Toner and developing device using the same
a technology of developing devices and toners, applied in the field of toners, can solve the problems of reducing the transfer efficiency and filming on the photoconductor surfa
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example 1
Production of Toner by Polymerization Method
Production of Toner Mother Particle 1
[0128] A monomer mixture comprising 80 parts by weight of styrene monomer, 20 parts by weight of butyl acrylate and 5 parts by weight of acrylic acid was added to an aqueous solution mixture containing 105 parts by weight of water, 1 part by weight of nonionic emulsifier (Emulgen 950, produced by Dai-ichi Kogyo Seiyaku Co., Ltd.), 1.5 parts by weight of anionic emulsifier (Neogen R, produced by Dai-ichi Kogyo Seiyaku Co., Ltd.) and 0.55 parts by weight of potassium persulfate, and polymerized at 70° C. for 8 hours with stirring in a nitrogen stream. By cooling after polymerization reaction, a milky white resin emulsion having a particle size of 0.25 μm was obtained.
[0129] Thereafter, 200 parts by weight of the resin emulsion obtained above, 20 parts by weight of polyethylene wax emulsion (Permarin PN, produced by Sanyo Chemical Industries, Ltd.) and 7 parts by weight of phthalocyanine blue were dispe...
production example 1
of Toner
[0175] First, 0.8 parts by weight of hydrophobic silica having a mean primary particle size of 12 nm, which is a fluidity improving agent, and 0.7 parts by weight of hydrophobic silica having a mean primary particle size of 40 nm were added and mixed per 100 parts by weight of Toner Mother Particle 1 to prepare a toner.
[0176] Thereafter, toners containing 0.4 parts by weight of monodisperse spherical silica having a mean particle size distribution shown in Table 2, 0.5 parts by weight of hydrophobic titanium oxide of 20 nm, 0.2 parts by weight of hydrophobic titanium oxide having a particle size distribution of 200 to 750 nm in terms of the primary particle size and being treated with a negatively chargeable n-butyltrimethoxysilane coupling agent and further with zinc stearate, and 0.2 parts by weight of metal soap (fine particulate calcium stearate (M7StCa), produced by NOF Corporation) shown in Table 4 were produced and designated as Toner 1-1, Toner 1-2 and Toner 1-3, re...
example 2
[0190] Toners containing 0.7 parts by weight of hydrophobic silica having a mean primary particle size of 7 nm, which is a fluidity improving agent, 0.6 parts by weight of hydrophobic silica having a mean primary particle size of 40 nm, 0.4 parts by weight of hydrophobic titanium oxide having a mean primary particle size of 20 nm, 0.4 parts by weight of Monodisperse Spherical Silica 2 shown in Table 2, which was hydrophobed with a hexamethyldisilazane coupling agent, 0.2 parts by weight of hydrophobic titanium oxide having a particle size distribution of 200 to 750 nm in terms of the primary particle size and being treated with a negatively chargeable n-butyltrimethoxysilane coupling agent and further with zinc stearate, and 0.2 parts by weight of metal soap shown in Table 5, per 100 parts by weight of Toner Mother Particle 2 (mean particle size on the volume basis: 7.9 μm, mean particle size on the number basis: 7.0 μm, work function: 5.64 eV, sphericity: 0.976) of Example 1 were p...
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