Anticancer Chinese traditional extracts and a preparation process and an application thereof
A technology of anti-cancer activity and extracts, applied in the direction of medical preparations containing active ingredients, drug delivery, drug combination, etc., can solve the problems of increasing patient pain, improper application, and patients' susceptibility to infectious diseases, so as to ensure safety Sexuality and effectiveness, reducing toxic and side effects, good anticancer effect
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Embodiment 1
[0051] Take 100kg of Sage vine, add 800kg of water, boil and extract for 1 hour, filter, and the filtrate is set aside, add 700kg of water to the dregs, boil and extract for 1 hour, filter, combine the filtrate twice, and concentrate the combined filtrate to a relative density of 1.08 The dilute extract, the dilute extract through D101 macroporous adsorption resin, first eluted with water until colorless, discarded the water eluate, then eluted with 85% ethanol until colorless, collected the 85% ethanol The eluent, the 85% ethanol eluate after recovering ethanol is concentrated into a thick extract with a relative density of 1.11, and the thick extract is spray-dried to obtain a japonica extract containing 50% saponin, that is, the saponin content It is 50% Chinese medicine extract with anticancer activity.
Embodiment 2
[0053] Take 100kg of Aegypti sinensis, add 900kg of water, boil and extract for 2 hours, filter, and the filtrate is set aside, add 900kg of water to the dregs, boil and extract for 1 hour, filter, combine the two filtrates, concentrate to a relative density of 1.05, add ethanol to the ethanol content 40%, let it stand for 18 hours, take the supernatant, recover the ethanol from the supernatant to form a thin extract with a relative density of 1.02, pass the thin extract through D201 macroporous adsorption resin, and first elute with 15% ethanol To colorless, discard the 15% ethanol eluate, then elute with 60% ethanol until colorless, collect the 60% ethanol eluate, concentrate the 60% ethanol eluate after recovering ethanol to relative density The thick extract is 1.10, and the thick extract is dried under reduced pressure to obtain the extract of Aegypti japonica containing 40% saponin, that is, the Chinese medicine extract with anticancer activity with a saponin content of 4...
Embodiment 3
[0055] Take 100kg of Sage vine, add 1000kg of water, boil and extract for 2 hours, filter, and set aside the filtrate, add 900kg of water to the dregs, boil and extract for 1 hour, filter, add water to the filtrate, add 900kg of water to the dregs, boil and extract for 1 hour, filter , combined three filtrates, concentrated to a relative density of 1.05, added ethanol until the ethanol content was 95%, left standstill for 24 hours, took the supernatant, and reclaimed the ethanol from the supernatant to become a dilute extract with a relative density of 1.05, and dilute the dilute extract The extract was passed through D201 macroporous adsorption resin, first eluted with 20% ethanol until colorless, discarded the 20% ethanol eluate, then eluted with 50% ethanol until colorless, collected the 50% ethanol eluate , the 50% ethanol eluate after recovering ethanol is concentrated into a thick extract with a relative density of 1.09, and the thick extract is dried under reduced pressu...
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