Preparation method of phospholipid functional photoluminous reinforced type nuclear shell structure quantum point
A core-shell structure, photoluminescence technology, applied in the field of composite materials, can solve the problems of non-stable chemical bond connection, no biological and chemical stability, etc., achieve good colloidal stability, enhance photoluminescence performance, photoluminescence Performance-enhancing effects
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Embodiment 1
[0027] Using cadmium oxide, selenium, dimethyl zinc and bistrimethyl silicon sulfide as the initial raw materials, cadmium selenide / zinc sulfide type core-shell structure quantum dots are formed after solution cooling and crystallization at high temperature, and then react with phospholipids with mercapto groups, through The interaction between zinc and sulfur to prepare phospholipid-functionalized photoluminescence-enhanced core-shell quantum dots.
[0028] Step a: Add 0.0615 grams of cadmium oxide, 0.2211 grams of tetradecyl phosphonic acid and 3.7750 grams of trioctylphosphine oxide in a 25 ml flask, seal and feed into argon for protection, heat to 320 degrees Celsius, let the cadmium oxide Fully melt in the mixed solution of tetraalkylphosphonic acid and trioctylphosphine oxide.
[0029] Step b: reduce the temperature of the reaction system to 270 degrees Celsius, and add the stock solution of Group IV non-metal elements to the flask (this solution is prepared by dissolvin...
Embodiment 2
[0035] Using cadmium oxide, selenium, dimethyl zinc and bistrimethyl silicon sulfide as the initial raw materials, cadmium selenide / zinc sulfide type core-shell structure quantum dots are formed after solution cooling and crystallization at high temperature, and then react with phospholipids with mercapto groups, through The interaction between zinc and sulfur to prepare phospholipid-functionalized photoluminescence-enhanced core-shell quantum dots.
[0036] Step a: Add 0.01 gram of cadmium oxide, 0.01 gram of tetradecyl phosphonic acid and 0.01 gram of trioctylphosphine oxide in a 25 ml flask, seal it, feed it with argon for protection, heat to 320 degrees Celsius, and let the cadmium oxide Fully melt in the mixed solution of tetraalkylphosphonic acid and trioctylphosphine oxide.
[0037] Step b: reduce the temperature of the reaction system to 270 degrees Celsius, and add the stock solution of Group IV non-metallic elements to the flask (the solution is prepared by dissolvin...
Embodiment 3
[0043] Using cadmium oxide, selenium, dimethyl zinc and bistrimethyl silicon sulfide as the initial raw materials, cadmium selenide / zinc sulfide type core-shell structure quantum dots are formed after solution cooling and crystallization at high temperature, and then react with phospholipids with mercapto groups, through The interaction between zinc and sulfur to prepare phospholipid-functionalized photoluminescence-enhanced core-shell quantum dots.
[0044] Step a: add 1 gram of cadmium oxide, 1 gram of tetradecyl phosphonic acid and 10 grams of trioctylphosphine oxide in a 25 ml flask, seal and feed into argon for protection, heat to 320 degrees Celsius, let cadmium oxide Fully melt in the mixed solution of tetraalkylphosphonic acid and trioctylphosphine oxide.
[0045] Step b: reduce the temperature of the reaction system to 270 degrees Celsius, and add the stock solution of Group IV non-metallic elements to the flask (the solution is prepared by dissolving 1 gram of Group ...
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