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Process for treating ammonia-nitrogen waste water

A technology for ammonia nitrogen wastewater and treatment methods, which is applied in the direction of combustion methods, osmosis/dialysis water/sewage treatment, chemical instruments and methods, etc., can solve the problems of ineffective treatment of high-concentration ammonia nitrogen wastewater, ammonia nitrogen wastewater discharge standards, etc., to achieve waste discharge Less, low operating costs, and the effect of reducing pollution

Active Publication Date: 2008-10-22
ZHEJIANG FENGDENG CHEM
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Problems solved by technology

[0004] The technical problem to be solved by the present invention is to provide a kind of ammonia nitrogen wastewater treatment with advanced technology, simple and easy process, low operating cost and less waste discharge in view of the above-mentioned problem of not being able to effectively treat high-concentration ammonia nitrogen wastewater and low-concentration ammonia nitrogen wastewater. method

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  • Process for treating ammonia-nitrogen waste water

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specific Embodiment approach

[0009] The main production process includes membrane filtration, kana recovery, ammonia water concentration, coal water slurry preparation, gas generation, conversion, wet desulfurization, PSA hydrogen extraction, synthesis and other steps.

[0010] Ammonia nitrogen waste water (flow rate 10.5-12.3 tons / hour) produced in the production process of amikacin is firstly filtered through a membrane filter, and the filtrate is ammonia containing 0.5%-0.6% (flow rate 8-9 tons / hour) Dilute ammonia water enters the isobaric recovery process to prepare concentrated ammonia water, which is then carbonized to produce ammonium bicarbonate. The retentate (flow rate: 2.5-3.3 t / h) enters the Kanakine recovery device, where Kanakine is extracted after hydrolysis and reused in the production of Amikacin. The organic waste water containing 3-5% ammonia nitrogen produced by kanaine recovery is pumped into the pulping process to prepare coal water slurry; the coal water slurry with a concentration...

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Abstract

A method for treating ammonia nitrogen wastewater is disclosed. The ammonia nitrogen wastewater is firstly filtered by a membrane filter, and dilute ammonia water filtered out is processed by isobaric pressure recycling to prepare concentrated ammonia water which is carbonized to produce ammonium bicarbonate. Trapped solution is firstly hydrolyzed to extract Kana alkali, and organic wastewater which contains ammonia nitrogen and is produced by the recycling of the trapped solution is used for preparing coal water slurry; the coal water slurry prepared, the concentration of which is 60 percent, together with pure oxygen by air separation are gasified and cracked at the temperature of 1350 DEG C to 1450 DEG C and the pressure of 1.3 MPa to produce CO, CO2, H2, N2 and water gas with trace amount of hydrogen sulfide; by changing the process, CO and water vapor react and produce CO2 and H2; trace amount of hydrogen sulfide is removed by carrying out desulfurization by a wet process; some gas is treated by carbonization process to remove CO2, and ammonium carbonate is produced at the same time. The left gas is treated by PSA hydrogen-extraction process to prepare high-purity hydrogen as finished product or for preparing product liquid ammonia. The method of the invention changes waste into valuable and requires low operating cost.

Description

technical field [0001] The invention relates to a method for treating ammonia nitrogen wastewater Background technique [0002] In the production of amikacin, the treatment of ammonia-nitrogen wastewater is very important. If the treatment of ammonia-nitrogen wastewater cannot meet the requirements, it will not only pollute the environment, but also affect the comprehensive recycling and utilization of the high-energy-consuming product kanarine in the wastewater. [0003] At present, my country's ammonia nitrogen wastewater treatment methods generally include physical and chemical methods, combined biochemical methods, and new biological nitrogen removal methods. The above processes all have disadvantages such as complex process, large investment, immature technology, difficulty in control, secondary pollution, and high operating costs. How to economically and effectively treat high-concentration ammonia-nitrogen wastewater and low-concentration ammonia-nitrogen wastewater t...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C02F1/44F23G7/04C01C1/26C01B3/48C01C1/04
Inventor 王明霞何先标徐永萍唐量华冯庆贤张小杨
Owner ZHEJIANG FENGDENG CHEM
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