medicine. Background technique [0002] Lumbar Common Disease is a common clinical disease in the Department of Orthopedics and Traumatology of Traditional Chinese Medicine. The disease is mostly caused by cold pathogen invasion, choroidal obstruction and other factors. It should be treated to relieve swelling and pain, evacuate cold pathogens, and warm meridians. At present, most of the chemical drugs used to treat such diseases have relatively large toxic and side effects. There are many kinds of traditional Chinese medicines for the treatment of such diseases, but most of the effects are not significant. [0003] The purpose of the present invention is to overcome the shortcomings of the existing medicines and provide a traditional Chinese medicine compos...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K36/56A61P29/00A61P19/00G01N30/02G01N30/90G01N33/15A61K35/64A61K35/646
Inventor 吴逸芳
Owner 吴逸芳
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