Production method of medium and high pressure formed foil
A manufacturing method, medium and high pressure corrosion foil technology, applied in the direction of electrolytic capacitors, electrical components, circuits, etc., can solve the problem of poor electrical properties and water resistance of oxide films, poor water resistance film performance of foils, and foils are not practical To reduce the interference, excellent hydration resistance, and increase the specific volume
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Embodiment 1
[0027] Use medium and high pressure to corrode the foil, boil it in pure water above 98°C for 12 minutes, and then perform the first stage formation voltage at 85°C in a mixed solution of 5wt% boric acid and 0.3wt% ammonium borate (or sodium) aqueous solution When the voltage reaches 250V, keep the voltage constant for 10 minutes; then carry out the second-stage formation at 85°C in 5wt% boric acid, 0.15wt% ammonium borate (or sodium) aqueous solution, and keep the voltage constant for 15 minutes when the voltage reaches 480V; then use 5wt% boric acid, 0.08wt% ammonium borate (or sodium) mixed solution was carried out at 85°C for the third-stage formation, and the voltage reached 580V for 30 minutes; then heat treatment was carried out at 480°C for 2.5 minutes; ℃, 5g / L phosphoric acid solution for 4.5 minutes; then carry out re-formation in the above-mentioned third-stage chemical solution; then carry out the second heat treatment at 480°C for 2.5 minutes; The second re-format...
Embodiment 2
[0029] Use medium and high pressure to corrode the foil, boil it in pure water above 98°C for 10 minutes, and then perform the first-level chemical formation at 85°C in a mixed solution of 6wt% boric acid and 0.2wt% ammonium borate (or sodium) aqueous solution, When the voltage reaches 250V, keep the voltage constant for 10 minutes; then carry out the second stage formation at 90°C in 5wt% boric acid, 0.15wt% ammonium borate (or sodium) aqueous solution, and keep the voltage constant for 15 minutes when the voltage reaches 480V; , 0.08wt% ammonium borate (or sodium) mixed solution at 90 ° C for the third level of chemical formation, when the voltage reaches 580 V constant voltage for 30 minutes; then heat treatment, the temperature is 500 ° C, the time is 2 minutes; The temperature in the L phytic acid aqueous solution is 60 °C, and the treatment time is 6 minutes; after that, it is re-formed in the above-mentioned third-level chemical conversion solution; then the second heat ...
Embodiment 3
[0031] Use medium and high pressure to corrode the foil, boil it in pure water above 98°C for 12 minutes, and then perform the first-level chemical formation at 85°C in a mixed solution of 6wt% boric acid and 0.3wt% ammonium borate (or sodium) aqueous solution, When the voltage reaches 250V, keep the voltage constant for 10 minutes; then carry out the second-stage formation at 85°C in 5wt% boric acid and 0.15wt% ammonium borate (or sodium) aqueous solution, and keep the voltage constant for 15 minutes when the voltage reaches 480V; , 0.08wt% ammonium borate (or sodium) mixed solution at 85 ° C for the third level of chemical formation, when the voltage reaches 580V constant voltage 30 minutes; then heat treatment, the temperature is 500 ° C, the time is 2.5 minutes; The temperature in the L ammonium hypophosphite solution is 70°C, and the treatment time is 8 minutes; after that, it is reformed in the above-mentioned third-stage chemical conversion solution; then, the second hea...
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